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101.
A. A. Lamberov E. V. Dement’eva Kh. Kh. Gil’manov S. R. Egorova N. V. Romanova 《Russian Journal of Applied Chemistry》2006,79(9):1453-1457
The effect of the paste molding pressure on the physicomechanical and texture characteristics of catalysts was studied. An indirect criterion is suggested to evaluate the molding pressure in industrial extruders, whose optimal value ensures good physicomechanical properties of the catalysts and kinetic control over the catalyzed reaction. The results obtained were verified in paste molding on various industrial extruders, and this enabled the optimal choice of the molding equipment. 相似文献
102.
A. V. Kel’manov L. V. Mikhailova 《Computational Mathematics and Mathematical Physics》2006,46(1):165-181
The problem of joint a posteriori detection of reference fragments in a quasi-periodic sequence and its partition into segments containing series of recurring fragments from the reference tuple is solved. It is assumed that (i) an ordered reference tuple of sequences to be detected is given, (ii) the number of desired fragments is known, (iii) the index of the sequence term corresponding to the beginning of a fragment is a deterministic (not random) value, and (iv) a sequence distorted by an additive uncorrelated Gaussian noise is available for observation. It is established that the problem consists in testing a set of hypotheses about the mean of a random Gaussian vector. The cardinality of the set grows exponentially as the vector dimension (i.e., the sequence length) increases. An efficient a posteriori algorithm producing a maximum-likelihood optimal solution to the problem is substantiated. Time and space complexity bounds related to the parameters of the problem are derived. The results of numerical simulation are presented. 相似文献
103.
The atomic structure and magnetic and electric properties of the Cr0.5TiSe2-Cr0.5TiTe2 system of intercalated phases were studied in detail by gradually replacing selenium by tellurium. It was revealed that this replacement changes the crystalline structure from monoclinic in the initial compounds to hexagonal in the compounds containing various types of chalcogen atoms; this is accompanied by disordering of chromium atoms in the van der Waals gaps. The electrical resistance and magnetic characteristics vary nonmonotonically on replacement of selenium by tellurium, which is associated with a change in the degree of atomic disordering during the transition from Cr0.5TiSe2 to Cr0.5TiTe2. 相似文献
104.
The viscosity behavior, index of refraction, and density of dilute polycaproamide solutions in DMAc containing lithium chloride have been studied. On the basis of temperature dependences of the index of refraction and the density of solutions, the θ-condition of polycaproamide solutions in DMAc containing 2.5% lithium chloride is estimated as 21.3°C. From intrinsic viscosity [η] measurements, the coefficients of swelling of a polymer coil, the mean-square distance between chain ends, and other parameters of macromolecules in solution are calculated. 相似文献
105.
A. P. Tyutnev R. Sh. Ikhsanov E. L. Grin’ G. P. Safonov A. I. Kononenko A. M. Sorokin I. V. Rudenko 《Polymer Science Series A》2006,48(11):1190-1195
A general theory of the phenomenon of recovered voltage in polymers was considered on the basis of representation of an actual poling process by a discrete set of Debye relaxators. Examples of numerical solution of the direct and inverse problems are given. A correlation expression between intentionally aged polymer specimens and recovered-voltage curves was proposed for use in the assessment of the material state of a polymer under actual service conditions. It was shown that it is sufficient to restrict consideration to three relaxation processes in analysis of the phenomenon. 相似文献
106.
N. F. Morozov Yu. K. Startsev Yu. V. Sud’enkov A. A. Suslikov G. A. Baranov A. A. Belyaev 《Technical Physics》2006,51(7):872-877
The radiation hardness and mechanical strength of single-and two-phase glasses are studied for the case when nanosecond laser pulses (λ= 1.06 μm, τ0.5 ≈ 12.5 ns) are focused inside the material. Laser interferometry is applied to measure the displacement of the free surface, find optical breakage thresholds, and carry out the fractographic analysis of damaged regions. It is shown that breakdown channels and damage regions develop in a nonlinear manner according to optical breakdown mechanisms, changing each other with an increase in the laser energy. The strength of the two-phase glass is found to be more than four times that of the single-phase glass, although their elastic properties differ insignificantly. Such a considerable difference in the hardness of these materials with chemically similar constitutents is attributed to the presence of the double-lattice nanometer-scale structure of the two-phase glass. 相似文献
107.
I. P. Dobrovol’skaya M. V. Mokeev Yu. N. Sazanov A. V. Gribanov T. E. Sukhanova 《Russian Journal of Applied Chemistry》2006,79(8):1312-1315
Variation of the supramolecular structure of heat-resistant polymide films in the course of high-temperature treatment was studied by X-ray diffraction analysis and NMR spectroscopy in solids. 相似文献
108.
Experimental data on the equilibrium and dynamics of chemisorption of vapors of organic substances on a silica gel modified with color reagents are presented. 相似文献
109.
Reactions of 5-substituted furan-2(3H)-ones with ethylenediamine, 2-aminoethanol, and o-aminophenol do not stop at the stage of formation of the corresponding 4-oxoalkanoic acid amides but lead to new bi-and tricyclic structures as a result of double intramolecular cyclodehydration. 相似文献
110.