镍钛记忆合金自补偿磨粒磨损性能研究

研究了高临界温度镍钛记忆合金一维自补偿磨粒磨损特性.结果表明,在一定温度下,镍钛记忆合金在摩擦过程中具有形状恢复能力,从而产生一维磨损自补偿作用.超弹状态镍钛记忆合金具有热弹性马氏体相变、高阻尼、应力感生马氏体、超弹性、高应变硬化指数和时效弥散析出强化等特性,这使得硬度较低的镍钛合金的耐磨性能远优于硬度较高的淬火45#钢.利用超弹状态镍钛记忆合金的磨损自补偿作用可望开发出新型抗磨形状记忆合金产品.     

中心裂纹圆盘应力强度因子的测试误差分析

本文在中心裂纹圆盘应力强度因子解析解的基础上,利用一阶微分法则,给出了与裂纹相对长度和加载角相关的应力强度因子(K 和K )的4个误差传递函数。这4个误差传递函数关于裂纹相对长度和加载角均是非线性的,它们既是误差分析的基础,又是合理确定裂纹相对长度和加载角的基础。分析结果表明,加载角的误差Δθ除了对纯 型K 的误差几乎没有影响,对纯 型K 影响较小外,对复合型K 、K 的误差均有较大影响。最后,本文建议裂纹相对长度的取值范围为0.4～0.6;还建议在复合型断裂试验时,必须依据对K 、K 的总体精度要求来严格控制加载角的精度。     

New conversion of Friendlnder reaction of 3-amino-1H-benzo[f]chromene-2-carbonitriles with cyclohexanone

Two different skeletons of heterocyclic compounds,quinoline and quinazolinone analogs could be obtained by a novel one-pot synthesis from substituted 3-amino-1 H-benzo[f]chromene-2-carbonitrile derivatives and cyclohexanone in DMF in the catalyst of anhydrous zinc chloride under reflux.A plausible mechanism was proposed.     

Nanocatalytic resonance scattering spectral analysis

The resonance scattering spectral technique has been established using the synchronous scanning technique on spectrofluorometry.Because of its advantages of simplicity,rapidity and sensitivity,it has been widely applied to analyses of proteins,nucleic acids and inorganic ions.This paper summarizes the application of immunonanogold and aptamer modified nanogold(AptAu) catalytic resonance scattering spectral technique in combination with the work of our group,citing 53 references.     

Isolation and Purification of Unstable Iridoid Glucosides from Traditional Chinese Medicine by Preparative High Performance Liquid Chromatography Coupled with Solid-phase Extraction

An efficient preparative method was successfully developed for isolation and purification of unstable components from medicinal plant extracts, using a combined method of preparative high performance liquid chro-matography(HPLC) and solid-phase extraction(SPE). The aim of this study was to obtain an effective method with high preparative efficiency and importantly to avoid the transformation of unstable compounds. The preparative HPLC system was based on an LC/MS controlled four-channel autopurification sys...     

颗粒流的动力学模型和实验研究进展

首先叙述了颗粒流研究的背景和基本概念,接着概述了颗粒流动力学研究的三种基本数学力学模型:颗粒动理论(kinetic theory)模型、摩擦塑性模型和离散元模拟模型.介绍了它们的基本原理,并分析了各个模型的优缺点和适用范围.随之,对颗粒流的实验研究情况作了简要的介绍,列举了研究中几种常用的试验方法和观测手段,以及观测到的一些典型现象.最后,我们简述了颗粒流研究的主要困难,并提出了某些有待解决的研究课题.      

固体力学中侵入问题的若干新进展

本文主要介绍了固体力学中侵入问题近10余年来的发展情况。重点综述了侵入断裂实验及理论研究的新成果;讨论了动静态侵入断裂的关系;简述了侵入方法在测定材料断裂韧性方面的应用。      

基于增广Lagrange函数的RQP方法

Recursive quadratic programming is a family of techniques developd by Bartholomew-Biggs and other authors for solving nonlinear programming problems.This paperdescribes a new method for constrained optimization which obtains its search di-rections from a quadratic programming subproblem based on the well-known aug-mented Lagrangian function.It avoids the penalty parameter to tend to infinity.We employ the Fletcher‘s exact penalty function as a merit function and the use of an approximate directional derivative of the function that avoids the need toevaluate the second order derivatives of the problem functions.We prove that thealgorithm possesses global and superlinear convergence properties.At the sametime, numerical results are reported.     

A large deviation for occupation time of critical branching α-stable process

In this paper we establish a large deviation principle for the occupation times of critical branching α-stable processes for large dimensions d > 2α, by investigating two related nonlinear differential equations. Our result is an extension of Cox and Griffeath’s (in 1985) for branching Brownian motion for d > 4.     

Lukasiewicz n值命题逻辑中命题的真度理论

利用势为 n的均匀概率空间的无穷乘积在 Lukasiewicz n值命题逻辑中引入了公式的真度概念,当3≤n≤17时证明了全体公式的真度值之集在[0,1]上是稠密的,并给出了公式真度的表达通式;利用真度定义了公式间的相似度,进而导出了全体公式集上的一种伪距离,为n值Lukasiewicz命题逻辑系统的近似推理理论提供了一种可能的框架。