全文获取类型
收费全文 | 20644篇 |
免费 | 3546篇 |
国内免费 | 2297篇 |
专业分类
化学 | 14748篇 |
晶体学 | 261篇 |
力学 | 1259篇 |
综合类 | 187篇 |
数学 | 2065篇 |
物理学 | 7967篇 |
出版年
2024年 | 75篇 |
2023年 | 469篇 |
2022年 | 673篇 |
2021年 | 735篇 |
2020年 | 824篇 |
2019年 | 794篇 |
2018年 | 668篇 |
2017年 | 628篇 |
2016年 | 977篇 |
2015年 | 984篇 |
2014年 | 1114篇 |
2013年 | 1447篇 |
2012年 | 1868篇 |
2011年 | 1897篇 |
2010年 | 1252篇 |
2009年 | 1112篇 |
2008年 | 1302篇 |
2007年 | 1284篇 |
2006年 | 1134篇 |
2005年 | 1010篇 |
2004年 | 721篇 |
2003年 | 632篇 |
2002年 | 569篇 |
2001年 | 432篇 |
2000年 | 416篇 |
1999年 | 472篇 |
1998年 | 358篇 |
1997年 | 373篇 |
1996年 | 314篇 |
1995年 | 301篇 |
1994年 | 305篇 |
1993年 | 251篇 |
1992年 | 198篇 |
1991年 | 198篇 |
1990年 | 177篇 |
1989年 | 112篇 |
1988年 | 86篇 |
1987年 | 89篇 |
1986年 | 60篇 |
1985年 | 45篇 |
1984年 | 43篇 |
1983年 | 24篇 |
1982年 | 25篇 |
1981年 | 18篇 |
1980年 | 14篇 |
1975年 | 2篇 |
1957年 | 4篇 |
1936年 | 1篇 |
排序方式: 共有10000条查询结果,搜索用时 0 毫秒
71.
单扫描示波极谱测定痕量银 总被引:1,自引:0,他引:1
本文首次提出了运用单扫描极谱直接测定银的方法。在含N-烯丙基-N′-对苯磺酸钠硫脲及四乙烯五胺的硼砂缓冲液中,银离子在-0.66V(相对饱和甘汞电极)有一灵敏还原波。运用经典极谱或单扫描极谱,此波均可用于微量银的定量测定。“银波”的单扫描示波极谱波可在5×10~(-7)~3×10~(-5)mol/L范围内检测银。方法已用于废定影液中银含量的分析,结果满意。 相似文献
72.
73.
PARAMETER ESTIMATION OF SPATIAL AR MODEL 总被引:1,自引:0,他引:1
Jiang Jiming 《数学年刊B辑(英文版)》1991,12(4):432-444
Consider a stable AR model of two parameter spatial series {X_t, t∈N~2}, i. e. {X_(t)t∈N~2} is homogeneous and satisfies the following difference equationX_t-sum from n=s∈相似文献
74.
After taking into account energy conservation and the particle’s self-gravitation interaction, Hawking radiation of the massive
particle as tunneling from Schwarzshild-anti-de Sitter black hole is studied by using Parikh-Wilczek’s semi-classical quantum
tunneling approach. Meanwhile, Hawking radiation as tunneling from the black hole is reexamined by developing Angheben–Nadalini–Vanzo–Zerbini
(ANVZ) covariant method to cover energy conservation and the particle’s self-gravitation interaction. Both the results perfectly
generalize those obtained by Parikh and Wilczek, and show that the tunneling rate is related to the change of Bekenstein-Hawking
entropy, and the factual emission spectrum is not exactly thermal, but satisfies the underlying unitary theory.
PACS: 04.70-s, 9760. Lf. 相似文献
75.
The purpose of the present note is to establish some new delay integral inequalities, which provide explicit bounds on unknown functions and generalize some results of Li et al. [Some new delay integral inequalities and their applications, J. Comput. Appl. Math. 180 (2005) 191–200]. The inequalities given here can be used to investigate the qualitative properties of certain delay differential equations and delay integral equations. 相似文献
76.
77.
采用溶胶-凝胶工艺与原位生长技术,制备了ZnSe/SiO2复合薄膜.X射线衍射分 析表明薄膜中ZnSe晶体呈立方闪锌矿结构.X射线荧光分析结果显示薄膜中Zn与Se摩尔比为1 ∶1.01—1∶1.19.利用场发射扫描电子显微镜观察了复合薄膜的表面形貌,结果表明复合薄 膜表面既存在尺寸约为400nm的ZnSe晶粒,也存在尺寸小于100nm的ZnSe晶粒.利用椭偏仪测 量了薄膜椭偏角Ψ,Δ与波长λ的关系,采用Maxwell-Garnett有效介质理论对薄膜的光学 常数、厚度、气孔率、ZnS
关键词:
2复合薄膜')" href="#">ZnSe/SiO2复合薄膜
光学性质
椭偏光度法
荧光光谱 相似文献
78.
Nanocrystalline FeS2 cathode material of lithium cell was synthesized from cheap materials of FeSO4, Na2S2O3, and sulfur by a hydrothermal process. The scanning electron microscopy analysis showed the obtained material was nano-sized,
about 500 nm. The X-ray powder diffraction analysis showed that the synthetic FeS2 material had two phases of the crystalline structure, pyrite and marcasite. The phase of marcasite seems to have no negative
effect on the electrochemical performance of the material. The synthetic FeS2 showed a significant improvement of electrochemical performance for Li/FeS2 cells. 相似文献
79.
Yangyang Jiang Chen Guo Huizhou Liu 《中国颗粒学报》2007,5(1):130-133
A magnetically rotational reactor (MRR) has been developed and used in absorbing benzene emissions. The MRR has a permanent magnet core and uses magnetic ionic liquid [bmim]FeCl4 as absorbent. Benzene emissions were carried by N2 into the MRR and were absorbed by the magnetic ionic liquid. The rotation of the permanent magnet core provided impetus for the agitation of the magnetic ionic liquid, enhancing mass transfer and making benzene better dispersed in the absorbent. 0.68 g benzene emissions could be absorbed by a gram of [bmim]FeCl4, 0.27 and 0.40 g/g higher than that by [bmim]PF6 and [bmim]BF4, respectively. The absorption rate increased with increasing rotation rate of the permanent magnet. 相似文献
80.
Fe-doped TiO2 powder was prepared by high-energy ball milling, using TiO2 Degussa P-25 and α-Fe powders as the starting materials. The structure and magnetic properties of the Fe-doped TiO2 powder were studied by X-ray diffraction, 57Fe Mossbauer spectroscopy and vibrating sample magnetometer. The Reitveld refinement of XRD revealed that ball milling not only triggered incorporation of Fe in TiO2 lattice but also induced the phase transformation from anatase to rutile in TiO2 and consequently the milled Fe-doped TiO2 powder contained only rutile.57Fe Mössbauer effect measure showed that Fe atoms existed in Fe2+ and Fe3+ state, which were assigned to the solid solution FexTi1−xO2. The magnetization measurements indicated that the milled Fe-doped TiO2 powder was ferromagnetic above room temperature. The ferromagnetism in our milled Fe-doped TiO2 powder seemingly does not come from Fe and iron oxides particles/clusters but from the Fe-doped TiO2 powder matrices. 相似文献