Error Bounds for Hermite Interpolation by Quadratic Splines on an {alpha}-Triangulation

For l, an -triangulation F of a planar domain is such that,for every T F, there holds 1 R_T/2r_T , where R_T (resp. r_T)denotes the radius of the circumscribed (resp. inscribed) circleof the triangle T. When T is varying in F the centre of itsinscribed circle is varying in a compact interior to T and itsorthogonal projections on the sides are varying in compact intervalsinterior to these sides. Precise results are given about thesizes of these compacts and are used for the computation oferror constants in the problem of Hermite interpolation by Powell-Sabinquadratic finite elements, bringing to the fore their dependenceon the parameter .     

肉苁蓉精油化学成分的研究

肉苁蓉 Cistanche Salsa(C.A.Mey.)G.Beak 是列当科 Orobanchaceae 植物肉苁蓉的肉质茎;又名大芸,纵蓉。它分布在北疆地区荒漠戈壁地带,有益肾壮阳,延年益寿等功能,故有“沙漠人参”之称。肉苁蓉是一种常用的中药,新疆地区资源丰富,其精油化学成分在国内外未见报道。为了整理和发掘祖国医药学宝库,我们对其化学成分进行了研究。     

微波消解ICP-MS测定唐古特乌头中的多种微量元素

采用HNO3-H2O2混合酸体系微波消解及电感耦合等离子体-质谱法,消解唐古特乌头样品,测定其中Mn、Fe、Co、As、Ni、Se、Cu、Zn、V和Cr共10种微量元素。探讨了样品消解的条件,通过加标回收实验,回收率为94.08%—103.50%,验证了分析数据的可靠性。结果表明,该法具有快速、简便、准确度高、能同时分析多元素的优点,结果令人满意。     

Dynamic analysis of on-line high-performance liquid chromatography for multivariate statistical process control

A continuous process was studied over 83.32 h using on-line high-performance liquid chromatography, involving the acquisition of 252 chromatograms. A method for analysis of these data using multivariate statistical process control on peak tables, in real-time, is described. The normal operating condition (NOC) region of the process was identified using evolving principal components analysis to be between 5.77 and 8.13 h. 19 out of the 37 peaks detected throughout the process were found in the NOC region, the remainder representing undesirable contaminants found elsewhere in the process. A major challenge is to develop the peak table as the process evolves, which is dynamically updated as new peaks are detected after the NOC region: this approach involving an "unlocked" peak table is contrasted to an approach using a "locked" peak table where only peaks detected during the NOC region are included in the model. In addition, results are compared to those obtained using baseline corrected and aligned chromatograms, using a NOC region of 5.85-8.33h. D- and Q-charts were obtained. It is shown that the "unlocked" peak table detects out of control samples best and provides good diagnostic insight into problems with the process.