线圈炮电枢电磁-热耦合仿真分析

 从麦克斯韦方程组和导热微分方程出发,导出了3维多级感应线圈炮电磁场、温度场分布的基本方程,并以电磁场和温度场有限元分析为基础,建立了3维有限元分析模型,忽略级间的相互影响,多级线圈炮中电枢温升可以等效为多个单级电枢的温升,运用通用有限元分析软件ANSYS的耦合计算流程,对单级感应线圈炮中电枢电磁场和温度场进行仿真。计算中考虑了材料物理参数随温度变化对温度场的影响。仿真结果表明：电枢内的温升主要分布在电枢的外表面和尾部;电枢的温度随着电容器组电压和电容增加而升高,这是因为总能量增大,电枢中涡流也增大,从而电枢的温度升高;电枢的触发位置和速度匹配关系,也会对电枢温升造成很大的影响;电枢的温度随着级数的增加逐渐升高,说明电枢在一定级数后达到了材料的熔点而被破坏。     

Ultrasound-assisted extraction of phillyrin from Forsythia suspensa

Forsythia suspensa (Thunb.) Vahl is one of the most widely used traditional Chinese medicines, and possesses important biological activities, such as antibacterial, antiviral, anti-inflammatory and antioxidant activities. Phillyrin is the main bioactive component of Forsythia suspensa. In this paper, ultrasound-assisted extraction of phillyrin from Forsythia suspensa was studied with HPLC-photodiode array detection. Effects of several experimental parameters, such as type and concentration of extracting solvent, ratio of liquid to material, extraction temperature, and time of sonication on extraction efficiencies of phillyrin from Forsythia suspensa were evaluated. The optimal extraction conditions were 1g plant sample with 10 ml of 20% methanol and the extraction for 60 min at 60°C under ultrasonic irradiation. Under the optimum conditions, the yield of phillyrin was 0.713±0.009 mg/g. The results indicated that the ultrasound-assisted extraction is a very useful method for the extraction of important phytochemicals from plant materials.     

Methane non-oxidative aromatization on Mo/ZSM-5: Effect of adding triethoxyphenylsilanes into the synthesis system of ZSM-5

A series of ZSM-5 zeolites were synthesized by adding triethoxyphenylsilane (PTEOS) into the initial sol of the synthesis system. The samples were studied by XRD, SEM, N₂ adsorption-desorption and acid assessment of d₃-acetonitrile adsorption. Characterization results showed that the crystal size of the ZSM-5 zeolites could be adjusted in a certain range by introducing different contents of PTEOS. Besides, the resultant materials possess hierarchical porosity in addition to those micropores generated by the MFI channels. Moreover, supported Mo/ZSM-5 catalysts were prepared, and their catalytic performances were investigated in the methane non-oxidative aromatization. It was found that the Mo/ZSM-5 catalyst, bearing suitable crystal size and mesoporous characteristic showed relatively high shape-selectivity to benzene and high stability for the reaction of methane aromatization.     

水中镉含量的激光诱导击穿光谱高灵敏快速检测

 为了对水中的痕量镉进行高灵敏快速检测,实验采用一种未受污染的薄木片作为基底来吸收水样品,将其晾干后再用激光诱导击穿光谱（LIBS）技术对其进行分析,克服了用LIBS技术直接分析水样品时灵敏度低和稳定性差等问题。实验中选择214.44 nm的镉离子线作为分析线以提高光谱检测的灵敏度,建立了用于定量分析的校正曲线,镉的检出限达到55 μg/L,重复测量的信号相对标准偏差小于5%,单次测量的时间短于5 min。     

A low-threshold and high-power oxide-confined 850-nm AlInGaAs strained quantum-well vertical-cavity surface-emitting laser

