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21.
Crystal Structure of the Zinc Amide Zn[N(SiMe3)2]2 X‐ray quality crystals of Zn[N(SiMe3)2]2 (monoclinic, P21/c) are obtained by sublimation of the zinc amide Zn[N(SiMe3)2]2 at —30 °C in vacuo (300 torr). According to the result of the X‐ray structural analysis, Zn[N(SiMe3)2]2 contains an almost linear N‐Zn‐N unit with two short N‐Zn bonds. 相似文献
22.
23.
O. Dumbrajs M. Thumm J. Pretterebner D. Wagner 《International Journal of Infrared and Millimeter Waves》1992,13(6):825-840
Mode conversion at discontinuities of an ordinary gyrotron cavity is examined. It is shown how the production of unwanted spurious modes can be reduced substantially by introducing smooth transition regions between the individual parts of the cavity. The cavity of the 140 GHz KfK gyrotron operating in the TE10,4 mode is used as an example. Cavity and adjacent tapered output waveguide are optimized as a single unit. 相似文献
24.
An improved method including extraction procedures is presented for the analysis of nucleotides in suspension-cultivated animal cells. Quantification was performed by ion-pair high-performance liquid chromatography after perchloric acid extraction. It was found that the amount of perchloric acid taken for extraction influenced the yield and that cell washing procedures caused deterioration of the analysis results for triphosphates. More than thirty nucleotides and sugar-nucleotides were separated within 25 min using a Supelcosil reversed-phase column (3 microns) with tetrabutylammonium hydrogensulphate as pairing agent and methanol-pH gradient elution. Cultivated hybridoma cells showed variations in intracellular nucleotide concentrations as well as relative amounts during different growth phases, which could reflect the physiological state of a cell culture. 相似文献
25.
Hyperfine Interactions - The YFe4Al8 and ErFe4Al8 intermetallics were studied by57Fe Mössbauer spectroscopy between 2 K and room temperature. The spectra are consistent with iron occupying 8f... 相似文献
26.
Conrad Plaut 《Topology and its Applications》2006,153(14):2430-2444
This paper develops the basic theory of quotients of uniform spaces via sufficiently nice group actions. We generalize and unify two fundamental constructions: quotients of topological groups via closed normal subgroups and quotients of metric spaces via actions by isometries. Basic results about inverse limits of topological groups are extended to inverse limits of group actions on uniform spaces, and notions of prodiscrete action and generalized covering map are introduced. 相似文献
27.
Preparation and mechanical properties of layers made of recombinant spider silk proteins and silk from silk worm 总被引:1,自引:0,他引:1
F. Junghans M. Morawietz U. Conrad T. Scheibel A. Heilmann U. Spohn 《Applied Physics A: Materials Science & Processing》2006,82(2):253-260
Layers of recombinant spider silks and native silks from silk worms were prepared by spin-coating and casting of various solutions.
FT-IR spectra were recorded to investigate the influence of the different mechanical stress occurring during the preparation
of the silk layers. The solubility of the recombinant spider silk proteins SO1-ELP, C16, AQ24NR3, and of the silk fibroin
from Bombyx mori were investigated in hexafluorisopropanol, ionic liquids and concentrated salt solutions. The morphology and thickness of
the layers were determined by Atomic Force Microscopy (AFM) or with a profilometer. The mechanical behaviour was investigated
by acoustic impedance analysis by using a quartz crystal microbalance (QCMB) as well as by microindentation.
The density of silk layers (d<300 nm) was determined based on AFM and QCMB measurements. At silk layers thicker than 300 nm
significant changes of the half-band-half width can be correlated with increasing energy dissipation. Microhardness measurements
demonstrate that recombinant spider silk and sericine-free Bombyx mori silk layers achieve higher elastic penetration modules EEP and Martens hardness values HM than those of polyethylenterephthalate (PET) and polyetherimide (PEI) foils. 相似文献
28.
Kaon production is studied within the Giessen Boltzmann–Uehling–Uhlenbeck (GiBUU) model. Results are compared with experiment and with other models. The influence of the kaon potential on the kaon azimuthal distributions at SIS energies is considered. We also discuss the role of the many-body collisions at high-density phase of reaction. 相似文献
29.
Ivan Nunes da Silva Wagner Caradori do AmaralLucia Valeria de Arruda 《Applied Mathematical Modelling》2007
This paper presents an efficient approach based on recurrent neural network for solving nonlinear optimization. More specifically, a modified Hopfield network is developed and its internal parameters are computed using the valid subspace technique. These parameters guarantee the convergence of the network to the equilibrium points that represent an optimal feasible solution. The main advantage of the developed network is that it treats optimization and constraint terms in different stages with no interference with each other. Moreover, the proposed approach does not require specification of penalty and weighting parameters for its initialization. A study of the modified Hopfield model is also developed to analyze its stability and convergence. Simulation results are provided to demonstrate the performance of the proposed neural network. 相似文献
30.
Greg Gillen Albert Fahey Matt Wagner Christine Mahoney 《Applied Surface Science》2006,252(19):6537-6541
Thin monolayer and bilayer films of spin cast poly(methyl methacrylate) (PMMA), poly(2-hydroxyethyl methacrylate) (PHEMA), poly(lactic) acid (PLA) and PLA doped with several pharmaceuticals have been analyzed by dynamic SIMS using SF5+ polyatomic primary ion bombardment. Each of these systems exhibited minimal primary beam-induced degradation under cluster ion bombardment allowing molecular depth profiles to be obtained through the film. By combing secondary ion imaging with depth profiling, three-dimensional molecular image depth profiles have been obtained from these systems. In another approach, bevel cross-sections are cut in the samples with the SF5+ primary ion beam to produce a laterally magnified cross-section of the sample that does not contain the beam-induced damage that would be induced by conventional focussed ion beam (FIB) cross-sectioning. The bevel surface can then be examined using cluster SIMS imaging or other appropriate microanalysis technique. 相似文献