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61.
Two methods for multi-element preconcentration from copper by reductive matrix precipitation are presented. In systematic investigations on the coprecipitation behaviour of Ag, Al, Au, Bi, Cd, Co, Cr, Fe, Ga, In, Mn, Mo, NJ, Pb, Sb, Se, Sn, Te and Zn during precipitation of the copper matrix as Cu2O or CuSCN, the separation parameters were optimized. By combination with a hexamethyleneammonium hexamethylenedithiocarbamate collector precipitation, a concentration of 8 elements (Cu2O precipitation) or 13 elements (CuSCN precipitation) in a small volume was achieved. The limits of detection of the procedures are, depending on the element, 0.1–5 μg g?1 for flame atomic absorption spectrometry (AAS) and 0.01–0.1 μg g?1 for graphite furnace AAS. The relative standard deviations are about 3%. The analytical performance of the procedures is compared with that of an electrolytic copper separation. 相似文献
62.
D. A. Tikhomirov O. S. Slyadevskaya A. V. Eremeev 《Chemistry of Heterocyclic Compounds》1991,27(9):966-969
A convenient method of synthesis of 2-(methoxycarbonylmethylene)-substituted imidazolidines and imidazolidinium bromides, and also of bicyclic diazo compounds has been developed starting from methyl bromopropiolate and ethylenediamine and its derivatives.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 9, pp. 1205–1208, September, 1991. 相似文献
63.
E. V. Zakharov A. G. Davydov Yu. V. Pimenov G. M. Tikhonov 《Computational Mathematics and Modeling》1991,2(1):79-84
Translated from Chislennye Metody Resheniya Obratnykh Zadach Matematicheskoi Fiziki, pp. 119–127. 相似文献
64.
I. L. Davies K. E. Markides M. L. Lee M. W. Raynor K. D. Bartle 《Journal of separation science》1989,12(4):193-207
Although coupled liquid chromatographygas chromatography (LC-GC) was first demonstrated ten years ago, only in the last few years has there been a sudden surge of interest in the technique. Approximately 70% of the total number of LC-GC applications have been published in the last two years (1987–88) alone. This review categorizes LC-GC publications into four main application areas: fossil fuels, foods, environmental samples, biologiical/pharmaceutical samples, and miscellaneous samples. Multidimensional separations carried out using other coupled-column chromatographic techniques (such as supercritical fluid chromatography (SFC) with GC, and on-line trace enrichment-GC) have also been included in this review. 相似文献
65.
E. Dror Farjoun 《Israel Journal of Mathematics》1989,66(1-3):132-142
Using a new group of singular chains on polyhedra, a transfer map is defined on the chain level for fibrations with singularities.
These include usual transfer on homology as well as Oliver transfer and other cases. 相似文献
66.
67.
Palle E. T. Jorgensen 《Mathematische Zeitschrift》1989,201(4):455-476
Work supported in part by the NSF 相似文献
68.
A firm's logistics cost, including shipping and inventory-carrying, is a substantial percentage of its sales. Nevertheless, typical inventory-control methods ignore or insufficiently represent the shipping cost. This paper describes a recursive algorithm that determines the reorder cycle-time that minimizes total logistics cost. It allows for a realistic accounting of shipping cost, which is modelled here as a function of shipping distance and weight. The algorithm uses a relaxation procedure to identify a suitable initial approximation to the optimal order cycle-time and then, through a series of recursive steps, moves to the optimal result. We demonstrate the algorithm with a single item, with a group of items that share a common order cycle, and with multi-items when item demands are random variables. Experience with this algorithm indicates that it converges to the optimal result in a very few steps. 相似文献
69.
70.
José E. Valdés 《Operations Research Letters》2006,34(1):49-52
Components C1 and C2 form a series system. Suppose we can allocate the spare R1 in parallel with C1 and the spare R2 in parallel with C2, or otherwise, allocate R1 with C2 and R2 with C1. In this paper, we compare these two options using hazard rate ordering. 相似文献