激光陀螺读出信号高速采集系统

介绍了激光陀螺（RLG）读出信号高速采集系统的设计和实现方案。该系统包括板卡和相应的应用软件,提供两路最高60MHz采样频率、14位精度的数据采集通道,能够同时对RLG两路光强拍频信号进行高速高精度数据采集,为RLG特性分析提供重要依据。该系统通过上位机软件控制板卡的工作状态、设置和切换采样模式。板卡利用FPGA接收计算机指令并协调控制模数转换器、SDRAM和USB接口芯片,完成RLG输出拍频信号的采集、缓存和传输。FP—GA设计中结合了硬件逻辑高速灵活的优点和NIOSⅡ软核处理器在控制方面的优势。SDRAM完成海量数据缓存,USB接口芯片工作在SlaveFIFO模式下,实现板卡与计算机的通信。实验证明该系统工作稳定,在RLG测试和性能分析中具有很好的实用性。     

三维超分子化合物(C20O2H14)(C12N2H8)的合成、晶体结构与荧光性质

合成了一个三维超分子化合物(C20O2H14)(C12N2H8)(命名为BP1),通过元素分析、红外光谱、核磁共振氢谱和X射线单晶衍射对其结构进行了表征,结果表明分子之间通过氢键和π-π堆积弱的相互作用形成超分子化合物。对所有合成的超分子化合物进行了紫外光谱和荧光光谱的测试。在室温DMSO溶液中,当激发波长为342 nm时,化合物在373 nm处有一强发射峰,呈现紫色荧光,这可以归属于分子内的π*→π跃迁。X射线单晶衍射分析结果表明,该超分子化合物属于三斜晶系,P1空间群,晶胞参数a=1.087 8(2)nm,b=1.125 2(2)nm,c=1.168 0(2)nm,α=97.89(3)°,β=110.91(3)°,γ=109.62(3)°,V=1.203 2(4)nm3,Z=2,R1=0.053 1,wR2=0.163 4,GOF值为1.034。     

Phenolic Components from Rhododendron latoucheae Part 5 in the series "Chemical Studies on Ericaceae Plants

Chemicalc0mponentsofthegenusRhododendronwithvariousbioactivities,suchasantitussiveandantitracheitishavebeenidentifiedbefore'.T0thebestofourkn0wledge,theplantRhododendronlatoucheaeFinetetFranchofthegenushasnotbeenstudiedchemicallyupt0n0w.Wehereinrep0rtthestructuraIelucidationoftw0newnaturalphen0licc0mpoundsnamed( )-rhodolat0uchollandisoepirh0d0dendrin4fromtheleavesofR.laloucheae.Besides,sixotherknownc0mpounds,( )-rh0d0dendr0l2,epirh0d0dendrin3.4-(3'-O-0-D-glucopyranosyl-4'-hy5,4-(4'-O-6-D-g…     

用多孔玻璃膜管悬浮聚合法制备单分散性聚苯乙烯微球

Monodisperse polystyrene microspheres are prepared by shell porous glass(SPG)-suspension polymerization. The influences of SPG on size and size dispersity of the microspheres are investigated. The properties of the microspheres are studied by GPC, TEM and SEM. The results indicate that the polystyrene microspheres possess definite monodispersibity and their particle size is in the range of 5～12μm.     

一种高效便捷的红外探测卡

我们利用稀土直接掺杂工艺 ,通过向带隙宽为 4～ 5ｅＶ的ⅡＡ ⅥＡ族化合物中掺入稀土离子Ｅｕ、Ｓｍ ,合成了电子俘获材料 (ＥＴＭ ＥｌｅｃｔｒｏｎＴｒａｐ ｐｉｎｇＭａｔｅｒｉａｌ)ＣａＳ :Ｅｕ ,Ｓｍ。该材料具有红外上转换和光存储特性 ,其红外响应光谱宽 ( 0 .8～ 1 .6μｍ)、量子转换效率高达 76% [1 ,2 ] 、热稳定性好、使用方便 (室温下工作 ,不需制冷 )、造价低 ,并且具有“常光充能”特性 ,即不需紫外线预激发就能在室温下将红外光 ( 0 .8～ 1 .6μｍ)直接转换为醒目的可见红光 ,是一种优良的红外探测材料 ,利用该材料制作的…     

Study on Fluorescence Property of Sparfloxacin Derivatizing System and its Application

Spartloxacin (SPFX) is the fourth generation of the antibacterial quinolones. Due to itsintensive and efficient antibacterial activity compared to the common quinolones '. it hasbeen widely used in clinical practice. Nevertheless. because of the structural dit'ferencesbetween SPFX and other quinolones. the fluorescence of SPFX is so weak that it can notbe determined by means of fluorescence spectra. Hence, it will be of great interest tomake a detailed study on its fluorescence enhancemen…     

百叶窗浓缩器气固两相流动的试验研究

本文在以往试验基础上对百叶窗浓缩器进行了更加深入的试验研究，分析了百叶窗结构、气流等因素对浓缩器性能，即浓淡风比、阻力系数、浓缩率三个参数的影响，从而得到了优化的百叶窗结构。     

毕竟正则半群上的同余及■(■)关系

探讨了毕竟正则半群上的(～Γ)(～R)等价关系.通过毕竟正则半群的同态像得到了一些信息,并且利用已知半群的性质及同态象的信息构造了一类半群.我们的结果推广了Edwards和Hall的相应结果.     

A Simple X-ray Spectrometer and PC-based Data Acquisition System for Newly Developed X-ray Source Based on Laser Compton Scattering

A simple X-ray spectrometer and a PC-Based Data Acquisition System(DAS) have been developed newly in Shanghai Institute of Applied Physics(SINAP),Chinese Academy of Sciences (CAS) for the measurement of the X-ray source generated using laser Compton scattering.The system consists of liquid nitrogen cooled high resolution Si(Li) detector,electronics and a DAQ.The Si(Li) detector was designed and made by Center of Advanced Instruments in SINAP,CAS,it allows us to measure X-rays with the energy up to 60 keV and the energy resolution(FWHM) of 184 eV at 5.9 keV.We measured the system uncertainty was 0.2 eV and time drifting of detector was 0.05% both at 5.9 keV.The DAQ was based on Object-Oriented software LabVIEW 7.1,it has data on-line analysis and original data saved functions.     

施用三乙膦酸铝后铝在黄瓜及叶片上的残留分析与评价

建立了湿法消解-石墨炉原子吸收光谱法测定黄瓜及其叶片上铝的背景含量及其施用三乙膦酸铝后铝的最终残留量. 方法线性范围为10～400 μg/L, r=0.991 6, 检出限为62.4 pg. 黄瓜中铝的添加回收率为92.1%～98.7%, RSD为4.8%～5.1%; 黄瓜叶片中铝的添加回收率为89.0%～100.1%, RSD为14%～18%, 方法的准确度和精密度均符合痕量分析要求. 结果表明, 施用三乙膦酸铝后黄瓜上铝的残留量低于参照的限量标准(＜100 mg/kg); 黄瓜叶片上的铝积累较明显, 与施药剂量和施药次数有一定的相关性.