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991.
H Akiyama H Toyoda S Yamanashi Y Sagehashi T Toida T Imanari 《Biomedical chromatography : BMC》1991,5(5):189-192
A high performance liquid chromatographic (HPLC) system is described for determination of the unsaturated disaccharide (delta Di-HA) derived from hyaluronic acid (HA) in human urine by digestion with hyaluronidase SD. The effects of eluents on the separation of delta Di-HA and delta Di-0S, which is derived from the reaction of chondroitin with the enzyme, have been studied. The established chromatographic conditions were as follows--column: a stainless steel tube (4 mm i.d. x 250 mm) packed with TSKgel NH2-60; eluent: a mixture of acetonitrile and 0.1 M Tris-HCl buffer containing 0.1 M boric acid and 10 mM sodium sulphate, pH 7.0 (64:36, v/v). The strong fluorescence of unsaturated disaccharide after the reaction with 2-cyanoacetamide in alkaline medium was used for post-column detection. The calibration curve for delta Di-HA was linear in the range 5 pmol-5nmol with a practical detection limit of 2 pmol. The assay coefficients of variation (n = 5) at 200 pmol for delta Di-HA and delta Di-0S were 1.7 and 1.5%, respectively. This HPLC system has been applied to the determination of HA in human urine. 相似文献
992.
A commercial baker’s yeast was subjected to selection in a continuous turbidostat cultivation with increasing concentration of acetic acid. The final acetic acid content in fresh medium was 0.6% or 0.8% v/v. Two of seven selected variants were stable over 15 sequential shake flask cultivations without selection pressure. After laboratory scale production of baker’s yeast, one of the variants also showed increased acetic acid tolerance in sour dough. The overall raising power (mL CO2/h) in sour dough was improved 36%. 相似文献
993.
B. M. Forster J. M. Bailey G. A. Beer J. L. Beveridge J. H. Brewer W. N. Hardy T. M. Huber K. R. Kendall A. R. Kunselman J. A. Macdonald G. M. Marshall G. R. Mason A. Olin M. Senba J. B. Warren 《Hyperfine Interactions》1991,65(1-4):1007-1013
Muonic hydrogen isotopes (μ− p, μ− d, and μ−t) are simple quantum mechanical systems ideally suited for studies of numerous fundamental phenomena in electroweak and strong
interactions as well as in applied areas such as muon chemistry or muon catalyzed fusion.
Emission of muonic hydrogen isotopes into vacuum helps to overcome the limitations which are normally imposed on conventional
investigations with gaseous and liquid targets. A proof of principle experiment for this new technique was performed at TRIUMF
last year. Negative muons with 30 MeV/c momentum were stopped in a thin film of solid hydrogen and produced very low energy μ−d in vacuum. The distribution center of the normal velocity components of emitted μ−d atoms was measured to be ∼1 cm/μs. The yield of μ−d in vacuum is an increasing function of H2 film thickness δ up to a value of δ≥1 mm. 相似文献
994.
R. Kadono R. F. Kiefl J. H. Brewer G. M. Luke T. Pfiz T. M. Riseman B. J. Sternlieb 《Hyperfine Interactions》1991,64(1-4):635-640
The diffusion rate of muonium in the III–V compound semiconductor GaAs has been determined from measurements of muon spinT
1 relaxation induced by motion in the presence of nuclear hyperfine interactions. It is shown for the first time in a semiconductor
that (a) there is a crossover of the transport mechanism at about 90 K from stochastic to zero-phonon hopping, as evidenced
by a steep rise in the hop rate at lower temperatures, and that (b) the muonium diffuses at the hop rate of 1010 s−1 (corresponding diffusion constantD≈10−6 cm2s−1) at lower temperatures as well as at room temperature. 相似文献
995.
996.
997.
R. Klein R. Grieser L. Hoog G. Huber I. Klaft P. Merz T. Kühl S. Schröder M. Grieser D. Habs W. Petrich D. Schwalm 《Zeitschrift für Physik A Hadrons and Nuclei》1992,342(4):455-461
We have performed for the first time precision spectroscopy on a coasting fast7Li+ ion beam in a storage ring. The ion beam moving with 6.4% speed of light was first electron cooled and then merged with two counterpropagating laser beams acting on two different hyperfine transitions sharing a common upper level (λ-system). One laser was frequency locked to thea 3 127J2 hfs frequency component established as a secondary frequency standard at 514 nm. The second laser was tuned over theλ-resonance, which was recorded relative to127J2 hfs components. This experiment is sensitive to the time dilation in fast moving frames and will lead to new limits for the verification of special relatively. The present status of the experiment and perspectives in accuracy are discussed. 相似文献
998.
999.
The edge structure and stability of monolayer-high islands fabricated on Si(001) surfaces by scanning tunneling microscopy have been analyzed theoretically. In contrast to the edges of similar islands grown by depositing Si, the properties of edges of fabricated islands are determined by the length of the trench of dimers that are removed to create the island. We demonstrate the possibility of controlling the edge structure, and thus the stability, through a selective process of atom removal. 相似文献
1000.
M. Kopcewicz J. Jagielski A. Grabias F. Stobiecki T. Stobiecki 《Hyperfine Interactions》1998,112(1-4):25-28
The Ar-ion-beam mixing of Fe/Zr bi- and multilayers is studied by conversion electron Mössbauer spectroscopy as a function of ion dose ranging from 1×1014 to 1×1017 at./cm2. The mixing leads to amorphization of the Fe/Zr system. It was shown that the mixing process in bilayers depends strongly on the thickness of the Zr substrate. The amorphization is much more effective and occurs at lower ion doses in multilayers as compared to corresponding bilayers. 相似文献