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11.
金的化学状态对Au/CoCeOx催化剂CO氧化性能的影响 总被引:1,自引:1,他引:0
以CoCeOx复合氧化物为载体,采用沉积沉淀法制备了负载型的金催化剂,并通过不同温度的预处理控制Au的化学状态. 使用粉末X射线衍射、高分辨透射电子显微镜、程序升温还原和X射线光电子能谱对催化剂进行了表征,考察了在室温条件下该系列催化剂的一氧化碳氧化性能. 结果表明, Au/CoCeOx催化剂的CO氧化性能与催化剂表面Au 的含量成正比, Au 可能是反应的主要活性物种. 添加水汽对反应有一定的促进作用,但由于Au 不能稳定存在,特别是当催化剂表面Au 的含量过高时,在水汽的作用下Au 迅速发生歧化反应,使得催化剂的性能下降. 相似文献
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M. B. Tsetlin A. A. Teplov S. I. Belousov S. N. Chvalun E. A. Golovkova S. V. Krasheninnikov E. K. Golubev E. B. Pichkur P. V. Dmitryakov A. I. Buzin 《Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques》2018,12(2):277-285
Samples of composites with polytetrafluoroethylene as the matrix and a powder of 0, 1, 2, 4, 8, 16, and 32 vol % Al–Cu–Fe quasi-crystal as the filler are prepared. Electron microscopy studies of the sample structure are carried out, the influence of the filler on the degree of crystallinity and the melting and destruction temperatures of the samples is investigated; mechanical tensile tests and tribological tests are performed. The composite samples with filler contents of 4, 8, 16, and 32 vol % show ultralow wear with the coefficient K < 5 × 10–7 mm3/N m. The highest wear resistance exceeding that of unfilled polytetrafluoroethylene by 2200–3100 times is recorded in composites with 16 vol % filler. An increase in the wear resistance is associated with formation on the friction surface of a thin crust containing quasi-crystal particles 0.2–0.3 μm in size, revealed by scanning electron microscopy in combination with energy dispersive analysis. 相似文献
13.
给出了示波器观测铁磁材料物质磁滞回线的基本原理,针对实验中常见的错误,介绍了如何选取合理的数据并快速描绘磁滞回线的技巧。 相似文献
14.
In this study, ultrasonic backscattering signals in cancellous bones were obtained by finite difference time domain (FDTD) simulations, and the effect of trabecular material properties on these signals was analyzed. The backscatter coefficient (BSC) and integrated backscatter coefficient (IBC) were numerically investigated for varying trabecular bone material properties, including density, Lame coefficients, viscosities, and resistance coefficients. The results show that the BSC is a complex function of trabecular bone density, and the IBC increases as density increases. The BSC and IBC increase with the first and second Lame coefficients. While not very sensitive to the second viscosity of the trabeculae, the BSC and IBC decrease as the first viscosity and resistance coefficients increase. The results demonstrate that, in addition to bone mineral density (BMD) and microarchitecture, trabecular material properties significantly influence ultrasonic backseattering signals in cancellous bones. This research furthers the understanding of ultrasonic backscattering in cancellous bones and the characterization of cancellous bone status. 相似文献
15.
In this study, a coupled-channel (CC) analysis of the elastic and the inelastic scattering of 20.4 MeV polarized protons from
a 64Zn target leading to the deformed 2 + , 3 −, 22+2_2^+ states was performed. The CC potential parameters and the deformation parameters of the excited states corresponding to the
best fit to the experimental differential cross-sections and the analysing powers data were determined. For 22+2_2^+ excited state, a mixed type was used and a good fit to the data was provided. The CC calculation results were compared to
the pure distorted wave Born approximation (DWBA) calculation results which were calculated using the new parameters. All
calculations were conducted using the computer code ECIS06. 相似文献
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Belyakova LA Besarab LN Roik NV Lyashenko DY Vlasova NN Golovkova LP Chuiko AA 《Journal of colloid and interface science》2006,294(1):11-20
Silicas chemically modified with attached aminopropyl, imidazolyl, and trimethylsilyl groups, with adsorptive and coordinative grafted hemin were synthesized. Adsorption of some bile acids on the surface of hydroxylated silica, synthesized siliceous adsorbents and cholestyramine has been studied. It was found that the main contribution to the total adsorption is caused by electrostatic attraction between anions of bile acids and positively charged sites of the surface of modified silica and also by dispersion interactions between steroid skeleton of bile acids and functional groups of modified silicon dioxides. It was established that the kinetic parameters of adsorption and adsorptive capacity for all investigated siliceous adsorbents exceed similar characteristics for cholestyramine. The best of synthesized adsorbents is hemin-containing adsorbent IX, and the sequence of increase in its adsorptive capacity in relation to bile acids corresponds to the following series: I < III < II, IV < VI < V < VIII < VII < IX. 相似文献
20.
Recently, the notion of an S-metric space is defined and extensively studied as a generalization of a metric space. In this paper, we define the notion of the S∞-space and prove its completeness. We obtain a new generalization of the classical "Picard Theorem". 相似文献