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61.
Bajdik J. Pintye-Hódi K. Novák Cs. Kelemen A. Regdon G. Erős I. 《Journal of Thermal Analysis and Calorimetry》2002,68(2):613-627
The extents of the protective effects of coating films on the surface of crystals were determined. Three different samples
were made with different quantities of coating fluid (Sepifilm LP 010 in 10% aqueous solution). Since the atomizing rate was
constant, the coating time increased in parallel with the volume of coating fluid applied. The direct measurement of film
thickness and smoothness is very difficult, and therefore indirect methods were used. Dimenhydrinate was chosen as model drug;
this is a heat-sensitive antihistamine with a low melting point. This temperature can be reached during the tableting process.
The behaviour of samples on exposure to heat was examined by differential scanning calorimetry. The water uptakes of the samples
were determined with an Enslin apparatus. Plasticity was studied with an instrumented tablet machine. These indirect methods
(thermal conductivity, water uptake and plasticity measurements) revealed connections between the results of the various experiments.
An overlong coating time decreased the protective effect of the coating film.
This revised version was published online in August 2006 with corrections to the Cover Date. 相似文献
62.
Rossella Bartolo Anna Germinario Miguel Sánchez 《Annals of Global Analysis and Geometry》2002,21(1):63-84
In this paper the problem of the geodesic connectedness and convexity ofincomplete Riemannian manifolds is analyzed. To this aim, a detailedstudy of the notion of convexity for the associated Cauchy boundary iscarried out. In particular, under widely discussed hypotheses,we prove the convexity of open domains (whose boundaries may benondifferentiable) of a complete Riemannian manifold. Variationalmethods are mainly used. Examples and applications are provided,including a result for dynamical systems on the existence oftrajectories with fixed energy. 相似文献
63.
An experimental method for determining the real-time depth of laser-drilled holes is presented. The proposed method involves
detecting the laser-induced optoacoustic waves generated during the interaction of the laser beam with the material. Our optodynamic
study involved measuring the propagation times of these waves as they traveled through the material and analyzing their temporal
behavior during the drilling process. The experimental observations revealed an exponential relationship between the propagation
time of the longitudinal stress wave and the number of consecutive laser pulses.
Received: 25 October 2001 / Accepted: 27 October 2001 / Published online: 20 December 2001 相似文献
64.
Enrique Fernández-Cara Sergio Guerrero Oleg Yurievich Imanuvilov Jean-Pierre Puel 《Comptes Rendus Mathematique》2004,338(5):375-380
This Note deals with the controllability of Stokes and Navier–Stokes systems with distributed controls with support in possibly small subdomains. We first present a new global Carleman inequality for the solutions to Stokes-like systems that leads to the null controllability at any time T>0. Then, we present a local result concerning exact controllability to trajectories of the Navier–Stokes system. To cite this article: E. Fernández-Cara et al., C. R. Acad. Sci. Paris, Ser. I 338 (2004). 相似文献
65.
I. M. Kolthoff S. R. Cooper V. J. Tulane F. Reimers H. A. J. Pieters K. Höppner V. H. Matula C. B. Macek W. N. Skworzow J. S. Schepelewa F. Čuta K. Kámen S. Cohen R. E. Oesper D. S. Narayanamurthi T. R. Seshadri H. M. State A. W. Kirssanow W. M. Tscherkassow D. M. Mukherjee T. Akiyama Y. Mine S. Yabe Y. Volmar M. Déribéré 《Analytical and bioanalytical chemistry》1937,111(5-6):192-197
66.
Sauer, Shelah, Vapnik and Chervonenkis proved that if a set system on n vertices contains many sets, then the set system has full trace on a large set. Although the restriction on the size of the
groundset cannot be lifted, Frankl and Pach found a trace structure that is guaranteed to occur in uniform set systems even
if we do not bound the size of the groundset. In this note we shall give three sequences of structures such that every set
system consisting of sufficiently many sets contains at least one of these structures with many sets. 相似文献
67.
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69.
Neutron irradiation of Cp2MoCl2 for 24 h afforded the radiotracer Cp299MoCl2 which was characterised by UV–Vis spectroscopy and thin layer chromatography. Binding experiments with the thiol containing protein human serum albumin (HSA) or calf thymus DNA, were monitored for 99Mo using a gamma counter. Under the conditions investigated, molar ratios of binding of 0.2:1 (Cp2MoCl2:DNA) and 9.4:1 (Cp2MoCl2:HSA) were calculated. The results are consistent with in vitro coordination studies that have shown strong preferential interaction of Cp2MoCl2 with thiols versus other donor sites in biomolecules including DNA. 相似文献
70.
Howard Anton and Robert C. Busby, John Wiley & Sons, Inc., 2002. 相似文献