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51.
Muhammad Ali Ehsan Muhammad Adil Mansoor Muhammad Mazhar Asif Ali Tahir Mazhar Hamid K. G. Upul Wijayantha 《应用有机金属化学》2012,26(9):493-498
A single molecular heterobimetallic complex, [Co2Ti(μ3‐O)(TFA)6(THF)3] (1) [TFA = trifluoroacetate, THF = tetrahydrofuran], was synthesized, structurally and spectroscopically characterized and implemented as a single‐source precursor for the preparation of CoTiO3–CoO composite thin films by aerosol‐assisted chemical vapour deposition (AACVD). The precursor complex was prepared by interaction of Co(OAc)2.4H2O [OAc = (CH3COO?)] with Ti(iso‐propoxide)4 in the presence of trifluoroacetic acid in THF, and was analysed by melting point, CHN, FT‐IR, single‐crystal X‐ray diffraction and thermogravimetric analysis. The precursor complex thermally decomposed at 480 °C to give a residual mass corresponding to a CoTiO3–CoO composite material. Good‐quality crystalline CoTiO3–CoO composite thin films deposited at 500 °C by AACVD and characterized through powder X‐ray diffraction and scanning electron microscopy/energy‐dispersive X‐ray spectroscopy show that the crystallites have a rose‐flower‐like morphology with an average petal size in the range of 2–6 µm. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
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Firouz Matloubi Moghaddam Zohreh Mirjafary Marjan Jebeli Javan Sara Motamen Hamid Saeidian 《Tetrahedron letters》2014
A mild and efficient tandem process for the synthesis of new highly substituted 2-pyrones starting from commercially available 2-arylacetic acids has been developed. The synthesis is based on the Knoevenagel condensation of 1,3-cyclohexadiones with various β-formyl-esters, followed by lactonization in the presence of nano ZnO (20 mol %). Moderate to high yields and readily available cheap starting materials are the key features of the present method. 相似文献
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Malik Abdul Waseem ShireenAnjali Srivastava Arjita SrivastavaRahila I.R. Siddiqui 《Tetrahedron letters》2014
Reusable [bmIm]OH was found to be a highly efficient renewable homogenous catalyst for the rapid and convenient synthesis of benzoxazine-4-one derivatives from o-iodobenzoic-acid and benzonitrile at 75 °C in moderate to good yields. This methodology provides a facile and straightforward path to construct other related heterocycles in an eco-compatible fashion. 相似文献
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Mohammadreza Moghaddam-manesh Hamid Beyzaei Mostafa Heidari Majd Sara Hosseinzadegan Kiarash Ghazvini 《Journal of heterocyclic chemistry》2021,58(7):1525-1530
In this study, anticancer, antibacterial (against hospital-isolated antibiotic-resistant Escherichia coli strains), antifungal, and antioxidant effects of synthesized heterocyclic compounds 5 and 7 containing thiazole core were examined. Cytotoxicity testing was utilized against MCF-7 breast cancer cells via MTT cell viability assay. Antibacterial and antifungal activities were checked out according to Clinical and Laboratory Standards Institute (CLSI) guidelines, and antioxidant properties were evaluated through scavenging 2,2-diphenyl-1-picrylhydrazyl (DPPH) free radicals. Results showed the viability of breast cancer cell lines was reliant on concentration of heterocycles and time of incubation. Synthetic compounds exhibited excellent antibacterial and antifungal properties base on their minimum inhibitory concentration (MIC), minimum bactericidal concentration (MBC), and minimum fungicidal concentration (MFC) values as well as high antioxidant activities according to their IC50 values. Higher anticancer and antibacterial properties were observed with compound 7; on the contrary, thiazole 5 had better antioxidant effects. They can be introduced as potent antimicrobial, antioxidant, and anticancer agents. 相似文献
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Latif Pourkarimi 《Optimization》2016,65(11):1983-2005
This paper deals with the robustness issue in deterministic multi-objective linear programming from two new standpoints. It is shown that a robustness notion recently reported in the literature is equivalent to strict efficiency. Corresponding to an efficient solution, a new quantity, robustness order (RO) is defined with respect to the interiority order of the cost matrix in the binding cone. A linear programming problem is provided to calculate the RO of a given efficient solution. The second part of the paper is devoted to investigating the robustness with respect to the eligible angle deviation of the cost matrix in the binding cone. Theoretical results are given to obtain the maximum eligible angle deviation. Finally, the relationship between two above-mentioned robustness standpoints is established. To have a better geometrical view, we prove the results for single-objective LP problems at first, and then we extend them to the multi-objective case. In addition to the theoretical results, some clarifying examples are given. 相似文献
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