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排序方式: 共有1008条查询结果,搜索用时 15 毫秒
11.
Biabangard Fatemeh Nazari Hadiseh Arefinia Reza 《Journal of Solid State Electrochemistry》2021,25(3):881-893
Journal of Solid State Electrochemistry - A stable suspension of nanopolyaniline (nPANI) particles can be used in various applications instead of a polyaniline film. The electrochemical behavior of... 相似文献
12.
Preparation and characterization of Cu (II) supported on poly(8‐hydroxyquinoline‐p‐styrene sulphonate) and its application as catalyst for the synthesis of hexahydroquinolines
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Ardeshir Khazaei Mahsa Tavasoli Vahid Jamshidi Fatemeh Gohari Ghalil Ahmad Reza Moosavi‐Zare 《应用有机金属化学》2018,32(7)
Cu ( II ) supported on poly(8‐hydroxyquinoline‐p‐styrenesulfonate) (Cu ( II )@PHQSS) was prepared and fully characterized by the different techniques including fourier transform infrared spectroscopy (FT‐IR), 1H NMR, 13C NMR, thermal gravimetric analysis (TGA), differential thermal gravimetric (DTG), differential thermal analysis (DTA), scanning electron microscope (SEM) and energy dispersive X‐ray analysis (EDS). Afterward, the Cu ( II )@PHQSS as nanostructured catalyst was used as catalyst for the synthesis of hexahydroquinolines. 相似文献
13.
A simple, inexpensive, environmentally friendly and efficient route for Michael addition of indoles to α,β-unsaturated ketones using pentafluorophenylammonium triflate (PFPAT) as a catalyst is described. Various indole derivatives were synthesized in good to excellent yields. The preparation of PFPAT catalyst from simple and readily available starting materials makes this method more affordable. 相似文献
14.
Maryam Mohammadikish Fatemeh Davar Mohammad Reza Loghman-Estarki 《Journal of Cluster Science》2013,24(1):217-231
In this work, we report a facile hydrothermal method for the preparation of three dimensional hollow ZnS nanostructures, using Zinc bis(salicyle aldehitato), Zn(Sal)2, thioacetamide (TAA) and thioglycolic acid (TGA) as Zn2+, sulfur source and capping agent, respectively. The ZnS solid and hollow sphere was produced from the self-assembly of nanoparticles with diameters of 11 ± 2 nm with TGA and TGA, TAA, respectively. Furthermore, with changing zinc precursor from Zn(Sal)2 to zinc acetate [Zn(OAC)2], ZnS nanorods were obtained. The products were characterized by XRD, SEM, TEM, selected area electron diffraction, and FT-IR spectra. The influence of surfactant (Polyethylene glycol) on the morphology of the products was also investigated. Possible formation mechanism and optical properties of these architectures were also reported. 相似文献
15.
Masoud Salavati-Niasari Bahareh Shoshtari-Yeganeh Fatemeh Mohandes 《Journal of Cluster Science》2013,24(3):657-667
In this work, Pb(II)N,N-bis(salicylidene)-ethylenediamine; [Pb(salen)]; was applied as lead precursor to synthesis PbSe nanostructures. Besides [Pb(salen)], SeCl4 and reducing agents like N2H4·H2O have been employed for the production of PbSe nanostructures via a solvothermal route at 180 °C for 3 h in propylene glycol. The effect of preparation factors such as temperature, reaction time, and surfactant on the morphology of PbSe nanostructures was investigated. The experimental results indicated that PbSe synthesized at 150 and 210 °C was composed of agglomerated particles. On the other hand, the use of KBH4 as reducing agent led to produce PbSe with higher particle size and agglomeration. The as-prepared PbSe nanostructures were characterized by XRD, SEM, TEM, EDS, and FT-IR. 相似文献
16.
17.
Fatemeh Osanlou Firouzeh Nemati Samaneh Sabaqian 《Research on Chemical Intermediates》2017,43(4):2159-2174
18.
By the reaction of 4-chlorobenzaldehyde with ethyl acetoacetate, malononitrile, and hydrazine hydrate, 6-amino-4-(4-chlorophenyl)-3-methyl-2,4-dihydropyrano[2,3-c]pyrazole-5-carbonitrile was prepared and then reacted with salicylaldehyde and CoCl2·6H2O to produce nano-Co-[4-cholorophenyl-salicylaldimine-methylpyranopyrazole]Cl2 (nano-[Co-4CSMP]Cl2). The prepared nano-Schiff base complex was reported for the first time and fully characterized by Fourier transform-infrared spectroscopy, thermal gravimetric analysis, differential thermal gravimetric analysis, scanning electron microscopy, energy-dispersive X-ray spectroscopy, transmission electron microscopy, and Brunner–Emmett–Teller analyses and applied as an efficient catalyst for the synthesis of some 1-amidoalkyl-2-naphthol derivatives. 相似文献
19.
In this work, for the first time, Solanum melongena plant extract was used for the green synthesis of Pd/MnO2 nanocomposite via reduction osf Pd(II) ions to Pd(0) and their immobilization on the surface of manganese dioxide (MnO2) nanoparticles (NPs) as an effective support. The synthesized nanocomposite were characterized by various analytical techniques such as Fourier transform infrared (FT‐IR), X‐ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), energy dispersive X‐ray spectroscopy (EDS) and UV–Vis spectroscopy. The catalytic activity of Pd/MnO2 nanocomposite was used as a heterogeneous catalyst for the one‐pot synthesis of 5‐substituted 1H‐tetrazoles from aryl halides containing various electron‐donating or electron‐withdrawing groups in the presence of K 4 [Fe (CN) 6 ] as non‐toxic cyanide source and sodium azide. The products were obtained in good yields via a simple methodology and easy work‐up. The nanocatalyst can be recycled and reused several times with no remarkable loss of activity. 相似文献
20.
We present a facile and efficient method for modifying the surface of silica-coated Fe3O4 magnetic nanoparticles (MNPs) with bis(pyrazolyl) triazine ruthenium(II) complex [ MNPs@BPT–Ru (II) ] . Field emission-scanning electron microscopy, thermogravimetric/derivative thermogravimetry analysis, X-ray powder diffraction, Fourier-transform infrared spectroscopy, vibrating sample magnetometry, and energy-dispersive X-ray spectrometry analyses were employed for characterizing the structure of these nanoparticles. MNPs@BPT–Ru(II) nanoparticles proved to be a magnetic, reusable, and heterogeneous catalyst for the hydrogen transfer reduction of ketone derivatives. In addition, highly pure products were obtained with excellent yields in relatively short times in the presence of this catalyst. A comparison of this catalyst with those previously used for the hydrogen transfer reactions proved the uniqueness of MNPs@BPT–Ru(II) nanoparticle which is due to its inherent magnetic properties and large surface area. The presented method also had other advantages such as simple reaction conditions, eco-friendliness, high recovery ability, easy work-up, and low cost. 相似文献