荞麦花多糖的提取及含量测定

采用热水提取、乙醇沉淀的方法从荞麦花中提取出了水溶性多糖,采用硫酸-苯酚法在波长为497nm处进行了糖含量的测定,求得其校准曲线的回归方程为y=0.00508x 0.0294,相关系数为r=0.9978.平均回收率为99%-103%,RSD为0.74%.结果显示:荞麦花多糖的产率为2.5%.糖含量为41.63%.     

离子交换色谱法分离测定磷霉素的研究

分别采用全多孔型硅胶基键合强阴离子交换柱与氨丙基键合硅胶柱,在低波长 ２００ ｎｍ 处检测,分离测定了磷霉素 探讨了流动相条件,如ｐ Ｈ 值、离子强度等对磷霉素保留及分离选择性的影响,优化分离条件,建立了一种测定磷霉素的高效液相色谱新方法方法简便、快速     

交通流非参数回归模型

交通流宏观参数流量、速度和占有率在交通工程和管理中具有非常重要的作用 ,对这三者关系的刻划反映了道路本身特性和交通流的规律。到目前为止 ,基本上采用线性或非线性的参数模型来描述 ,此类模型在应用中具有一定的局限性 ,并交通变量时间序列进行预测 ,数据拟合表明 ,选择适当的核函数或邻近数以及窗宽 ,可以达到比较满意的效果     

A bivariate exponential distribution arising in random geometry

Summary In this paper a new bivariate exponential distribution, arising naturally in the theory of Poisson line processes, is studied. The distribution has some interesting and useful properties which renders it suitable for use in statistical modelling work. It is presented in the spirit of adding to the repertoire of bivariate exponential forms. It joins other models, such as those of Downton (1970,J. R. Statist. Soc., B,32, 408–417), Marshall and Olkin (1967,J. Appl. Prob.,4, 291–302) and Nagao and Kadoya (1971,Bulletin of the Disaster Prevention Research Institute,20, 3, 183–215), which have their origins in the theory of stochastic processes.     

An extension of Tanner's results on uncontrolled intersections

A delay formula is developed for the problem, analyzed by Tanner in 1962, where two streams of traffic have conflicting demands at an intersection. The situation is such that the major stream has absolute priority and the minor stream vehicles can only enter the intersection when sufficiently large gaps appear in the major stream. This paper extends Tanner's work by considering a generalised stochastic structure on the arrival streams. The paper also links Tanner's work to other papers of this author where the utilitarian value of this generalised model has been established in a wide range of traffic problems.     

Asymptotic formulae for likelihood-based tests of new physics

We describe likelihood-based statistical tests for use in high energy physics for the discovery of new phenomena and for construction of confidence intervals on model parameters. We focus on the properties of the test procedures that allow one to account for systematic uncertainties. Explicit formulae for the asymptotic distributions of test statistics are derived using results of Wilks and Wald. We motivate and justify the use of a representative data set, called the “Asimov data set”, which provides a simple method to obtain the median experimental sensitivity of a search or measurement as well as fluctuations about this expectation.