石墨炉原子吸收光谱法直接测定城市污泥中有机态镉

建立了真空冷冻干燥法制备有机相标准系列,氯化钯-磷酸氢二钾作基体改进剂,分步斜坡升温石墨炉原子吸收光谱法直接测定城市污泥中痕量有机态Cd的方法,有效地消除了基体干扰.方法的精密度(RSD,n=11)为5.7%,用于污泥样品的测定加标回收率在91%-107%之间,与常规消解法测定值比较结果令人满意.     

Synthesis of 1-indanones by intramolecular Friedel-Crafts reaction of 3-arylpropionic acids catalyzed by Tb(OTf)3

Intramolecular Friedel-Crafts acylation reaction of 3-arylpropionic acids was efficiently catalyzed by Tb(OTf)₃ at 250 °C to give 1-indanones. Even deactivated 3-arylpropionic acids with halogen atoms on the aromatic ring can be cyclized in moderation to good yields.     

一维光晶格中玻色凝聚气体的干涉

对捕限在三维轴对称谐振势阱叠加一维光晶格的组合势中的玻色凝聚气体，文章基于平均场G-P方程并运用传播子方法，求解玻色凝聚气体基态波函数及其随时间的演化，给出了物质波干涉图样的空间分布与光晶格势周期结构之间的关系.研究表明，运用这一方法得到的光晶格势中物质波干涉条纹与光学中的多光束干涉相类似，并且与Andrews 和Peil等人的实验结果一致.物质波干涉图样随时间的演化也与Sadhan K. Adhikari通过直接数值求解G-P方程所得结果基本相同. 关键词： 玻色凝聚气体 子凝聚原子云 光晶格势 干涉     

Intrinsic Decoherence on Two-Qubit Heisenberg XX Chain

Quantum teleportation is investigated by using the entangled states of two-qubit Heisenberg XX chain in an external uniform magnetic field as resources in the model of Milburn＇s intrinsic decoherence. Though intrinsic decoherence on quantum entanglement and quantum teleportation exerts different effects in different initial systems, proper magnetic fields and probabilities of different eigenstates in the initial states can weaken the effects.     

Electron Transport Property of CdTe under High Pressure and Moderate Temperature by In-Situ Resistivity Measurement in Diamond Anvil Cell

In situ resistivity measurement has been performed to investigate the electron transport property of powered CdTe under high pressure and moderate temperature in a designed diamond anvil cell. Several abnormal resistivity changes can be found at room temperature when the pressure increases from ambient to 33 GPa. The abnormal resistivity changes at about 3.8 GPa and 10 GPa are caused by the structural phase transitions to the rock-salt phase and to the Cmcm phase, respectively. The other abnormal resistivity changes at about 6.5 GPa, 15.5 GPa, 22.2 GPa and about 30 GPa never observed before are due to the electronic phase transitions of CdTe. The origin of the abnormal change occurred at about 6.5 GPa is discussed. The temperature dependence of the resistivity of CdTe shows its semiconducting behaviour at least before 11.3 GPa.     

Evolution of Matter Wave Interference of Bose-Condensed Gas in a 1D Optical Lattice

For a Bose-condensed gas in a combined potential consisting of an axially-symmetric harmonic magnetic trap and one-dimensional （1D） optical lattice, using the mean-field Gross-Pitaevskii （G-P） equation and the propagator method, we obtain the analytical result of the order parameter for matter wave interference at any time. The evolution of the interference pattern under a variation of the relative phase △Ф between successive subcondensates trapped on an optical lattices is also studied. For △Ф=π, the interference pattern is symmetric with two sharp peaks, which are symmetrically located on a straight line on both sides of a vacant central peak and moving apart from each other. This work is in agreement with available experimental results.     

Structural Transition of Gd2O3：Eu Induced by High Pressure

The structural transition of bulk and uano-size Gd2O3：Eu are studied by high pressure energy disperse x-ray diffraction （XRD） and high pressure photoluminescence. Our results show that in spite of different size of Gd2O3 particles, the cubic structure turns into a possible hexagonal one above 13.4 GPa. When the pressure is released, the sample reverses to the monoclinic structure. No cubic structure presents in the released samples. That is to say, the compression and relaxation of the sample leads to the cubic Gd2O3：Eu then turns into the monoclinic one.     

纯相位液晶空间光调制器拟合泽尼克像差性能分析

纯相位液晶空间光调制器作为波前校正器构成的高分辨率、低能耗、价格低廉、易于控制的自适应光学系统受到越来越多的关注.作为一种新型波前校正器件，它对波前像差的校正能力是反映其在自适应光学系统中应用的一个重要的指标，因此有必要仔细地研究它对各种像差的校正能力，以确定其可能的应用范围.波前校正器对各阶泽尼克像差的拟合效果有效地反映了该器件对不同像差的校正能力.利用256×256像素的纯相位液晶空间光调制器(LC-SLM)产生不同系数的前36项泽尼克像差分析LC-SLM对不同像差的校正能力.讨论了填充因子、离散像素     

紫外光固化光纤油墨对着色光纤光衰减的影响

紫外光固化油墨;聚丙烯酸酯;着色纤维;紫外光固化光纤油墨对着色光纤光衰减的影响