Determination of the levels of 1-octacosanol is important in food stuff for the study of its pharmacological activities and health benefits. In this study, a novel, simple and fast internal standard method for the non-derivatization ultra-performance liquid chromatographic determination of 1-octacosanol in raw materials and health products was developed and validated based on evaporative light scattering detection. The linearity (r2 > 0.998), recovery (99.1–100.2%, RSD <2.7%), intra- and inter-day precision (RSD <3.8%), limit of detection (1.0 mg/L), limit of quantification (2.2 mg/L) of the 1-octacosanol were determined. The method was successfully applied to nine real 1-octacosanol products. The results of analyses had close agreement with the labeled claims of 1-octacosanol content in these products. Compared with the classical gas chromatography method, the developed method was simpler, faster and more environmentally friendly due to avoiding any derivatization step. This protocol represents a rapid and feasible method for quality control of 1-octacosanol products.
In this paper we investigate the
probabilistic linear $(n,\delta)$-widths and $p$-average linear
$n$-widths of the Sobolev space $W^r_2$ equipped with the Gaussian
measure $\mu$ in the $L_{\infty}$-norm, and determine the
asymptotic equalities
\begin{eqnarray*}
\lambda_{n,\delta}(W^r_2,\mu,L_{\infty})
&\asymp&\frac{\sqrt{\ln
(n/\delta)}}{n^{r+(s-1)/2}},\\[3pt]
\lambda^{(a)}_n(W^r_2,\mu,L_{\infty})_p &\asymp&\frac{\sqrt{\ln
n}}{n^{r+(s-1)/2}}, \qquad 0 < p < \infty.
\end{eqnarray*} 相似文献
There exists a set S with 3 elements such that if f is a non-constant entire function satisfying E(S,f)=E(S,f′), then f≡f′. The number 3 is best possible. The proof uses the theory of normal families in an essential way. 相似文献
