Functionalization and Dispersion of Hexagonal Boron Nitride (h‐BN) Nanosheets Treated with Inorganic Reagents

A mixture of bulk hexagonal boron nitride (h‐BN) with hydrazine, 30 % H₂O₂, HNO₃/H₂SO₄, or oleum was heated in an autoclave at 100 °C to produce functionalized h‐BN. The product formed stable colloid solutions in water (0.26–0.32 g L ^?1) and N,N‐dimethylformamide (0.34–0.52 g L ^?1) upon mild ultrasonication. The yield of “soluble” h‐BN reached about 70 wt %. The dispersions contained few‐layered h‐BN nanosheets with lateral dimensions in the order of several hundred nanometers. The functionalized dispersible h‐BN was characterized by IR spectroscopy, X‐ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis spectroscopy, X‐ray diffraction (XRD), dynamic light scattering (DLS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and atomic force microscopy (AFM). It is shown that h‐BN preserves its hexagonal structure throughout the functionalization procedure. Its exfoliation into thin platelets upon contact with solvents is probably owing to the attachment of hydrophilic functionalities.     

??????????????????о????

综述了连续介质方法在碳纳米管研究中的最新进展. 主要叙述梁、壳模型, 膜模型,多尺度方法,分子结构力学方法,非局部连续介质方法,以及无网格法的基本原理、 基本方法,及其最新进展,指出其局限性,并预测连续介质方法在碳纳米管研究的发展趋势 和方向.     

Measurement of the Temperature Dependence of the ddμ-Molecule Formation Rate in Dense Deuterium at Temperatures 300–800 K

Muon catalyzed fusion in deuterium was studied by the MCF collaboration at JINR phasotron. The measurements were carried out with a high-pressure deuterium target at the JINR phasotron in the temperature range 300–800 K at densities ≃0.5 LHD. The first experimental results for ddμ-molecule formation rate λ _ddμ in the temperature range 400–800 K with deuterium density 0.5 LHD are presented. This revised version was published online in August 2006 with corrections to the Cover Date.     

Evaluation of the effectiveness of demonstration experiment

The results of the use of sensors in the demonstration of chemical experiment were described. In spite of some complication of the equipment, the effectiveness of the demonstration experiment was shown to be high while using sensors.     

An increase in entropy at separation cascade nodes and separation work loss

The pressure of combined fractions and total entropy changes at pyramidal cascade nodes were estimated for the general case of processing of a binary mixture with an arbitrary composition. The difference between the work of separation determined using the Dirac-Peierls potential and the thermodynamically estimated work of mixing of products obtained was shown to be a consequence of an increase in entropy caused by combining fractions at cascade nodes.     

大连广电中心广播电视剧场声学设计

广播电视剧场是随着电视技术的发展和需要而产生的一种新的观演建筑的形式，它不同于一般的演播室，也有别于普通的剧场。它不仅要求能够进行电视节目的转播和录制，还要求能够进行音乐、歌舞等各种文艺节目的演出，并能够举行会议和放映立体声电影，因此，广播电视剧场对音质有很高的要求。本文介绍了大连广播电视中心广播电视剧场的建声设计，在该剧场内采用了计算机控制的可调混响装置，使得各种使用功能都能有一个较为理想的建声环境。     

Computer-aided designing of simple electron-optical systems for electron image tubes

We consider the possibility of designing time-analyzing electron-optical systems for electron image tubes with subpicosecond resolution, containing no spherical electrodes, fine-structure grids, or narrow slots (i.e., extremely simple systems with high spatial and temporal resolutions).     

共轭聚合物发光二极管

链状共轭聚合物的带隙能与可见光能相当，在一定条件下具有特殊的颜色，可用于多色显示元件。本文评述和介绍了近年来关于用共轭聚合物制作发光二极管的原理、方法和性能的关系及应用前景。     

1,3-Dipolar cycloaddition of diphenylnitrilimine and 5-arylmethylidene-1-phenyl-1,5,6,7-tetrahydro-4H-indazol-4-ones to afford novel spiro[indazole-5,3′-pyrazole] derivatives

Chemistry of Heterocyclic Compounds - Novel 4'-aryl-1,2',5'-triphenyl-2',4',6,7-tetrahydrospiro[indazole-5,3'-pyrazol]-4(1H)-ones have been synthesized in moderate yields by...