不确定时滞Lurie系统的鲁棒绝对稳定性分析

研究了一类不确定Lurie时滞系统的鲁棒绝对稳定性问题，不确定项范数有界。通过构造特殊的李亚普诺夫函数，分别考虑了时滞相关和时滞无关两情况，得到了系统鲁棒绝对稳定的充分条件。     

非对称八烷氧基取代酞菁聚硅氧烷的合成及其单分子膜

非对称八烷氧基取代酞菁聚硅氧烷的合成及其单分子膜穆劲，夏强，华玉晶，周伟东，肖童（山东大学胶体与界面化学研究所，济南，２５０１００）关键词酞菁聚硅氧烷，ＬＢ膜，π－Ａ曲线酞菁化合物是具有高稳定性的大π键共轭体系。目前，酞菁ＬＢ膜研究大多采用单体小分子...     

在极移的Chandler分量上的调制现象

本文利用1980年IPMS重新发表的八十年来地极坐标的新资料(归一化的),采取在非倍频点上进行谱分析的非整数方法,得到了Chandler极移分量的振幅变化与位相变化的频谱。文中还利用相对于这些谱的周期进行叠加,得到了八十年来x_c,y_c的拟合曲线(精度±0.″017),并讨论了太阳黑子的Wolf数的变化周期,认为太阳活动的影响对极移产生调制是造成Chandler极移频谱多峰的原因。     

防激光、防眩光PMMA材料的研制

以聚甲基丙烯酸甲酯为基材,分别以激光吸收剂A和激光吸收剂B作为功能添加剂,制备了能有效地吸收530nm、1060nm波长激光和500～580nm波长眩光的防激光、防眩光PMMA材料。对其防激光、防眩光的性能、可见光透过率和力学性能进行了测试和分析。研究结果表明,实验所制得的防激光、防眩光PMMA材料在530nm波长处的透过率为0.01%,在1060nm波长处的透过率为0.02%,在500～580nm波长范围内该PMMA材料的平均透过率为0.1%左右。     

区域空间演进的宏观、微观产业视角

"城市化、城市现代化,都是一种经济现象,也是一种经济过程",而作为促进经济发展的产业结构调整,则表现出更多的空间特征,随着产业周期的变动,区域结构具有内生性的振荡,如何适时转变便成为一个关键性的课题.以日本为例,探究区域城镇结构变动的内涵.在宏观层次上,分析国际经济环境、产业区位、城市产业集聚动力机制变动所引致的空间变化.在微观层次上,分析公司(企业)的空间组织与效应、产业技术升级与区域城市空间等.     

0212型Ca3Cu2O4+δCl2-y化合物高温高压合成与研究

 利用“顶角氧掺杂”机制，即以二价氧部分替代顶角一价氯，用Ag₂O做氧源，在高温高压下制备了单相的Ca₃Cu₂O_4+δCl_2-y样品。X射线衍射分析发现，随着Ag₂O含量的增加，Ca₃Cu₂O_4+δCl_2-y样品的晶格常数a逐渐变小，c逐渐增大，体现了空穴掺杂的本质。进行了电阻率和磁化率测量，没有发现超导性，可能是空穴载流子没有达到合适的浓度所致。     

钽铌合金材料的冲击压缩特性研究

 对一种新型的钽铌合金材料进行了冲击压缩特性实验研究，通过超声测量得到了其常态下的横波和纵波声速，进而计算得到了其相关的一些静态力学参量。通过二级轻气炮加载技术，得到其在60~196 GPa压力范围内的冲击Hugoniot线。这一测量结果与混合物叠加法估算的结果符合较好，并将这种新型合金材料的力学特性与两种钨合金材料进行了简单对比。比较结果显示，Ta-Nb合金材料是一种具有较好工程应用前景的材料。     

A Novel CFC-12 Hydrolysis Catalyst: WO3/SnO2

Thousands of studies have continuously confirmed that chlorofluorocarbons (CFCs) arekillers of the stratospheric ozone which protects life on earth against harmful ultravioletradiation from the sun'. Although many CFCs have been banned since the MontrealProtocol, there are still 2.25 million ton CFCs all over the world and numerous airconditioning systems still use them. These CFCs are leaking out of existing equipmentsand will not be degraded in nature for 50-100 years because of their c…     

Metal/Matrix Enhanced Time-of-flight Secondary Ion Mass Spectrometry for Single Cell Lipids Analysis

The chemical components analysis of single cell is important for the understanding of physiological processes such as cell growth, signal transduction and apoptosis. Time-of-flight secondary ion mass spectrometry (ToF-SIMS) is a sensitive surface analysis technique with high spatial resolution, which has been used for single cell and micro-area analysis. However, relatively low ionization yield of biomolecules limited its wide applications in single cell analysis. Herein, we used metal substrate and matrix material to enhance the ionization yield of lipids. The signal intensity of phosphatidylcholine (PC 40:0) casted on the matrix/gold-coated silicon substrate was 65 times higher than that on the silicon wafer. The signal enhancement of phosphatidylcholine (PC 34:1) on single cell surface cultured on matrix/gold-coated silicon substrate was observed as well. Owing to the influence of irregular topography and complex chemical environment of cell, the increase of lipids signal was smaller. Delayed extraction mode of ToF-SIMS overcame the effects of cell topography, leading to further enhancement of the signal intensity of lipids. Meanwhile, simultaneous high spatial resolution of chemical imaging and high mass resolution of the mass spectra of single cells were obtained. Our strategies provided new insights into the study of cell metabolism and cell-environment interactions.     

A New Macrocyclic Trichochecene from Soil Fungus

From fermentation broth of soil fungus 254-2 obtained from Yunnan province, a new macrocylic trichochecene was isolated. The structure was determined on the basis of spectroscopie evidences especially the 2-D NMR spectra.