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2-Carbomethoxybenzoyl chloride reacted with some 5-methylamino-l-phenyl-3-R-pyrazoles to yield N-methyl-l-phenyl-3-R-pyrazol-5-yl)-2-carbomethoxybenzamides. These products were readily transformed into the corresponding acid, which in turn, refluxed in phosphorus oxychloride afforded the tricyclic system, l-phenyl-3-R-pyrazolo[3,4-b]benzazepine-4,9-dione. 相似文献
13.
S. Plescia G. Daidone V. Sprio E. Aiello G. Dattolo G. Cirrincione 《Journal of heterocyclic chemistry》1978,15(8):1287-1290
Preparation and structural evidence of N-methyl-(1,3-R,R'-pyrazol-5-yl)-o-nitrobenzamides (VIIIa, b) are discussed. Diazotisation of related o-aminobenzamides XIa,b followed by the Pschorr reaction afforded a very complex mixture from which pyrazolo[3,4-c]isoquinolin-5-ones XIIa.b in 7–10% yields together with N-methyl-(1,3-R,R'-pyrazol-5-yl)-o-hydroxybenzamides (XIIIa) in 15–20% yields were isolated. 相似文献
14.
Salvatore Plescia Giuseppe Daidone Maria L. Bajardi 《Journal of heterocyclic chemistry》1982,19(3):685-687
By reaction of some 4-carbethoxy(or cyano)-3(5)-R-5(3)-aminopyrazoles 1 with 2-nitrobenzoyl chloride or 2-nitrobenzenesulfonyl chloride, a number of novel 3- and 5-amino-1-(2-nitrobenzoyl or 2-nitrobenzene-sulfonyl)pyrazoles 6 and 7 were obtained. Every compound appearing during the endocyclic N-substitution process can be identified and determined by glc. The use of nmr offers a rapid, unambigous method for determining the proposed structures. 相似文献
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16.
Stochastic Burgers' equation 总被引:6,自引:0,他引:6
Guiseppe Da Prato Arnaud Debussche Roger Temam 《NoDEA : Nonlinear Differential Equations and Applications》1994,1(4):389-402
We consider a Burgers' equation perturbed by white noise. We prove the existence and uniqueness of the global solution as well as the existence of an invariant measure for the corresponding transition semigroup. 相似文献
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E. Aiello G. Dattolo G. Cirrincione S. Plescia G. Daidone 《Journal of heterocyclic chemistry》1978,15(4):537-539
A new synthesis of pyrrolo[3,2-b] pyridine starting with pyrrole ring is described. The procedure allows the synthesis of 4-azaindoles bearing a sensitive group at C-7. The nitration of 4b with nitric acid and acetic anhydride at ?15° gave 5 . The hydrogenation of 5 led to simultaneous reduction of N-hydroxy and nitro groups and to hydrogenolysis of the isoxazole nucleus, affording an appropriate chain of atoms to building up the pyrrolo[3,2-b] pyridine ring. 相似文献
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Stefano Marchese Daniela Perret Alessandra Gentili Guiseppe D'Ascenzo Angelo Faberi 《Rapid communications in mass spectrometry : RCM》2002,16(2):134-141
An evaluation was made of the feasibility of using reversed-phase liquid chromatography/tandem mass spectrometry with an electrospray interface (LC/ESI-MS/MS) to measure traces of phenoxyacid herbicides and their metabolites in surface and drinking water samples. The procedure involved passing 0.5 L of river and drinking water samples through a 0.5 g graphitized carbon black (GCB) extraction cartridge. Recovery was higher than 85% irrespective of the aqueous matrix in which the analytes were dissolved. A conventional 4.6-mm i.d. reversed-phase LC C-18 column operating with a mobile phase flow rate of 1 mL/min was used to chromatograph the analytes. A flow of 200 microL/min of the column effluent was diverted to the ESI source. The limits of detection (signal-to-noise ratio = 3) of the method for the pesticides considered in drinking and surface water samples are less than 0.1 ng/L for phenoxyacid herbicides, and about 5-10 ng/L for their metabolites (2,4-dichlorophenol and 4-chloro-2-methylphenol). 相似文献