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91.
[reaction: see text] Treatment of allyl beta-iodoacetals with ethylmagnesium bromide in THF provided tetrahydrofuran derivatives in good yields. On the other hand, the reaction in DME provided tetrahydrofuranylmethylmagnesium compounds in good yields. 相似文献
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Takuya Ogawa Jun Watanabe Yoshito Oshima 《Journal of polymer science. Part A, Polymer chemistry》2009,47(10):2656-2663
A catalyst‐free polysiloxane synthetic process that uses high temperature and pressure water for the hydrolysis and subsequent polycondensation of phenyltrimethoxysilane was studied in detail to gain insights into the reaction mechanism. It was suggested that this process is essentially composed of two stages: (1) oligomerization of phenyltrimethoxysilane yielding low‐molecular weight species with high contents of silanol and methoxy groups and (2) polycondensation of the oligomers yielding high‐molecular weight species. The use of a preformed oligosiloxane as a starting material was informative to understand the polycondensation stage. A modified synthetic process in which a stop valve was introduced to control the internal pressure was developed based on the understanding of the present process. This modified process enabled a two‐stage reaction resulting in a discernible increase of the molecular weight of polysiloxane. © 2009 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 47: 2656–2663, 2009 相似文献
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应用E-GOS(E-Gamma Over Spin)曲线方法研究了A≈110质量区奇A核结构随角动量增加的演化, 发现随着角动量的增加原子核的激发特性从振动逐渐演化为转动。 The E-GOS(E-Gamma Over Spin)curves were used to investigate the structure evolution in the odd A nuclei around A≈110 as a function of spin. The result shows that there is a clear transition from vibration to rotation while increasing spin. 相似文献
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Seiki Oshima 《Journal of Physics and Chemistry of Solids》2011,72(5):398-402
We have developed numerical simulation method for quasi-particle structures in the three-dimensional nano-sized superconductors, using the three-dimensional finite element method and the Bogoliubov-de Gennes equation. Using this method, we analyzed the superconducting state in the nano-sized cubic superconductors. We found the spatial oscillations of order parameter because of the confinement of superconducting electrons, and also we found the quasi-particle bound states at the corners of the cubic superconductors because of suppression of superconductivity at the corners. 相似文献
98.
Fang YongDe Zhang YuHu Oshima M. Toh Y. Xu FuRong Shi Yue Zhou XiaoHong Liu MinLiang Guo YingXiang Koizumi M. Kimura A. Hatsukawa Y. Morikawa T. Nakamura M. Sugaware M. Kusakari H. 《中国科学:物理学 力学 天文学(英文版)》2011,54(1):98-102
A new rotational band has been identified and assigned to 188Au for the first time using the 173Yb(19F,4nγ) reaction at the beam energies of 86 and 90 MeV. This band is proposed to be built on the πh 9/2 ⊗ νi 13/2 configuration by comparing the band properties with known bands in neighboring nuclei. The prolate-to-oblate shape transition through triaxial shape has been proposed to occur around 188Au for the ηh 9/2 ⊗ νi 13/2 bands in odd-odd Au isotopes on the basis of total Routhian surface (TRS) calculations.
相似文献99.
H. B. Zhou X. H. Zhou Y. H. Zhang Y. Zheng M. L. Liu N. T. Zhang L. Chen S. T. Wang G. S. Li H. X. Wang B. Ding X. G. Lei Y. X. Guo G. X. Dong F. R. Xu M. Oshima Y. Toh M. Koizumi A. Osa Y. Hatsukawa 《The European Physical Journal A - Hadrons and Nuclei》2011,47(9):1-7
High-spin states in 101Pd have been investigated by means of in-beam γ-ray spectroscopic techniques via the 76Ge(28Si, 3n) reaction at beam energies of 85 and 95 MeV. The previously known d 5/2 and 1/2?[550] bands were extended to higher spins, and the unfavored signature branch of the 1/2?[550] band was built. The band crossings observed experimentally are explained by the alignment of g 9/2 protons. The band properties in 101Pd are compared with those in the neighboring nuclei and are discussed within the framework of the cranked shell model (CSM). 相似文献
100.