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181.
182.
Benzildithiosemicarbazone (BDTSC) is proposed as a sensitive and selective analytical reagent for the extractive spectrophotometric determination of copper(II). BDTSC reacts with copper(II) in the pH range 1.0-7.0 to form a yellowish complex. Beer's law is obeyed in the concentration range 0.5-0.4 microg cm(-3). The yellowish Cu(II)-BDTSC complex in chloroform shows a maximum absorbance at 380 nm, with molar absorptivity and Sandell's sensitivity values of 1.63 x 10(4) dm3 mol(-1) cm(-1) and 0.00389 microg cm(-2), respectively. A repetition of the method is checked by finding the relative standard deviation (RSD) (n = 10), which is 0.6%. The composition of the Cu(II)-BDTSC complex is established as 1:1 by slope analysis, molar ratio and Asmus' methods. An excellent linearity with a correlation coefficient value of 0.98 is obtained for the Cu(II)-BDTSC complex. The instability constant of the complex calculated from Edmond and Birnbaum's method is 7.70 x 10(-4) and that of Asmus' method is 7.66 x 10(-4), at room temperature. The method is successfully employed for the determination copper(II) in pharmaceutical and environmental samples. The reliability of the method is assured by analyzing the standard alloys (BCS 5g, 10g, 19e, 78, 32a, 207 and 179) and by inter-comparison of experimental values, using an atomic absorption spectrometer. 相似文献
183.
184.
A. G. Chentsov 《Journal of Mathematical Sciences》2007,140(6):873-904
The paper considers the representations of attraction sets in topological spaces and their relations with the relaxation of
accessibility problems under the conditions of sequentially relaxed constraints. The author studies the structure of approximate
(in essence, asymptotic) solutions and generalized elements and establishes the possibility of their real identification for
a certain version (related to the Stone-Čech compactification and the Wallman relaxation) of relaxation of the initial problem.
__________
Translated from Sovremennaya Matematika i Ee Prilozheniya (Contemporary Mathematics and Its Applications), Vol. 26, Nonlinear
Dynamics, 2005. 相似文献
185.
186.
W. G. Habashi G. Baruzzi M. F. Peeters M. M. Hafez 《Numerical Methods for Partial Differential Equations》1991,7(2):193-207
Finite element solutions of the Euler and Navier-Stokes equations are presented, using a simple dissipation model. The discretization is based on the weak-Galerkin weighted residual method and equal interpolation functions for all the unknowns are permitted. The nonlinearity is iterated upon using a Newton method and at each iteration the linear algebraic system is solved by a direct solver with all unknowns fully coupled. Results are presented for two-dimensional transonic inviscid flows and two- and three-dimensional incompressible viscous flows. Convergence of the algorithm is shown to be quadratic, reaching machine accuracy in very few iterations. The inviscid results demonstrate the existence of nonunique numerical solutions to the steady Euler equations. 相似文献
187.
S. R. Tuikina 《Computational Mathematics and Modeling》2007,18(1):10-18
We consider a mathematical model of sorption that allows for external diffusion kinetics and a redox reaction. Two inverse
problems are considered for this model, uniqueness is proved, and numerical solution methods are proposed. The efficiency
of the numerical methods is investigated by computer experiments.
__________
Translated from Prikladnaya Matematika i Informatika, No. 23, pp. 15–23, 2006. 相似文献
188.
189.
I. P. Raevskii L. A. Reznichenko M. P. Ivliev V. G. Smotrakov V. V. Eremkin M. A. Malitskaya L. A. Shilkina S. I. Shevtsova A. V. Borodin 《Crystallography Reports》2003,48(3):486-490
(Na, K)NbO3 crystals with a perovskite structure and a KNbO3 content up to 40 mol % were grown from flux with the use of the solvent NaBO2. The dielectric measurements of the crystals grown revealed phase transitions that had never been observed before in ceramic samples. 相似文献
190.
We consider the method of Poincaré to investigate thelocal index of vector fields in the plane. If m is the degreeof the first non-zero jet, Xm, of the vector field X at an isolatedzero, we explore the geometry of the pencil generated by thecoordinate functions of Xm when the absolute value of the indexof X, |ind (X)|, is m. We also find necessary and sufficientconditions for |ind (X)| to be m. 相似文献