催化动力学测定食品中痕量甲醛

在H2SO4介质中,甲醛可灵敏催化溴酸钾氧化中性红的褪色反应,研究了该指标反应的动力学参数,建立了动力学光度法测定痕量甲醛的新方法。该方法的检出限为4.08×10-9g/mL,线性范围在0-1.0μg/25mL。用水蒸汽蒸馏法蒸馏甲醛用于食品中甲醛的测定,结果满意。     

ELECTRICALLY FORCED VIBRATION OF A THICKNESS-TWIST MODE PIEZOELECTRIC RESONATOR WITH NON-UNIFORM ELECTRODES

We study the effect of electrodes with varying thickness on thickness-twist vibration of a piezoelectric plate resonator of crystals of 6 mm symmetry.An exact theoretical analysis is performed.Results show that non-uniform electrodes have a strong effect on mode shapes,and suggest the possibility of using nonuniform electrodes for strong energy trapping.     

双色飞秒脉冲场作用下吡啶分子的弛豫动力学研究

利用自制的飞秒激光系统和飞行时间质谱仪结合泵浦探测的方法对吡啶分子的弛豫动力学进行了研究.用265和398nm的飞秒激光分别作为泵浦光和探测光,通过(1+2′)的共振增强多光电子电离的办法测量了C5H5N+离子强度随时间演化的情况,从而测得吡啶分子在265nm激发的S1电子态有一寿命为(3.3±0.1)ps的快速弛豫过程.     

部分相干光学成像系统的光学传递函数和像质评价准则

根据光学成像理论，建立了部分相干成像光学系统的光学传递函数。该函数与非相干成像光学系统传递函数相同，因而部分相干成像和非相干成像两者的光学系统波面像差公差标准也是相同的。这一点解释了显微镜光学系统的光学设计惯用法则：镜头像差公差标准的选择，并不因为采用成像照明方式的不同而有所差异。     

铜(Ⅱ)/H2O2对多巴氧化作用的紫外-可见光谱研究

本文采用紫外－可见光谱法研究了在不同pH条件下铜（Ⅱ）／H2O2对多巴氧化作用的影响。结果表明，pH可影响铜离子催化多巴氧化成黑色素的效率，在弱酸性环境下铜（Ⅱ）的催化作用要比pH7.4时强。     

粗糙波面光学传递函数像质评价准则和粗糙度公式理论

建立了包含波面像差和粗糙度影响的粗糙波面光学传递函数及其像质评价准则，讨论了粗糙度公差的理论和标准。     

SOME PROPERTIES OF A CLASS OF INTERCHANGE GRAPHS

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Synthesis,characterization and in vitro cytotoxicity screening of some triarylbismuth(V) di(N‐salicylidene)amino carboxylates and the crystal structure of (2‐HOC6H4CHNCH2CO2)2Bi(C6H5)3

Four novel triarylbismuth(V) di(N‐salicylidene)amino carboxylates were synthesized. Their structures were confirmed by IR, ¹H NMR, ¹³C NMR and elemental analysis. The crystal structure of (2‐HOC₆H₄CH?NCH₂CO₂)₂BiPh₃ was determined by X‐ray diffraction. The in vitro cytotoxicity of all compounds against three human cancer cells (HL‐60, BGC‐823 and MDA‐MB‐435) at 10 µM are reported. Copyright © 2005 John Wiley & Sons, Ltd.     

Time-resolved Luminescence-based Chemosensor for Fluoride Anion

Design and synthesis of new chemosensors for fluoride anion (F-)1-6 have been of interest to chemists for many years, because F- plays a crucial role in the dental care5 and the treatment of osteoporosis7. Recently, the fluorescent chemosensors of fluorid…     

A Step Tunable External Cavity Semiconductor Laser for WDM Network Deployment

We put forward a kind of tunable external cavity semiconductor laser with feedback on both chip facets. It outputs the single-frequency laser with high side-mode suppression ratio and the frequency could be step tuned.