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191.
The synthesis of unsaturated unnatural amino acids according to the Heck-Jeffery protocol using a ball-milling procedure is presented. NOE data recorded on the products confirm that the Z-isomer is formed. This type of mechano-chemistry provides an efficient, “solvent free” and reliable method for the synthesis of substituted dehydroalanines. These conditions provide patterns of reactivity complementary to conventional procedures. 相似文献
192.
The physico-chemical properties and reactivity tested by hydrogen reduction have been studied for two series of NiO-ZnO mixed oxides of various composition. The solid nickel oxide or zinc oxide in interaction with the solution of nitrate of the second component were used as the precursors in each series. The differences in some physico-chemical parameters of the samples in both series were correlated with their reduction behaviour, followed both in iso- and non-isothermal regime. Moreower, the influence of various factors modifying the reactivity of mixed oxides was also investigated and the results were compared with those obtained from earlier studied analogous systems of quite different origin.This revised version was published online in November 2005 with corrections to the Cover Date. 相似文献
193.
A new preconditioned conjugate gradient (PCG)-based domain decomposition method is given for the solution of linear equations
arising in the finite element method applied to the elliptic Neumann problem. The novelty of the proposed method is in the
recommended preconditioner which is constructed by using cyclic matrix. The resulting preconditioned algorithms are well suited
to parallel computation. 相似文献
194.
C. Adamuscin A.-Z. Dubnicková S. Dubnicka R. Pekárik P. Weisenpacher 《The European Physical Journal C - Particles and Fields》2003,28(1):115-118
A system of linear homogeneous algebraic equations for the coupling constant ratios of vector mesons to hadrons is derived
by imposing the assumed asymptotic behavior upon the VMD pole parameterization of an hadron electromagnetic form factor. A
similar system of equations with a simpler structure of the coefficients, taken as even powers of the vector-meson masses,
is derived by means of integral superconvergent sum rules for the imaginary part of the considered form factor using its
appropriate -function approximation. Although both systems have been derived starting from different properties of the electromagnetic
form factor and they each have their own appearances, it is shown explicitly that they are fully equivalent.
Received: 20 March 2002 / Revised version: 3 December 2002 / Published online: 7 March 2003 相似文献
195.
We observe that a term of the WZW-type can be added to the Lagrangian of the Poisson σ-model in such a way that the algebra of the first class constraints remains closed. This leads to a natural generalization of the concept of Poisson geometry. The resulting “WZW–Poisson” manifold M is characterized by a bivector Π and by a closed three-form H such that 1/2[Π,Π]Schouten=H,ΠΠΠ. 相似文献
196.
We investigate the connection between the dynamics of
synchronization and the modularity on complex networks. Simulating
the Kuramoto's model in complex networks we determine patterns of
meta-stability and calculate the modularity of the partition these
patterns provide. The results indicate that the more stable the
patterns are, the larger tends to be the modularity of the partition
defined by them. This correlation works pretty well in homogeneous
networks (all nodes have similar connectivity) but fails when
networks contain hubs, mainly because the modularity is never
improved where isolated nodes appear, whereas in the synchronization
process the characteristic of hubs is to have a large stability when
forming its own community. 相似文献
197.
M. C. Caracoche J. A. Martínez P. C. Rivas M. A. Taylor A. F. Pasquevich S. Barolin O. A. de Sanctis 《Hyperfine Interactions》2007,179(1-3):87-93
The hyperfine quadrupole interaction at Hf sites in films and powders of 14 mol% CaO–HfO2 and 20 mol% CaO–HfO2 has been determined as a function of temperature. Results indicate the formation of a cubic solid solution and other microstructures assigned to the ?1 (CaHf4O9) and ?2 (Ca6Hf19O44) phases. Dynamical effects on the electric field gradient reveal the existence of oxygen vacancies movements in the solid solution. The thermal behavior of the relaxation constant observed in films allowed the determination of activation energies of 0.54 eV and 0.70 eV for the 14 mol% and 20 mol% CaO doped hafnias, respectively. The influence of the microdomains and the stability of the cubic solid solution are discussed. 相似文献
198.
199.
In this note we make a correction in the paper [1] by two of the authors. Specifically we modify an auxiliary localization
result and prove that the applications to the saturation theory of some outstanding conservative operators remain valid. Moreover,
we enrich a corollary dealing with the well-known Szász-Mirakjan operators.
This revised version was published online in June 2006 with corrections to the Cover Date. 相似文献
200.
Mátyás Bognár 《Acta Mathematica Hungarica》2004,102(1-2):37-84
The following generalization of the Hahn-Mazurkiewicz theorem is proved: Let (E,e) be a locally compact locally connected metric space. Let M be a continuum in this space and let d,e∈ M. Then there is a continuous mapping f: [0,1]→E such that f(0) = d, f(1)= e and M⊂f([0,1]). Also some corollaries of this theorem are proved. 相似文献