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991.
Z. A. Samoilenko V. D. Okunev E. I. Pushenko T. A. D’yachenko A. Cherenkov P. Gierlowski S. J. Lewandowski A. Abal’oshev A. Klimov A. Szewczyk 《Technical Physics》2003,48(2):250-256
Crystallographic phase transitions in perovskite-like LaSrMnO metallic oxides are studied. The transitions are induced when
internal stresses generated during film synthesis (at temperatures between 450 and 730°C) vary (decrease or increase) upon
subsequent irradiation by a KrF laser emitting in the UV range. As the synthesis temperature T
s grows, the rhombohedral-to-orthorhombic phase transition occurs at 650–670°C. The resistivity is shown to be either temperature-independent,
ρ(T)=const, at T<T
crit, or varies and reaches a maximum, ρ(T)=ρmax, at the Curie temperature T
c. Optical transmission spectra taken at photon energies ℏω=0.5–2.5 eV exhibit both a high (0.8–0.9) and low (0.1–0.3) transmission
coefficient t, depending on the synthesis temperature. As follows from X-ray diffraction data, the laser irradiation causes a phase transition
only in LaSrMnO films grown at T
s<650°C. Phases of different size scales appear: the long-range-order orthorhombic matrix and mesoscopic-range-order rhombohedral
clusters are observed in the films grown at T
s=450–550°C and the rhombohedral matrix with orthorhombic clusters, in the films grown at T
s=550–650°C. 相似文献
992.
P. Mun F. C. Fonseca R. Muccillo R. F. Jardim 《Physica C: Superconductivity and its Applications》2003,390(4):363-373
A systematic study of the magnetic hysteresis in transport properties of polycrystalline YBa2Cu3O7−δ–Ag compounds has been made based on two kinds of measurements at 77 K and under applied magnetic fields up to 30 mT: critical current density Jc(Ba) and magnetoresistance R(Ba). The R(Ba) curves show a minimum in their decreasing branch occurring at B=Bmin which was found to be both the excitation current Iex and the maximum applied magnetic field Bam dependent. In addition, for a certain value of Bam>5 mT, we have observed that Bmin increases with increasing Iex and reaches a saturation value. The Jc(Ba) curves show a maximum in decreasing applied magnetic fields occurring at B=Bmax. We have also found that Bmax increases with increasing Bam and reaches a saturation value. The minimum in the R(Ba) and the maximum in Jc(Ba) curves were found to be related to the trapped flux within the grains. All the experimental results are discussed within the context of the flux dynamics and transport mechanisms in these high-Tc materials. 相似文献
993.
The N-carboethoxy precursor to (±)-tecomanine has been prepared in 11 steps from 2-methyl-1-buten-3-yne. The key step, Pauson-Khand cyclization of a methylated 5-aza-6-nonen-1-yne succeeds, but only in low yield, a consequence of the dialkyl substitution about the azaenyne framework. Nevertheless, the overall sequence to that point is one of the more efficient to be described. 相似文献
994.
The known plant growth regulator, Al'den [1-(3,7-dimethyloctyl)-1-allylpiperidinium bromide], and also 1-(3,7-dimethyloctyl)-1-methylpiperidinium iodide were synthesized by treatment with allyl bromide and methyl iodide, respectively, of exhaustively hydrogenated 1-nerylpiperidine which was obtained by anionic telomerization of isoprene with piperidine. Various quaternary ammonium salts having a terpene sub- stituent with unnatural dimethyloctane skeleton, which effectively stimulate florification of Aster Chinensis L., were prepared by the action of alkyl halides on telomerization products derived from isoprene and piperidine or morpholine in the presence of palladium complexes. 相似文献
995.
Komarov A. V. Yakovlev I. P. Novikov D. V. Semakova T. L. Zakhs V. E. 《Russian Journal of General Chemistry》2003,73(11):1806-1809
Methylmalonyl dichloride reacts with (2E)-3-phenylacrylamides and (2E)-3-(2-furyl)acrylamide to give the corresponding E-isomeric 2-substituted 4-hydroxy-5-methyl-6H-1,3-oxazin-6-ones. The reaction of methylmalonyl dichloride with acrylamide afforded N-(3-chloropropionyl)-2-methylmalonamic acid. The structure of the products was confirmed by the 1H and 13C NMR, IR, and UV spectra. 相似文献
996.
M. I. Kurkin V. V. Leskovets V. V. Nikolaev E. A. Turov L. V. Turov 《Physics of the Solid State》2003,45(4):685-690
The possibility of excitation of NMR signals by an ac electric field in magnetically ordered crystals is discussed. Such signals can be recorded using the time-dependent component of the electric polarization vector. It is assumed that the electric and magnetic characteristics are coupled to each other through magnetoelectric and antiferroelectric interactions. Several types of magnetic structures are analyzed in which these interactions are not forbidden by symmetry. Such structures include two-sublattice single-position ferro-and antiferromagnetic phases in centrosymmetrical crystals, two-sublattice magnetic crystals without a center of symmetry (such as KNiPO4), and four-sublattice antiferromagnetic crystals with three types of antiferromagnetism vectors (such as Cr2O3 and α-Fe2O3). 相似文献
997.
998.
S. S. Andreev A. D. Akhsakhalyan M. A. Bibishkin N. I. Chkhalo S. V. Gaponov S. A. Gusev E. B. Kluenkov K. A. Prokhorov N. N. Salashchenko F. Schafers S. Yu. Zuev 《Central European Journal of Physics》2003,1(1):191-209
We present research investigations in the field of multilayer optics in X-ray and extreme ultra-violet ranges (XUV), aimed
at the development of optical elements for applications in experiments in physics and in scientific instrumentation. We discuss
normal incidence multilayer optics in the spectral region of “water window”, multilayer optics for collimation and focusing
of hard X-ray, multilayer dispersing elements for X-ray spectroscopy of high-temperature plasma, multilayer dispersing elements
for analysis of low Z-elements. Our research pays special attention to optimization of multilayer optics for projection EUV-lithography
(ψ-13nm) and short period multilayer optics. 相似文献
999.
F. Forkusuz S. Işıklı S. Akın M. Ungan A. Şenköylü N. K. Aras 《Journal of Radioanalytical and Nuclear Chemistry》2004,259(3):365-368
The standard method to diagnose and follow-up osteoporosis is the measurement of bone mineral density (BMD) using dual X-ray
absorptiometry (DEXA). Manufacturers' manuals of DEXA devices state the intrascanner coefficient of variance is less than
0.01 g/cm2. The aim of this study was to evaluate the in vivo coefficient of variance of a Lunar DPX scanner in male and female healthy
adult subjects. Average BMD for females and males were 1.170±0.091 g/cm2 and 1.272±0.115 g/cm2, respectively. Monthly phantom measurements provided and controlled by the manufacturer were 1.243±0.008 g/cm2 (range 1.222 to 1.257) and the coefficient of variance was 0.006. It is concluded that the in vivo coefficient of variance
of DEXA devices can slightly be higher than that proposed by the manufacturer.
This revised version was published online in August 2006 with corrections to the Cover Date. 相似文献
1000.
We give an account of the appearance and first developments of the statistical model of atoms proposed by Thomas and Fermi, focusing on the main results achieved by Fermi and his group in Rome. Particular attention is addressed to the unknown contribution to this subject by Majorana, anticipating some important results reached later by leading physicists. 相似文献