InGaP光学微盘的显微荧光图像观测及分析

利用一套ＣＣＤ显微荧光图像观测和采集分析系统,分别在室 液氮温度下对半径为５μｍ发射波长０．６５μｍ的ＩｎＧａＰ半导体光学微盘的光图像进行了观测。     

Inverse optimization for linearly constrained convex separable programming problems

In this paper, we study inverse optimization for linearly constrained convex separable programming problems that have wide applications in industrial and managerial areas. For a given feasible point of a convex separable program, the inverse optimization is to determine whether the feasible point can be made optimal by adjusting the parameter values in the problem, and when the answer is positive, find the parameter values that have the smallest adjustments. A sufficient and necessary condition is given for a feasible point to be able to become optimal by adjusting parameter values. Inverse optimization formulations are presented with ℓ₁ and ℓ₂ norms. These inverse optimization problems are either linear programming when ℓ₁ norm is used in the formulation, or convex quadratic separable programming when ℓ₂ norm is used.     

纳米粒子在方管中传输与沉降的研究

采用有限体积法离散并应用Simple方法对方截面弯曲管道内的纳米粒子传输和沉降进行了数值计算,结果表明Reynolds数和Schmidt数是影响纳米粒子传输和沉降的重要参数。粒子较小时,弯管中轴向速度较大的区域就是粒子的高浓度区域,沉降增强因子最大值出现在外弯侧的中心位置;粒子较大时,截面浓度的梯度值降低,沉降增强因子趋于平均,此时整个截面的粒子平均沉降。弯曲作用对于粒子较大且Dean数也较大时的影响更加明显。     

High-throughput approaches for the discovery and optimization of new olefin polymerization catalysts

The discovery of new olefin polymerization catalysts is currently a time-intensive trial-and-error process with no guarantee of success. A fully integrated high-throughput screening workflow for the discovery of new catalysts for polyolefin production has been implemented at Symyx Technologies. The workflow includes the design of the metal-ligand libraries using custom-made computer software, automated delivery of metal precursors and ligands into the reactors using a liquid-handling robot, and a rapid primary screen that serves to assess the potential of each metalligand-activator combination as an olefin polymerization catalyst. "Hits" from the primary screen are subjected to secondary screens using a 48-cell parallel polymerization reactor. Individual polymerization reactions are monitored in real time under conditions that provide meaningful information about the performance capabilities of each catalyst. Rapid polymer characterization techniques support the primary and secondary screens. We have discovered many new and interesting catalyst classes using this technology.     

HgBa2CuO2正常态1/f噪声行为的研究

我们在１００－３００Ｋ温度范围测量了ＨａＢａ２ＣｕＯ２（Ｈｇ－１２１２）相块材样品和不同质量的Ｈｇ－１２１２相薄膜样品,发现Ｈｇ－１２１２相膜的噪声温行为显示较强的样品个性。     

以二乙氨基乙基交联葡聚糖凝胶为基质的铝荧光传感层

本文基于Ａｌ＾３＋离子对电价键固定在二乙氨基乙基交联葡聚糖凝胶上的水杨基荧光 酮的可逆荧光淬灭作用，研制了测定Ａｌ＾３＋离子浓度的荧光传感层。     

结晶猪、牛B1色氨酸胰岛素的制备及性质

猪、牛胰岛素经与MSC·ONSu选择性反应.随后Edman降解,和与MSC·Trp·ONp缩合,去保护制备了二个种属的[Trp]^B₁胰岛素类似物. 经醋酸纤维素电泳.氨基酸组成分析,UV吸收光谱和N-端分析鉴定,确定它们是均一的[Trp]^B₁胰岛素.鼠惊厥分析显示猪、牛[Trp]^B₁胰岛素的生物活力分别为18国际单位/毫克和17国际单位/毫克.分别相当于天然胰岛素的70％.     

Preparation of GaN-based cross-sectional TEM specimens by laser lift-off

Laser lift-off (LLO) technology is successfully used to prepare GaN-based TEM cross-sectional specimens. Detailed procedures of the method to prepare the specimens are demonstrated. Large thin areas suitable for TEM analysis were obtained. TEM images of the resulting GaN interface are studied, and the changes in structural quality are confined to approximately the first 250 nm of the epilayer. Clear TEM images of the whole epilayer and the InGaN quantum wells and the HRTEM images of the superlattice layer are demonstrated, showing that LLO is a quick and ideal method to study the crystal structure of the epilayer, especially if only the upper layers are of interest.     

Influence of indenter tip geometry on elastic deformation during nanoindentation

Nanoindentation with a Berkovich indenter is commonly used to investigate the mechanical behavior of small volumes of materials. To date, most investigators have made the simplifying assumption that the tip is spherical. In reality, indenter tips are much more complex. Here, we develop a new method to describe the tip shape using the experimentally determined area function of the indenter at small depths (0-100 nm). Our analysis accurately predicts the elastic load-displacement curve and allows the theoretical strength of a material to be determined from pop-in data. Application of our new method to single crystal Cr3Si shows that the predicted theoretical strengths are within 12% of the ideal strength G/2pi, where G is the shear modulus.