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排序方式: 共有270条查询结果,搜索用时 15 毫秒
71.
Evelyne Simon Catherine M Halliwell Chee Seng Toh Anthony E G Cass Philip N Bartlett 《Bioelectrochemistry (Amsterdam, Netherlands)》2002,55(1-2):13-15
Immobilisation of enzymes is important for applications such as biosensors or biofuel cells. A poly(histidine) tag had been introduced on the C terminus of a lactate dehydrogenase enzyme. This mutant enzyme was then immobilised onto poly(aniline) (PANi)-poly(anion) composite films, PANi-poly(vinylsulfonate) (PVS) or PANi-poly(acrylate) (PAA). The NADH produced by the immobilised enzyme in the presence of beta-nicotinamide adenine dinucleotide (NAD(+)) and lactate is oxidised at the poly(aniline)-coated electrode at 0.05 to 0.1 V vs. saturated calomel electrode (SCE) at 35 degrees C. 相似文献
72.
Two new indole alkaloids, angustilodine ( 1 ), with an unprecedented pentacyclic carbon skeleton, and angustilocine ( 2 ), belonging to the seco‐angustilobine‐B group of alkaloids, were obtained from the leaf extract of the Malayan species Alstonia angustiloba, and their structures were established by spectroscopic analysis. 相似文献
73.
A. Kimura Y. Toh M. Oshima Y. Hatsukawa J. Goto 《Journal of Radioanalytical and Nuclear Chemistry》2007,271(2):323-327
Recycled steel products demands a new technique for determining tramp elements in steel. In this paper, As and Sb in iron
certified reference materials were determined by neutron activation analysis with the multiple gamma-ray detection method.
The determined values are in good agreement with certified and reference values. The lower determination limits (LDL) for
As and Sb in high purity iron are 0.012 and 0.0025 ppm, respectively. As the demanded LDL for As and Sb is 0.1 ppm, the method
described in this work is suitable for determining As and Sb in recycled steel. 相似文献
74.
T. Hayakawa M. Oshima Y. Hatsukawa J. Katakura H. Iimura M. Matsuda N. Shinohara Y. Toh S. Mitarai T. Shizuma M. Sugawara H. Kusakari 《The European Physical Journal A - Hadrons and Nuclei》2000,9(2):153-156
The in-beam spectroscopy on N = 91 isotones has been carried out using the 12C + 150Nd reaction. The νi
13/2 and νh
11/2 bands of 153Sm have been extended up to 33/2+ and 31/2-, respectively. Two new γ-rays have been located on the top of the unfavored band with νi
13/2 configuration in 157Dy. Two identical relationships have been established in the low-spin region of the yrast νi
13/2 configuration between 153Sm and 155Gd, and between unfavored bands of 155Gd and 157Dy. Here all these nuclei have the same neutron number N = 91.
Received: 28 June 2000 / Accepted: 20 October 2000 相似文献
75.
Kim-Chuan Toh 《Computational Optimization and Applications》1999,14(3):309-330
Primal-dual path-following algorithms are considered for determinant maximization problem (maxdet-problem). These algorithms apply Newton's method to a primal-dual central path equation similar to that in semidefinite programming (SDP) to obtain a Newton system which is then symmetrized to avoid nonsymmetric search direction. Computational aspects of the algorithms are discussed, including Mehrotra-type predictor-corrector variants. Focusing on three different symmetrizations, which leads to what are known as the AHO, H..K..M and NT directions in SDP, numerical results for various classes of maxdet-problem are given. The computational results show that the proposed algorithms are efficient, robust and accurate. 相似文献
76.
A series of azopyridine-containing hydrogen bonding acceptors (4a-c) with flexible spacers of oligo(methylene) were synthesised. Hydrogen-bonded polymeric complexes 4/5 and trimeric complexes 4/62 , where 5 and 6 are aromatic dicarboxylic acids and monocarboxylic acids, respectively, were prepared and their liquid crystallinity was examined using differential scanning calorimetry and polarising optical microscopy. The study showed that most of the complexes displayed reversible thermotropic nematic phase. The isotropic to nematic phase transition temperatures of polymeric complexes 4/5 and trimeric complexes 4/62 in general decreased with the increase in length of spacers and terminal groups in the corresponding proton acceptors 4 and the proton donors 5 and 6, respectively. Hydrogen bonding interactions in complexes 4/5 and 4/62 were studied by X-ray photoelectron spectroscopy and Fourier transform infrared spectroscopy. 相似文献
77.
X. H. Zhou M. Oshima F. R. Xu Y. Toh Y. H. Zhang Y. Zheng Y. B. Xu M. Koizumi A. Osa T. Hayakawa Y. Hatsukawa T. Shizuma M. Sugawara 《The European Physical Journal A - Hadrons and Nuclei》2004,19(1):11-23
High-spin states in 169Re were studied and resulted in the identification of a strongly coupled band based on the 9/2-[514] Nilsson state and a decoupled band built on the h
9/2 1/2-[541] intruder proton orbit. The cranked-shell-model calculations present configuration-dependent deformations that can explain the different band crossing frequencies. The 9/2-[514] band in 169Re shows the largest signature splitting at low spin among the known odd-mass Re isotopes. After the alignment of a pair of i
13/2 neutrons, the phase of the splitting is inverted with a significantly reduced amplitude. For the 9/2-[514] bands in light odd-A Re isotopes, the signature splitting of the Routhians and its relation with the signature dependence of M1 transition matrix elements are investigated in connection with the deviation of nuclear shape from axial symmetry, suggesting an appreciable negative
deformation for the very neutron-deficient odd-A Re isotopes. Additionally, a three-quasipariticle band was observed and assigned to be built likely on the
configuration.Received: 9 May 2003, Published online: 18 December 2003PACS:
21.10.Re Collective levels - 23.20.-g Electromagnetic transitions - 23.20.Lv
transitions and level energies - 27.70. + q
相似文献
78.
T. Shizuma Z. G. Gan K. Ogawa H. Nakada M. Oshima Y. Toh T. Hayakawa Y. Hatsukawa M. Sugawara Y. Utsuno Z. Liu 《The European Physical Journal A - Hadrons and Nuclei》2004,20(2):207-210
Excited states in 136Ba, populated in deep inelastic collisions by the interaction of 450 MeV 82Se ions with a 139La target, have been studied by means of in-beam
-ray spectroscopy. A new isomer with
has been identified at an excitation energy Ex = 3.357 MeV. The half-life was determined as
ns. The extracted B(E2) value is much smaller than those in 132Te and 134Xe. This hindrance is investigated by a shell model calculation.Received: 22 September 2003, Revised: 11 November 2003, Published online: 6 April 2004PACS:
21.10.Tg Lifetimes - 23.20.Lv
transitions and level energies - 27.60. + j
相似文献
79.
80.
MA Long ZHOU Xiao-Hong M.Oshima Y.Toh ZHANG Yu-Hu GUO Ying-Xiang LEI Xiang-Guo M.Koizumi A.Osa T.Hayakawa Y.Hatsukawa T.Shizuma M.Sugawara 《中国物理C(英文版)》2008,32(1)
The level structure of 190Pt has been studied experimentally using the 176Yb (18O, 4n) reaction at beam energies of 88 and 95 MeV. γ-γ-t coincidence measurements were carried out. Based onthe analysis of γ-γ coincidence relationships, the level scheme of 190Pt is extended to high-spin states. A new structure built on the 3413.6 keV 14+ state has been observed, and the vi1-213/2 vh-19/2 vj (j = p3/2 or f5/2) configuration is tentatively assigned to it. 相似文献