Thermal degradation behavior of multi-walled carbon nanotubes/polyamide 6 composites

This paper focuses on the thermal degradation behavior of multi-walled carbon nanotubes (MWNTs)/polyamide 6 (PA6) composites under air and nitrogen atmosphere using thermogravimetric analysis (TGA). The results show that the dispersion of amino-functionalized MWNTs (f-MWNTs) in PA6 is more homogeneous than purified MWNTs (p-MWNTs). The presence of MWNTs improves the thermal stability of PA6 under air obviously, but has little effect on the thermal degradation behavior of PA6 under nitrogen atmosphere. The activation energies for degradation under air, E_a, estimated by Kissinger method, are 153, 165 and 169 kJ/mol for neat PA6, p-MWNTs/PA6 and f-MWNTs/PA6 composites, respectively. The p-MWNTs/PA6 composites show two-step degradation not only under air but also under nitrogen atmosphere, however, neat PA6 and the f-MWNTs/PA6 composites exhibit two-step degradation only under air.     

取代金刚烷的异构体计数

采用图论方法对单一种取代基取代的金刚烷和烷基取代的金刚烷构型、手性构型和非手性构型数进行了计算,结果分别以母函数形式和表格形式给出。     

Study of Six Polycyclic Aromatic Hydrocarbons by Chemical Deoxygenation Microemulsion-Stabilized Room Temperature Phosphorimetry

Six polycyclic aromatic hydrocarbons (PAHs) are studied by chemical deoxygenation microemulsion-stabilized room temperature phosphorimetry with sodium sulfite as an oxygen scavenger and thallous nitrate as a heavy atom perturber in sodium dodecyl sulfate medium. Several factors influencing room temperature phosphorescence such as the concentration of sodium dodecyl sulfate, the heavy atom concentration, the pH, and the concentration of sodium sulfite are discussed and the quenching effect of NO₂⁻on room temperature phosphorimetry of PAHs was compared in the microemulsion and micelle media.     

Hypergraph Turán Numbers of Vertex Disjoint Cycles

The Turán number of a k-uniform hypergraph H,denoted by ex_k(n;H),is the maximum number of edges in any k-uniform hypergraph F on n vertices which does not contain H as a subgraph.Let C_l~((k)) denote the family of all k-uniform minimal cycles of length l;S(?₁,…,?_r) denote the family of hypergraphs consisting of unions of r vertex disjoint minimal cycles of length ?₁,…?_r,respectively,and C_l~((k))denote a k-uniform linear ...     

Generalized self-dual Yang-Mills flows,explicit solutions and reductions

An evolution equation is added to the generalized self-dual Yang-Mills equations. The evolution equation contains terms of negative powers of the spectral parameter as well as terms of positive powers. The Darboux matrix method is used to obtain explicit solutions, especially single and multiple solitons. All integrable soliton equations in the framework of AKNS system (inR ⁿ⁺¹ orR ¹⁺¹) can be derived from the generalized Yang-Mills flows by reduction.Supported by Chinese research project Nonlinear Science and K.C. Wong Education Foundation, Hong Kong.     

The application of principal component regression on simultaneous multicomponent determinations through a single catalytic kinetic run

The kinetic behaviors of Cr(VI) and W(VI), which catalyze a common indicator reaction between H(2)O(2) and I(-), were studied. A new concept, 'Rate Spectrum', is proposed. The two catalysts can be determined simultaneously by analyzing the rate spectra of their mixtures as the rate spectra of each catalyst are linearly independent. Principal Component Regression (PCR) was used to analyze the rate spectra of the mixtures of Cr and W, and in this way the two ions were determined simultaneously through a single kinetic run.     

治疗小儿厌食症中药强壮灵冲剂微量元素测定及其与疗效关系探讨

已证明小儿厌食症除与缺乏微量元素锌关系密切外,还与其他多种微量元素和宏量元素的缺乏或低下也有关。本院以自行研制的中药强壮灵冲剂治疗小儿厌食症疗效显著。其于浸膏粉经２０余种微量元素测定表明含有锌、铁、钴、铜、镍、锰、铬、锗、锶、铝、钡、硒、硅、钛等多种人体必需且品种齐全,含量适度的微量元素。上述元素又恰是患儿体内所缺乏和低下的品种,无疑对患儿全面适度的补充大有裨益．中药强壮灵与西药硫酸锌临床对比研究表明,无论比发锌回升数值以及从厌食等全面疗效统计,中药组均明显优于西药组,并且发现疗效与药物的补锌量不成正相关。说明中药的调理脾胃功能及综合整体治疗作用是其突出优点,值得推广．