全文获取类型
收费全文 | 1509篇 |
免费 | 17篇 |
国内免费 | 5篇 |
专业分类
化学 | 853篇 |
晶体学 | 63篇 |
力学 | 31篇 |
数学 | 100篇 |
物理学 | 484篇 |
出版年
2022年 | 23篇 |
2021年 | 26篇 |
2020年 | 19篇 |
2019年 | 23篇 |
2018年 | 20篇 |
2017年 | 22篇 |
2016年 | 35篇 |
2015年 | 24篇 |
2014年 | 39篇 |
2013年 | 115篇 |
2012年 | 73篇 |
2011年 | 86篇 |
2010年 | 44篇 |
2009年 | 46篇 |
2008年 | 52篇 |
2007年 | 55篇 |
2006年 | 66篇 |
2005年 | 45篇 |
2004年 | 46篇 |
2003年 | 28篇 |
2002年 | 40篇 |
2001年 | 24篇 |
2000年 | 20篇 |
1999年 | 14篇 |
1998年 | 13篇 |
1997年 | 13篇 |
1996年 | 10篇 |
1995年 | 15篇 |
1994年 | 18篇 |
1993年 | 18篇 |
1992年 | 28篇 |
1991年 | 18篇 |
1990年 | 21篇 |
1989年 | 19篇 |
1988年 | 17篇 |
1987年 | 13篇 |
1986年 | 19篇 |
1985年 | 25篇 |
1984年 | 22篇 |
1983年 | 25篇 |
1982年 | 18篇 |
1981年 | 19篇 |
1980年 | 29篇 |
1979年 | 25篇 |
1978年 | 20篇 |
1977年 | 19篇 |
1976年 | 11篇 |
1975年 | 15篇 |
1973年 | 12篇 |
1971年 | 9篇 |
排序方式: 共有1531条查询结果,搜索用时 0 毫秒
81.
Acharya Balkrishna Pradeep Nain Monali Joshi Lakshmipathi Khandrika Anurag Varshney 《Molecules (Basel, Switzerland)》2021,26(4)
Putrajeevak (Putranjiva roxburghii Wall.; synonym Drypetes roxburghii (Wall.) Hurus) seeds have been used since ancient times in the treatment of infertility in the Ayurvedic system of medicine in India. In this study, the oil component of Putrajeevak seeds (PJSO) was extracted using the supercritical fluid extraction (SCFE) method using liquid CO2 and the constituents were analyzed using gas chromatography-flame ionized detectorand high-performance thin-layer chromatography. PJSO contained trace amounts of β-sitosterol with oleic and linoleic acids as the major fatty acid constituents. Male and female zebrafish were mutagenized with N-ethyl-N-nitrosourea (ENU) and fish that produced less than 20 viable embryos were selected for the study. SCFE oil extracts from the P. roxburghii seeds were used in this study to reverse fertility impairment. The mutant fish were fed with PJSO for a period of 14 days and the rates of fertility, conception, and fecundity were determined with wild-type healthy fish as a breeding partner. Treatment with PJSO increased the ovarian follicle count as well as the number of mature eggs, while reducing the number of ovarian cysts. Sperm count as well as sperm motility were greatly enhanced in the ENU-mutagenized male zebrafish when treated with PJSO. The results obtained in this study demonstrate the effectiveness of P. roxburghii seed oil in reversing impaired fertility in both male and female zebrafish models. 相似文献
82.
Desai Nisheeth C. Vaja Darshita V. Joshi Surbhi B. Khedkar Vijay M. 《Research on Chemical Intermediates》2021,47(2):573-587
Research on Chemical Intermediates - We have developed a simple synthetic protocol for the preparation of novel 3-(3-(4-fluorophenyl)-1-phenyl-1H-pyrazol-4-yl)-5-arylisoxazoles. The structure of... 相似文献
83.
Novel one-pot synthesis of 4H-chromene derivatives using amino functionalized silica gel catalyst 总被引:2,自引:2,他引:0
Vijaykumar M.Joshi Rupali L.Magar Prashant B.Throat Sunil U.Tekale Bhagavan R.Patil Mangal P.Kale Rajendra P.Pawar 《中国化学快报》2014,25(3):455-458
A simple, efficient, and environmentally benign method for the synthesis of 4H-chromene derivatives was developed using well ordered and recoverable amino functionalized silica gel as a base catalyst. The 4H-chromene derivatives were obtained in short time and excellent yield(87%–96%) by three component reaction of aldehydes, malononitrile and cyclic 1,3-diketones in water at 70 8C. 相似文献
84.
