Photonic instantaneous microwave frequency measurement based on two different phase modulation to intensity modulation conversions

A novel photonic technique for instantaneous frequency measurement of microwave signal based on phase modulation to intensity modulation conversion is proposed and demonstrated. In the proposed system, an optical carrier is modulated by a microwave signal with its frequency to be measured through a phase modulator. The phase-modulated optical signal is then converted to intensity-modulated signals in two independent paths using a dispersive media and a frequency discriminator respectively. Since the dependence of the received microwave power on the input microwave frequency in the two paths differs, the microwave power ratio between the two paths can be used to uniquely determine the microwave frequency. The major advantages of the approach lie in that only one laser source and the bias-free phase modulator is employed in the system, which improves the stability of the system. Experimental demonstrations of the frequency measurement based on the proposed approach are presented.     

Depolarization properties of cirrus clouds from polarization lidar measurements over Hefei in spring

A new polarization lidar has been developed for detecting depolarization characteristics of aerosol and cirrus over Hefei (31.90°N, 117.16°E), China. The fundamental principle of polarization lidar is briefly introduced.     

一种新型微透镜阵列成象式投影光刻系统的研究

从理论和实验两方面入手,系统地研究了微透镜阵列的形成原理和制作工艺,分析了微透镜阵列的面形结构,得到了联系微透镜阵列矢高与制作工艺参量的经验公式.并且将四片微透镜阵列耦合,形成一个深紫外光刻的1:1成象的多孔径微小光刻系统.从几何光学理论出发,分析了这个光刻系统综合成象的特点,讨论了这种光刻系统的光学性能,并给出了实验测量方法.     

共焦扫描显微成象系统的点扩散函数再商讨

针对共焦扫描显微成象中物体相对于被扫描点的位置矢量是反向移动的特性,探讨了物体移动后的物函数在此基础上,根据成象的理论进行了计算,得到新的系统点扩散函数表达式,最后根据计算结果分析成象的性质,得出了系统成象的相干性.     

ICP-MS法测定不同采收时间宽叶荨麻中微量元素含量

采用微波消解,ICP-MS法分析不同采收时间宽叶荨麻中18种微量元素Al,Ba,Ca,Co,Cr,Cu,Fe,K,Li,Mg,Mn,Mo,Na,Ni,P,Pb,S和Zn的含量。该方法的相对标准偏差在1.2%～5.3%之间,加标回收率在95.4%～101.2%之间。结果表明宽叶荨麻中K,P,S,Ca,Na含量较高;Fe,Mg,Mn,Zn含量次之;有潜在生理毒性的元素Al,Cr,Pb的含量较低,并且在宽叶荨麻中微量元素呈现明显的季节性动态变化,此结果为进一步研究宽叶荨麻药理药效与微量元素的关系以及更好的开发这一资源提供理论数据。     

光声内窥镜系统在人体直肠癌离体组织中的实验研究

研制了基于4阵列传感器的光声内窥镜探头,并基于此搭建了光声内窥镜成像系统,开展了仿体实验成像研究,通过内窥镜探头4个阵元位置激光吸收强度的变化情况来分析仿体中吸收体的位置,论证了其定位能力,利用光声内窥镜系统对人体离体的正常组织、直肠癌早期组织进行成像研究;通过对不同阵元位置的光吸收强度分布进行统计分析,证明了光声内窥镜对早期直肠癌组织和正常组织的辨别能力,此项技术有望提高直肠癌早期诊断的准确率,具有潜在的临床应用前景。     

Simultaneous Determination of Acetylsalicylic Acid and Caffeine in Pharmaceutical Formulation by First Derivative Synchronous Fluorimetric Method

A sensitive, rapid, and specific assay has been developed for the simultaneous determination of acetylsalicylic acid and caffeine in commercial tablets based on their natural fluorescence. The mixture of these drugs was resolved by first derivative synchronous fluorimetric technique using two scans. At Δλ=106 nm, using first derivative synchronous scanning, only acetylsalicylic acid yields a detectable signal at 316 nm (peak to zero method) which is unaffected by caffeine. At Δλ=30 nm, the signal of caffeine at 288 nm (peak to zero method) is not affected by acetylsalicylic acid. The range of application is between 0.021 and 41.62 μg ml⁻¹ (correlation coefficient, R=0.9995) for acetylsalicylic acid and between 0.4486 and 44.86 μg ml⁻¹ (correlation coefficient, R=0.99786) for caffeine. The recovery range of 98.40–102% for acetylsalicylic acid and 90–100.5% for caffeine from their synthetic mixture was reported. Overall recovery of both compounds about 97–99% for acetylsalicylic acid and 97–98% for caffeine was obtained from real sample analysis. The detection limits are 0.0013 μg ml⁻¹ and 0.0306 μg ml⁻¹ for acetylsalicylic acid and caffeine, respectively. The relative standard deviation (n=10) for 20 μg ml⁻¹ of acetylsalicylic acid is 2.75% and for 2.2 μg ml⁻¹of caffeine is 1.7%.     

单级G-M 150制冷机性能实验研究

为满足高温超导和低温气体处理系统等工程应用项目的大冷量需求,单级大冷量G-M制冷机成为目前国内外的研究热点。文章中描述了以G-M150为基础的制冷机综合性能测试方法及实验平台,并对其制冷温度和制冷量两个主要性能的影响因素进行实验研究,为探讨20K单级大冷量G-M制冷机的研究提供参考。