丙酮在XeCl准分子激光辐射下的多光子电离和碎裂研究

我们用扩散分子束多光子电离光谱技术研究了丙酮在XeCl准分子激光辐射下的多光子电离和碎裂行为。实验表明丙酮没有产生母体离子峰(m/e=58), 只给出m/e=43和15两个峰, 分别对应于丙酮光解所产生的两个碎片CH_3 CO和CH_3。其离子信号(1)分别与激光强度(Ⅰ)的3和3.6次方成正比。分析表明离子是由中性碎片电离产生的。     

胆汁酸的薄层层析——数理统计法用于层析溶剂系统的选择

本文选择氯仿、乙醇、乙酸乙酯、醋酸和水等五种溶剂作为胆汁酸薄层层析的展开剂,采用正交设计法[L_(16)(4~5)]安排实验,对胆固醇、胆酸、脱氧胆酸、甘氨胆酸、甘氨脱氧胆酸、牛磺胆酸、牛磺脱氧胆酸和卵磷脂等八种化合物的R_f值及层析谱斑点的集中情况,用直观分析和方差分析法处理,得到了单向一次薄层层析全部分离胆汁的溶剂系统,较文献报道方法为佳。     

Characterization of tunnel oxide passivated contact with n-type poly-Si on p-type c-Si wafer substrate

The junction properties of tunnel silicon oxide (SiO_x) passivated contact (TOPCon) with n-type poly-Si on p-type c-Si wafer are characterized using current-voltage (J-V) and capacitance-voltage (C-V) measurements. The dark J-V curves show a standard diode characteristic with a turn-on voltage of ～0.63 V, indicating a p-n junction is formed. While the C-V curve displays an irregular shape with features of 1) a slow C increase with the decrease of the magnitude of reverse bias voltage, being used to estimate the built-in potential (V_bi), 2) a significant increase at a given positive bias voltage, corresponding to the geometric capacitance crossing the ultrathin SiO_x, and 3) a sharp decrease to negative values, resulting from the charge tunneling through the SiO_x layer. The C of depleting layer deviates from the normal linear curve in the 1/C²-V plot, which is caused by the diffusion of P dopants from the n-type poly-Si into the p-type c-Si wafer as confirmed by the electrochemical capacitance-voltage measurements. However, the 1/C^2+γ-V plots with γ > 0 leads to linear curves with a proper γ and the V_bi can still be estimated. We find that the V_bi is the range of 0.75–0.85 V, increases with the increase of the doping ratio during the poly-Si fabrication process, and correlates with the passivation quality as measured by the reverse saturated current and implied open circuit voltage extracted from transient photoconductivity decay.     

Numerical simulations of sloshing and suppressing sloshing using the optimization technology method

Sloshing is a common phenomenon in nature and industry, and it is important in many fields, such as marine engineering and aerospace engineering. To reduce the sloshing load on the side walls, the topology optimization and optimal control methods are used to design the shape of the board, which is fixed in the middle of the tank. The results show that the new board shape, which is designed via topology optimization, can significantly reduce the sloshing load on the side wall.     

Synthesis of deuterium-enriched and fluorine-substituted plinabulin derivatives and evaluation of their antitumor activities

Deuterium-enriched and fluorine-substituted compounds have been widely applied in drug discovery due to their advantages in the studies of clinical pharmacokinetics and metabolic profiles. Herein we synthesized a library of deuterated and fluorine-substituted plinabulin derivatives, and all 15 D- or F-compounds were characterized by MS, \(^{1}\hbox {H}\) NMR and \(^{ 13}\hbox {C}\,\hbox {NMR}\). Their antitumor activities were evaluated against human Jurkat T lymphocyte cells.     

P 1-nonconforming triangular finite element method for elliptic and parabolic interface problems

The lowest order P₁-nonconforming triangular finite element method (FEM) for elliptic and parabolic interface problems is investigated. Under some reasonable regularity assumptions on the exact solutions, the optimal order error estimates are obtained in the broken energy norm. Finally, some numerical results are provided to verify the theoretical analysis.     

基于约束共轭梯度的高能闪光照相图像复原算法

 针对闪光照相系统模糊较大、成像信噪比低的特点,提出了一种基于约束共轭梯度的闪光照相图像复原算法,将闪光照相图像复原问题转化为一个约束优化问题,引入基于非负、中值滤波和偏微分方程的光滑约束条件,并利用约束共轭梯度法迭代求最优解。数值试验表明,该算法能较好再现图像边缘信息,复原出的图像在信噪比和视觉方面都有较大提高。     

纳秒脉冲电压下气体开关的击穿特性

 采用快速Marx发生器产生ns量级的高电压脉冲,分别开展了不同脉冲电压值下气体开关自击穿实验,获得了气体开关在不同气压下的击穿电压和击穿延迟时间以及抖动。详细介绍了纳秒脉冲电压作用下,气体火花开关击穿电压和击穿延迟时间随工作气压变化的特点,指出了气体开关在不同场合应用时的要求。     

一种具有噪声抑制功能的红外图像锐化算法

锐化是图像增强中一项关键性的技术,但如果图像中包含噪声,噪声也会因为锐化而放大,最终导致信噪比的降低.探索了一种算法既可以对图像进行锐化滤波,又不降低图像的信噪比.采用模式识别的相关理论,基于隶属度和概率松弛技术对红外图像中由真实边缘和由各种噪声引起的亮度数值变化进行区分,对不同区域采用不同的锐化处理.该算法不同于传统图像锐化算法只基于局部对比度的缺点,在图像锐化过程中考虑图像边缘和噪声的空间分布的差异,改善了传统边缘增强算法对噪声放大的缺点.实验数据表明,该锐化方法未引起信噪比的降低,具有良好的前景和实用价值.