Mohan N. Patel Chintan R. Patel Hardik N. Joshi Pankaj A. Vekariya 《Applied biochemistry and biotechnology》2014,172(4):1846-1858
The platinum(II) complexes with N,S-donor ligand have been synthesised and characterised by physiological techniques like elemental, electronic, Fourier transform infrared, hydrogen-1 nuclear magnetic resonance (1H NMR) and liquid chromatography–mass spectrometry spectra. The synthesised complexes have been checked for their DNA binding ability by absorption titration and viscosity measurement, and the results show that the complexes binds to herring sperm DNA (HS DNA) via covalent mode of binding. The DNA cleavage activity of synthesised complexes has been carried out by gel electrophoresis experiment using supercoiled form of pUC19 DNA, showing the unwinding of the negatively charged supercoiled DNA. Brine shrimp (Artemia cysts) lethality bioassay technique has been applied for the determination of toxic property of synthesised complexes in terms of micromolars. 相似文献
85.
Augustine Elizabeth Desigan N. Pandey N. K. Joshi J. B. 《Journal of Radioanalytical and Nuclear Chemistry》2020,324(1):211-218
Journal of Radioanalytical and Nuclear Chemistry - In the present study, the dissolution kinetics of UO2 pellets in nitric acid has been investigated. Kinetic rate expressions based on... 相似文献
86.
87.
Nonlinear Dynamics - Based on a non-classical plate theory, a nonlinear analytical model is proposed to analyze transverse vibration of thin partially cracked and submerged orthotropic plate in the... 相似文献
88.
Procedure for hydrothermal synthesis of ZSM-8-type zeolite crystals, using TEA—OH as a template, in the system having molar composition 16.2 (Na2O) — Al2O3 — 117 (SiO2) — 4.8 (TEA)2O — 3887 H2O at 170 °C is described. Results of characterization of these crystals by XRD, IR, EDAX, SEM, TGA, and adsorption studies are described and discussed. X-ray diffraction studies establish that the crystals are ZSM-8-type with structure similar to that of ZSM-5-type crystals. Crystals have prismatic bipyramidal morphology with average size 18–25 microns. Degased calcined samples adsorb xylenes in the order p > m > 0. Pore length per unit cell, estimated from n-hexane adsorption studies, is 46 Å. 相似文献
89.
Results of microtopographical investigations on prism faces of cultured quartz crystals grown by hydrothermal crystallization techniques, undertaken with a view to determine the influence of microcrystals which get attached to the growing host prism face and then get detached, at some stage of growth, from or still remain attached to the host face, with special reference to the role played by them in the growth and development of host prism faces in particular and the quartz crystals in general, are discussed. The study is an extension of, and obviously to be dealt in continuation with, the earlier one (Part-I, see JOSHI , KOTRU ). Polygonal cavities of various shapes and structures observed on the prism faces are described. Mechanism of formation of the polygonal cavities is explained. Also described are pyramidal depressions, striations, growth hillocks, and etch pits within the cavities on the growing host prism faces. Some of the observed structures within the cavities are attributed to the imprints of the surface structures on the faces of detached microcrystals of quartz. Evidence of growth within the cavities is offered and the implications of such a growth are discussed. Evidence of micro-etching in the cavities is suggestive of the possibilities of some of the grown cultured quartz crystals to get etched in the autoclave. Two different suggestions are made for the interpretation of the origin of etch pits within the cavities, and there is support for the view that they are as a result of etching, only at a time when the supply quartz gets exhausted, of some of the grown crystals where the growing chamber is the hottest. 相似文献
90.
Bintinger D Kees KH Masek GE Miller ES Thompson JR Vernon W White JT Eisner AM Palmer DA Sullivan MK Armitage JC Buijs A Van Driel MA Erné FC Langeveld WG Paar HP Sens JC Timmer J Van Uitert B Cain MP Ko W Lander RL Maeshima K McNeil RR Pellett DE Smith JR Williams MC Caldwell DO Joshi UP Lu A Schwitkis KA Yellin SJ 《Physical review letters》1985,54(8):763-766