Experimental analysis of metal coated dielectric waveguides

This paper concerns the experimental characteristics of metal coated dielectric waveguides with a rectangular surface corrugation. Waveguide are designed to operate at a second Bragg frequency of 90 GHz. The period, height and the duty cycle of a rectangular grating were calculated using the chosen frequency. A metallic layer of aluminum is sputtered on one side of the slab waveguide. The purpose of the metallic layer is to simulate a layer of high density plasma on the surface of the waveguide similar to that obtained by optical excitation of semiconductor structures. Experiments were performed to examine the far field radiation pattern, attenuation constant and the dispersion relation. Due to the presence of the plasma layer there will be an angular shift in the far field radiation pattern. We have observed angular shifts of about 20 in the radiation pattern of the waveguide before and after coating. Measurements are made in the frequency range of 88–95 GHz. This waveguide structure can be used to design an electronically steerable antenna and an electronic phase shifter operating in the millimeter-wave frequency band.Supported in part by the Army Research Office.     

液态铅的电阻率

采用精确的结构因数实验数据和Ｂｅｈａｖｉ模型赝势，用Ｚｉｍａｎ理论计算了液态铅的电阻率．计算结果和实验数据符合很好．讨论了Ｚｉｍａｎ理论对液态铅的适用性以及适合于液态铅的赝势的特征．     

Pt-Pd /y-A120.催化剂氧化性能的研究‘

本文采用浸演法制备了一系列Pt-Pd/Y-AlzO,催化剂，并考察其对正己烷，正丁醉和苯的催化氧化性能.结果表明，Pt-Pd双组分催化剂对极性有机物正丁醉有很高的氧化活性，而对于非极性有机物苯和正己烷的氧化活性相对较差.对Y-AlzOa载体进行高温预处理后，催化剂对苯和正己烷的氧化活性有明显提高.     

麻黄生物碱中一对光学异构体在薄层色谱原位的表面增强拉曼光谱研究

应用表面增强技术(SERS)将薄层色谱(TLC)与傅里叶变换拉曼光谱(FT-Raman)联用,在薄层色谱分离斑点原位,获得中草药麻黄中麻黄生物碱衍生物中一对关于手性碳的光学异构体：去甲基麻黄碱,去甲基伪麻黄碱指纹光谱的新方法。研究表明,在薄层色谱原位仅16 μg的样品,就可获得以上分子的主要特征谱带;并且光学异构体的光谱特征明显不同,在银溶胶微粒表面增强作用下去甲基麻黄碱、去甲基伪麻黄碱分子中与苯环相关的波数为1 004,1 605 cm-1振动获最大增强。从而阐明了应用TLC-SERS联用技术,可有效地对中草药主要化学成分中光学异构体进行高灵敏度分离与指纹鉴定。