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51.
In this paper, tubular structure has been obtained by self-assembly of cholesterol derivative via sol–gel process. The tube structure and the formation mechanism have been studied and certified by scanning electron microscopy, infrared, ultraviolet-visible spectroscopy (UV–vis) and x-ray diffraction (XRD) data. It is predicated that the tube has been formed by the curl of sheet structure, and the aggregates are composed of two molecules of 1 with H aggregate in laminar structure at micro level. 相似文献
52.
A new PVC membrane mercury(II) ion electrode based on N,N-dimethylformamide-salicylacylhydrazone (DMFAS) as an ionophore is described, which shows excellent potentiometric response characteristics and displays a linear log[Hg(2+)] versus EMF response over a wide concentration range between 6.2 x 10(-7) and 8.0 x 10(-2) M with a Nerstian slope of 29.6 mV per decade and a detection limit of 5.0 x 10(-7) M. The response time for the electrode is less than 30 s and the electrode can be used for more than 2 months with less than a 2 mV observed divergence in a potentials. The proposed electrode exhibits very good selectivity for mercury(II) ions over many cations in a wide pH range (pH 1 - 4). The electrode was also applied to the determination of a mercury(II) ion in vegetables and in Azolla filiculoides. 相似文献
53.
ON A MIN-MAX THEOREM 总被引:2,自引:0,他引:2
WUGUANGRONG HUANGWENHUA SHENZUHE 《高校应用数学学报(英文版)》1997,12(3):293-298
In this paper we prove a nonvariational form of a rain-max problem in [l] and give its application to a periodical problem. 相似文献
54.
我国教育体制的改革,给中等职业学校的教学工作提出了新的挑战.下面就中等职业学校的物理教学方法谈几点意见: 物理教学课分为4种主要类型:实验教学,概念教学,练习教学和复习教学.1 实验教学课 物理实验是在人为控制条件下,运用仪器、设备、使物理现象反复再现,从而有目 相似文献
55.
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57.
火焰原子吸收光谱法测定20型尼龙毡材料中的铁 总被引:2,自引:1,他引:1
采用空气-乙炔火焰原子吸收光谱法测定镍镉电池尼龙毡材料中的铁含量,对测定条件和干扰因素进行了综合分析。铁的浓度在0.0~5.0μg/mL内与吸光度成线性关系,相关系数为0.9998。测定尼龙毡样品铁含量的相对标准偏差不大于1.0%(n=8),标准加入回收率为97.0%~98.0%。该法适用于镍镉电池尼龙毡中铁含量的控制分析。 相似文献
58.
运用N2O-C2H2火焰原子吸收光谱法测定电化学浸渍液中的钴含量。通过试验确定了共振线、燃烧器高度、灯电流、酸性介质、火焰等实验条件。用该方法对样品中钴含量进行分析,测定结果的相对标准偏差小于1.0%(n=6),加标回收率为97.3%~98.8%。该方法适用于电化学浸渍液中钴含量的控制分析和样品系统分析。 相似文献
59.
Junhan?Liu Cheng?Yuan Guangrong?Hu Fuli?LiEmail author 《Applied biochemistry and biotechnology》2012,166(8):2127-2137
Scenedesmus spp. have been reported as potential microalgal species used for the lipid production. This study investigated the effects
of light intensity (at three levels: 50, 250, and 400 μmol photons m−2 s−1) on the growth and lipid production of Scenedesmus sp. 11-1 under N-limited condition. Carotenoid to chlorophyll ratio was higher when algae 11-1 grew under 250 and 400 μmol
photons m−2 s−1 than that under 50 μmol photons m−2 s−1, while protein contents was lower. Highest biomass yield (3.88 g L−1), lipid content (41.1 %), and neutral lipid content (32.9 %) were achieved when algae 11-1 grew at 400 μmol photons m−2 s−1. Lipid production was slight lower at 250 μmol photons m−2 s−1 level compared to 400 μmol photons m−2 s−1. The major fatty acids in the neutral lipid of 11-1 were oleic acid (43–52 %), palmitic acid (24–27 %), and linoleic acid
(7–11 %). In addition, polyunsaturated fatty acids had a positive correlation with total lipid production, and monounsaturated
fatty acids had a negative one. 相似文献
60.