A low-threshold and high-power oxide-confined 850-nm AlInGaAs strained quantum-well (QW) vertical-cavity surface-emitting laser (VCSEL) based on an intra-cavity contacted structure is fabricated. A threshold current of 1.5 mA for a 22 μm oxide aperture device is achieved, which corresponds to a threshold current density of 0.395 kA/cm². The peak output optical power reaches 17.5 mW at an injection current of 30 mA at room temperature under pulsed operation. While under continuous-wave (CW) operation, the maximum power attains 10.5 mW. Such a device demonstrates a high characteristic temperature of 327 K within a temperature range from -12℃ to 96℃ and good reliability under a lifetime test. There is almost no decrease of the optical power when the device operates at a current of 5 mA at room temperature under the CW injection current.     

Beam deflection and splitting using transformation optics

We propose a scheme to achieve beam defecting and splitting using a method of embedded coordinate transformation [1]. In this method one boundary of transformation region is not involved in the transformation, which means beam defecting and splitting can be realized by changing the geometric construction. Although there is a discontinuous boundary, the impendence is matched between transformation media and surrounding media according to the conventional transformation optics. Full-wave numerical simulations further verify the theoretical analysis.     

Nonvolatile photorefractive holographic recording in Sc:Ce:Cu:LiNbO3

In this paper experimental studies of nonvolatile photorefractive holographic recording in Ce:Cu:LiNbO₃ crystals doped with Sc(0,1,2,3 mol%) were carried out. The Sc:Ce:Cu:LiNbO₃ crystals were grown by the Czochralski method and oxidized in Nb₂O₅ powders. The nonvolatile holographic recording in Sc:Ce:Cu:LiNbO₃ crystals was realized by the two-photon fixed method. We found that the recording time of Sc:Ce:Cu:LiNbO₃ crystal became shorter with the increase of Sc doping concentration, especially doping with Sc(3 mol%), which exceeds the so-called threshold, and there was little loss of nonvolatile diffraction efficiencies between Sc(3 mol%):Ce:Cu:LiNbO₃ and Ce:Cu:LiNbO₃ crystals.     

Monte Carlo simulation of magnetic nanostructured thin films

Using Monte Carlo simulation, we have compared the magnetic properties between nanostructured thin films and two-dimensional crystalline solids. The dependence of nanostructured properties on the interaction between particles that constitute the nanostructured thin films is also studied. The result shows that the parameters in the interaction potential have an important effect on the properties of nanostructured thin films at the transition temperatures.     

利用傅里叶变换红外光谱法鉴定小麦品种

利用傅里叶变换红外(FTIR)光谱法分析了8个不同小麦品种根部的红外光谱图,对红外光谱图的吸收峰进行了归属分析,通过对各谱图的比对发现,在相同波数范围内,不同的小麦品种其红外谱图的形状、波数及吸收峰的多少有所不同。结果表明不同小麦品种的红外光谱图有明显的差异,其一在2800～2980cm-1波数范围内,此区反映的主要是甲基、亚甲基的伸缩振动,化合物分子链的长短、分子量的大小在此区有显现;其二差别较大的区域在1510～1730cm-1范围内,它反映的主要是酰胺的氮原子及α碳原子取代基的性质,可能是源于基因的差异,此区域内谱图差异较大。因此FTIR光谱法可用于不同小麦品种的鉴别。     

一种新型有机电致微腔结构的双模发射

采用结构Glass／DBR／ITO／NPB／NPB：Alq／Alq／Al制作了有机微腔电致发光器件。将空穴传输材料与发光材料以一定比例混合作为发光层，为了便于对比，在不改变有机层的膜厚的情况下同时制作了传统的异质结微腔器件，发现两种器件的发光光谱有很大不同，器件的复合效率与传统的异质结器件相比也得到了很大提高，这是因为将两种有机材料混合能消除界面势垒，提高器件的复合效率，从而提高了器件的发光性能，实现了微腔双模发射，且两个模式的半峰全宽分别为8nm和12nm。通过进一步优化器件结构可以实现微腔白光发射。