SOME TOPICS ON WAVELET ANALYSIS

A review of the advance in the theory of wavelet analysis in recent years is given.     

Molecular deposition film of porphyrin and phthalocyanine bearing oppositely charged substituents

Ｔｈｅｆｏｒｍａｔｉｏｎｏｆａｎｅｗｔｙｐｅｏｆｓｅｌｆ＿ａｓｓｅｍｂｌｅｄｍｕｌｔｉｌａｙｅｒｆｉｌｍｓ,ｍｏｌｅｃｕｌａｒｄｅｐｏｓｉｔｉｏｎ(ＭＤ)ｆｉｌｍｓ[1,2],ｉｓａｆａｓｔｄｅｖｅｌｏｐｉｎｇａｒｅａｏｆｔｈｉｎｆｉｌｍｒｅｓｅａｒｃｈ.Ｔｈｉｓｎｅｗｍｅｔｈｏｄｏｆｆｉｌｍｐｒｅｐａｒａｔｉｏｎｉｓｂａｓｅｄｏｎｉｏｎｉｃａｔｔｒａｃｔｉｏｎｂｅｔｗｅｅｎｏｐｐｏｓｉｔｅｃｈａｒｇｅｄｃｈｒｏｍｏｐｈｏｒｅｓ.ＩｎｃｏｍｐａｒｉｓｏｎｗｉｔｈｔｈｅｃｌａｓｓｉｃＬａｎｇｍｕｉｒ＿Ｂｌｏ…     

微波常压法合成水杨酸酯

在浓硫酸催化下，采用微波常压法由水杨酸分别与正丁醇、异丁醇、正戊醇和异戊醇反应合成相应的水杨酸酯。结果表明：当水杨酸：醇：Ｈ２ＳＯ４＝１：５．５：０．３（摩尔比）时，采用５６０Ｗ微波辐射２２ｍｉｎ，水杨酸酯的产率可达８８．７％￣９６．４％，反应速度至少是常规反应的１４倍。     

兖州高硫煤的加氢热解脱硫及脱硫动力学

在加压热天平上，考察了氢气和氮扬气氛下高硫煤的热解脱硫。利用气相色谱在线分析研究了硫化氢氢气的逸出规律。结果表明，加氢热解比氮气下的热解有着更显著的脱友作用，脱硫率可达９０％以上。而且加氢热解下６５％的脱除硫转化为气相硫化氢，而氮气下热解是有８０％的硫转化为液相。     

Study on fluorescence property of dopamine and determination of dopamine by fluorimetry

In this study, a rapid and sensitive high performance liquid chromatography-inductively coupled plasma-mass spectrometry (HPLC-ICP-MS) determination of primary As species in fish tissues and urine is reported. The separation was achieved on an Altima C18 column with a mobile phase containing citric acid and hexanesulfonic acid (pH 4.5). As(V), monomethylarsonic acid (MMA), As(III), dimethylarsinic acid (DMA) and arsenobetaine (AsB) were separated in less than 4 min with retention times of 83, 99, 130, 166 and 208 s, respectively. This separation of five species in less than 4 min should be attractive to those interested in As speciation. The quantification limits were 44, 56, 94, 64, 66 ng l(-1) and the relative standard deviations (R.S.D.) for day-to-day injections of As at 2 mug l(-1) were 2.0, 3.1, 2.4, 3.8 and 4.0%. The procedure was tested using two reference materials (DORM-2 dogfish muscle tissue, NIST SRM 2670 Freeze-dried Urine, normal level) and then applied to real-world samples. The results obtained demonstrate the suitability of the procedure for screening and quantification at physiological levels of primary As species in biological samples.