不同变质程度煤的高分辨率透射电镜分析

利用高分辨率透射电子显微镜(HRTEM)分析了三种不同变质程度煤样的结构特征。基于傅里叶-反傅里叶变换方法,并结合Matlab、Arcgis和Auto CAD软件,通过图像分析技术,获得了HRTEM照片的晶格条纹参数。结果表明,三种煤样的晶格条纹呈现不同特征,按条纹长度分别归属于1×1-8×8共计八个类型。以3×3为临界点,在1×1和2×2中,ML-8中芳香层片的比例高于DP-4和XM-3;在3×3-8×8中,ML-8中芳香层片的比例低于DP-4和XM-3。对比HRTEM和XRD参数d002发现,随着镜质组反射率的增加d002都呈现递减趋势。     

The Crystallization of Poly (3-dodecyltbiophene) in an Oriented Solidification Environment

Poly (3-alkylthiophenes) (P3ATs) have made up of a family of conductive polymerswhich are soluble, fusible and processable, since the introduction of flexible alkyl sidechains"'. It is generally accepted that P3ATs can form similar layered structures. inwhich the thiophene rings possess planarity and the side chains act as spacers'-'. Whenthe number. of 'carbon atoms of alkyl side chains is more than 10, some orderlyarrangements will occur for side chains betWeen the' layers'. It has been w…     

Tchebycheff-Fourier级数的Vallce Poussin平均逼近函数类Lip α

本文考虑用ＴｃｈｅｂｙｃｈｅｆＦｏｕｒｉｅｒ级数的ＶａｌéｅＰｏｕｓｉｎ平均逼近函数类Ｌｉｐα,在ｆ（ｘ）∈Ｃ［－１,１］时获得了逼近阶及逼近误差的表达式,推广并较大地改进了文献［１,２］中的有关结果．     

Correlation Analysis of the Fluorescence Data of Some Benzaldehyde Derivatives by the Dual-Parameter Equation

Ithasbeenrecentlyestablishedthattherearefourcategoriesofpossiblecircumstancesforcorrelati0nanalyses0fradicalreactivitiesandspectralpropertiesbyEq.(l),Eq.(2)andEq.(3)."(I)Bothp0larandspin-del0calisationeffectsaretwortant,O.2l.O.(III)Thespin-delocalizationeffectspredominate,lpmdpJJ'I<0.2.(IV)Nocorrelationcanbeachieved.Wehavef0undthatthebehavi0roffluorescencespectraldataofsomestyrenes,'bycorrelati0nanalysiswiththedual-parameterEq.(…     

A concise and diversity-oriented strategy for the synthesis of benzofurans and indoles via Ugi and Diels-Alder reactions

A one-pot synthesis of diverse benzofurans and indoles from readily available starting materials was achieved via the sequential Ugi four-component reaction, intramolecular Diels-Alder reaction, and oxidative aromatization.     

On（N,U）-Coherence of Modules and Rings

Let U be a flat right R-module and N an infinite cardinal number.A left R-module M is said to be (N,U)-coherent if every finitely generated submodule of every finitely generated M-projective module in σ[M] is (N,U)-finitely presented in σ[M].It is proved under some additional conditions that a left R-module M is (N,U)-coherent if and only if Л^Ni∈I U is M-flat as a right R-module if and only if the (N,U)-coherent dimension of M is equal to zero.We also give some characterizations of left (N,U)-coherent dimension of rings and show that the left N-coherent dimension of a ring R is the supremum of (N,U)-coherent dimensions of R for all flat right R-modules U.     

Polarization-independent self-collimating bends and beam splitters in photonic crystals

Polarization independent bends and beam splitters for transverse electric (TE) and transverse magnetic (TM) polarizations have been demonstrated in two-dimensional (2D) photonic crystals (PhCs). In virtuel of equi-frequency contour analysis and finite-difference time-domain calculations, self-collimation behaviors for TE- and TM-polarizations are achieved at the same frequency. Simulation results show a 90-degree bend with 90% efficiency and beam splitters with about 96% total efficiency for both TE- and TMpolarizations, where the light is self-guided by the self-collimation effect. Such bends and beam splitters are expected to play important roles in optical devices where polarization insensitivity is needed.