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111.
In order to investigate the long-term effect of the Százhalombatta power plant on the environment of the Csepel-Island subsoil samples were collected in 55 points within 200 km2. Using a microwave-assisted extraction procedure, Be, Ni and V were extracted from the soil samples by aqua regia and the metal concentrations were determined by inductively coupled plasma mass spectrometry (ICP-MS). The analytical results were evaluated by chemometric methods and interpreted considering the main mineral constituents of the subsoil. 相似文献
112.
Sans résumé 相似文献
113.
T. Kàmàn E. Lähderanta S. Leppävuori I. Halàsz I. Dòdony G. Zsolt T. Porjesz R. Laiho A. Uusimäki I. Kirschner Gy. Kovács 《Zeitschrift für Physik B Condensed Matter》1990,78(2):169-173
Tl–Ca–Ba–Cu–O compounds of the nominal composition of (1, 1, 1, 1) have been prepared from different starting materials and with the same heat treatment process. During the investigation of their properties a diamagnetic signal has been found up to the temperature of 132 K. This hints at the existence of a certain material content distributed into discrete superconducting domains. The parameters of it reflect a superstructure of the (2, 2, 2, 3) and (2, 1, 2, 2) compositions having a time-dependent behaviour. On the basis of the signal levels at 132 K and 4.2 K, the quantity of the high temperature superconducting material is about 0.01% of the total one at liquid He temperatures. 相似文献
114.
115.
Summary Reversed-phase, HPLC methods employing post-column derivatization and fluorescence detection were developed for the determination
of the peptide colistin and four aminoglycoside antibiotics in feeds. Extraction of the analytes was by sonication and shaking
with dilute hydrochloric acid. Post-column derivatization was performed using orthophtaldialdehyde-2-mercaptoethanol chemistry.
Assay of colistin was by using an acetonitrile-aqueous sodium sulphate-triethylammonium phosphate (pH 2.8) eluent. Aminoglycoside
antibiotics:amikacin, kanamycin, gentamycin and neomycin were analyzed using a tetrahydrofuran-aqueous sodium sulphate-sodium
pentanesulphonate-acetic acid mobile phase. The method was also applied to some pharmaceutical preparations. Preliminary results
showed that the method can be adapted for the assay of the above antibiotics in meat and animal serum for residue and pharmacokinetic
studies.
Presented at: Balaton Symposium on High-Performance Separation Methods, Siófok, Hungary, September 3–5, 1997. 相似文献
116.
Erika Szunyogová Katarína Györyová Daniela Hudecová Lenka Piknová J. Chomič Zuzanna Vargová V. Zeleňák 《Journal of Thermal Analysis and Calorimetry》2007,88(1):219-223
The thermal decomposition of the complexes Zn(form)2⋅2phen
(I), Zn(ac)2⋅2phen
(II), Zn(prop)2⋅2phen
(III), Zn(but)2⋅2phen
(IV), where phen=phenazone, form=formiate,
ac=acetate, prop=propionate, but=butyrate has been studied in air by TG/DTG
and DTA methods. The possible mechanism of the thermal decomposition was proposed.
The final product of thermal decomposition was ZnO. IR data show unidentate
coordination of carboxylate group to Zn(II) ion. The complexes were tested
against various strains of microorganisms and their efficiency decrease in
the sequence yeasts >bacteria>filamentous fungi. 相似文献
117.
Aart Blokhuis Győrgy Kiss István Kovács Aleksander Malnič Dragan Marušič János Ruff 《组合设计杂志》2007,15(6):491-501
Semiovals which are contained in the union of three concurrent lines are studied. The notion of a strong semioval is introduced, and a complete classification of these objects in PG(2,p) and PG(2,p2), p an odd prime, is given. © 2007 Wiley Periodicals, Inc. J Combin Designs 15: 491–501, 2007 相似文献
118.
K. Belina G. Balazs J. Varga Gy. Hardy J. Horvath K. Nyitrai A. R. Werninck A. J. Shand G. H. W. Milburn 《Liquid crystals》1990,7(3):399-410
As part of a programme investigating mesogenic diacetylenes a symmetrically disubstituted diacetylene has been synthesized and polymerized. Thermal, thermo-optical and IR studies have been carried out to investigate the different crystalline forms of the diacetylene. 相似文献
119.
Dr. Lucas Duffrène René Gy Hélène Burlet Roland Piques Annelise Faivre Anas Sekkat Joseph Perez 《Rheologica Acta》1997,36(2):173-186
The linear viscoelastic behavior of a soda-lime-silica glass under low frequency shear loading is investigated in the glass transition range. Using the time-temperature superposition technique, the master curves of the shear dynamic relaxation moduli are obtained at a reference temperature of 566°C. A method to determine the viscoelastic constants from dynamic relaxation moduli is proposed. However, some viscoelastic constants cannot be directly measured from the experimental curves and others cannot be precisely obtained due to non-linearity effects at very low frequencies. The generalized Maxwell model is investigated from the experimental dynamic moduli without fixing the viscoelastic constants. A set of parameters is shown to be in good agreement with the experimental dynamic relaxation moduli, but does not give the correct values of the viscoelastic constants of the investigated glass. The soda-lime-silica glass exhibits a non-linear viscoelastic behavior at very low stress level which is usually observed for organic glasses. This non-linear behavior is questioned. 相似文献
120.
Direct analysis in real time mass spectrometry (DART‐MS) of highly non‐polar low molecular weight polyisobutylenes
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Lajos Nagy Tibor Nagy György Deák Ákos Kuki Borbála Antal Miklós Zsuga Sándor Kéki 《Journal of mass spectrometry : JMS》2015,50(9):1071-1078
Low molecular weight polyisobutylenes (PIB) with chlorine, olefin and succinic acid end‐groups were studied using direct analysis in real time mass spectrometry (DART‐MS). To facilitate the adduct ion formation under DART conditions, NH4Cl as an auxiliary reagent was deposited onto the PIB surface. It was found that chlorinated adduct ions of olefin and chlorine telechelic PIBs, i.e. [M + Cl]? up to m/z 1100, and the deprotonated polyisobutylene succinic acid [M? H]? were formed as observed in the negative ion mode. In the positive ion mode formation of [M + NH4]+, adduct ions were detected. In the tandem mass (MS/MS) spectra of [M + Cl]?, product ions were absent, suggesting a simple dissociation of the precursor [M + Cl]? into a Cl? ion and a neutral M without fragmentation of the PIB backbones. However, structurally important product ions were produced from the corresponding [M + NH4]+ ions, allowing us to obtain valuable information on the arm‐length distributions of the PIBs containing aromatic initiator moiety. In addition, a model was developed to interpret the oligomer distributions and the number average molecular weights observed in DART‐MS for PIBs and other polymers of low molecular weight. Copyright © 2015 John Wiley & Sons, Ltd. 相似文献