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Wolfgang Jeitschko Joerg H. Albering Reinhold Brink Ursula Jakubowski‐Ripke Elke J. Reinbold 《ChemInform》2015,46(1):no-no
The new ternary phosphides ScFe5P3 (I), Sc(Ta0.18Fe0.82)Fe4P3 (II), ZrFe5P3 (III), ScRu6P4 (IV), ErRu6P4 (V), ZrCr6P4 (VI), Nd2Ru12P7 (VII), and U2Mo30P19 (VIII) are prepared from mixtures of the elements in most cases with elemental Sn as a flux (alumina crucibles, 650—950 °C, 7—10 d). 相似文献
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Jan H. Overbeck Jennifer Vögele Felix Nussbaumer Elke Duchardt-Ferner Christoph Kreutz Jens Wöhnert Remco Sprangers 《Angewandte Chemie (International ed. in English)》2023,62(23):e202218064
The synthetic neomycin-sensing riboswitch interacts with its cognate ligand neomycin as well as with the related antibiotics ribostamycin and paromomycin. Binding of these aminoglycosides induces a very similar ground state structure in the RNA, however, only neomycin can efficiently repress translation initiation. The molecular origin of these differences has been traced back to differences in the dynamics of the ligand:riboswitch complexes. Here, we combine five complementary fluorine based NMR methods to accurately quantify seconds to microseconds dynamics in the three riboswitch complexes. Our data reveal complex exchange processes with up to four structurally different states. We interpret our findings in a model that shows an interplay between different chemical groups in the antibiotics and specific bases in the riboswitch. More generally, our data underscore the potential of 19F NMR methods to characterize complex exchange processes with multiple excited states. 相似文献
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Dr. Elke Duchardt-Ferner Dr. Jan Ferner Dr. Boris Fürtig Dr. Martin Hengesbach Dr. Christian Richter Dr. Andreas Schlundt Dr. Sridhar Sreeramulu Dr. Anna Wacker Prof. Dr. Julia E. Weigand Dr. Julia Wirmer-Bartoschek Prof. Dr. Harald Schwalbe 《Angewandte Chemie (International ed. in English)》2023,62(14):e202217171
The outbreak of COVID-19 in December 2019 required the formation of international consortia for a coordinated scientific effort to understand and combat the virus. In this Viewpoint Article, we discuss how the NMR community has gathered to investigate the genome and proteome of SARS-CoV-2 and tested them for binding to low-molecular-weight binders. External factors including extended lockdowns due to the global pandemic character of the viral infection triggered the transition from locally focused collaborative research conducted within individual research groups to digital exchange formats for immediate discussion of unpublished results and data analysis, sample sharing, and coordinated research between more than 50 groups from 18 countries simultaneously. We discuss key lessons that might pertain after the end of the pandemic and challenges that we need to address. 相似文献
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