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81.
An effective and environmentally benign benzylic oxidation for transition of alkylarenes into the corresponding carbonyl compounds was reported.Alkylarenes were mixed and stirred with potassium bromide,m-chloroperbenzoic acid and a catalytic amount of iodobenzene in water at 60 8C for several hours,a series of the corresponding carbonyl compounds was obtained in moderate to good yields.In the reaction,iodobenzene was first oxidized by m-chloroperbenzoic acid into the hypervalent iodine intermediate which then reacted with potassium bromide to form the key radical initiator for the benzylic oxidation. 相似文献
82.
83.
Wang Chang-biao Tu Jian-nan Jian Hua-bei Sun Yan 《International Journal of Infrared and Millimeter Waves》1986,7(7):1005-1035
The kinetic theory based on the expansion of local field in the guiding center coordinate system, presented by paper[1]–[3], has successfully developed into a theoretical system. The mathematical background and physical explanation of setting up the guiding center coordinate system is expounded in the paper. By using the methods of the guiding center and waveguide coordinate systems respectively, the same dispersion equations for interaction of an axially symmetrical single momentum electron beam with TEmn field in the circular waveguide are rigorously derived. A number of mistakes in paper[4] are indicated as well. 相似文献
84.
Summary In the present paper, a diffraction integral formula for a misaligned optical system is derived. The interference effects
of opticalelement arrays are studied by means of such a formula. The possibility of eliminating interference fringes is discussed.
The conclusion is that the interference fringes could be eliminated when the αβγδ condition for arrays is satisfied. The synthetical
aberration is simultaneously eliminated. However, in this case, the synthetical image coincides with the individual images.
For some special application, the synthetical image does not coincide with the individual images and the αβγδ condition is
not fulfilled. But the interference fringes may disappear in some special cases.
Riassunto La formula di Collins, che esprime il cammino ottico fra un punto del piano oggetto e un punto del piano immagine nel caso di un sistema ottico centrato, è generalizzata al caso di un sistema ottico disallineato. La formula cosí ottenuta è applicata allo studio del fenomeno d’interferenza che ha luogo nel piano della cosiddetta ?immagine sintetica? fra i vari fasci emergenti da una cortina di elementi ottici. Si discutono infine le condizioni in cui non si hanno frange d’interferenza sull’immagine sintetica.相似文献
85.
86.
87.
Zero field Mössbauer spectra and powder susceptibility measurements show that the condensed, hydrogen bonded network compound FeSO3 3H2O orders antiferromagnetically (TNéel 9.5 K). The related anhydrous material FeSO3 also shows antiferromagnetic exchange but no evidence of long range three-dimenstional magnetic order to as low as 1.4 K.Supported by the U.S. National Science Foundation Division of Materials Research—Solid State Chemistry Program Grant No. DMR 8313710. 相似文献
88.
HL-1装置在环向磁场2.3T下运行,获得135kA平衡稳定等离子体,平顶时间160ms。实验表明,环向磁场杂散分量约为纵场的万分之一,导体壳和平衡场基本上能保证等离子体的平衡。观察到的电子温度约500eV,平均电子密度2.8×10~(13)cm~(-3),能量约束时间10ms,有效电荷数小于3,最低稳定运行安全因子2.5,最长放电持续时间1040ms。在对MHD稳定性进行观察的基础上,确定了稳定运行区域;极限密度服从Murakami定标律。 相似文献
89.
We illustrate that the recursion method is useful in the study of the electronic structure of metallic superlattices.It reduces considerably the amount of computational works,and gives,nevertheless,fairly satisfactory densities of states. 相似文献
90.
使用光发射谱(OES)对甚高频等离子增强化学气相沉积(VHF-PECVD)技术沉积硅薄膜时的等离子体发光基团的空间分布进行了在线监测和研究. 研究表明:等离子体的不同发光基团都存在着一个中间强度较大的区域和两边电极附近的暗区;增大硅烷浓度和提高辉光功率都会增大SiH*峰强度;硼烷的加入,使得SiH*和Hα*峰强度增大,但硼烷流量变化的影响很小;硼烷流量增大,材料的晶化率下降,而I[Hα*]关键词:
甚高频等离子增强化学气相沉积
等离子体
发光基团
空间分布 相似文献