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91.
A method for the determination of 3-chloro-4-(dichloromethyl)-5-hydroxy-2[5H]-furanone (MX), in drinking water by GC-MS with a limit of detection of 3.0 microg/l and a limit of quantification of 7.0 microg/l is presented. Clean-up by SPE and extraction of water samples with dichloromethane were carried out before the preconcentration of MX, which was derivatized directly in the injector of the GC, and the MX trimethylsilyl derivative was identified and quantitatively determined by MS. 相似文献
92.
Knowledge of the element content of biological systems is important in enabling understanding of uptake mechanisms and physiological response to stress conditions. In this work concentrations of mineral elements in sycamore (Acer pseudoplatanus L.) cells grown in the presence of cadmium have been analysed and compared with concentrations in control cells. Energy-dispersive X-ray fluorescence (EDXRF) was used to quantify the nutrients K, Ca, Mn, Fe, Cu, and Zn present in the cells. The reproducibility and accuracy of the technique were demonstrated by analysis of biological reference materials. Exposure of sycamore cells to cadmium had induced variation in the content of some elements. Mn, Cu, Zn, and, particularly, Fe concentrations in cells exposed to Cd were higher than those found in control cells. Ca is adsorbed on the cell walls and the concentration of K is not affected by the presence of Cd. 相似文献
93.
This is the first of two papers devoted to the study of a nonlocal evolution equation that describes the evolution of the local magnetization in a continuum limit of an Ising spin system with Kawasaki dynamics and Kac potentials. We consider subcritical temperatures, for which there are two local equilibria, and begin the proof of a local nonlinear stability result for the minimum free energy profiles for the magnetization at the interface between regions of these two different local equilibria; i.e., the fronts. We shall show in the second paper that an initial perturbation v
0 of a front that is sufficiently small in L
2 norm, and sufficiently localized that x
2
v
0(x)2
dx<, yields a solution that relaxes to another front, selected by a conservation law, in the L
1 norm at an algebraic rate that we explicitly estimate. There we also obtain rates for the relaxation in the L
2 norm and the rate of decrease of the excess free energy. Here we prove a number of estimates essential for this result. Moreover, the estimates proved here suffice to establish the main result in an important special case.on leave from 相似文献
94.
Carlos A. Aragão de Carvalho 《Nuclear Physics B》1977,119(3):401-412
We investigate a theory using Callan-Symanzik equations. Logarithmic corrections to trivial fixed-point behaviour are obtained. The theory is shown to correspond to a model for tri-critical phenomena in 3He4He mixtures. 相似文献
95.
Dominating proton structure has been identified in the Kπ=3+ band of 168Yb, contrasting with neutron structure in the corresponding band of 172Yb. A region of low-lying Kπ=3+ bands is now established, with N=98?104, Z=68?72. For all stable nuclei in this region, the IπK=4+3 state is excited by inelastic deutron scattering. 相似文献
96.
We study the dynamics of multipartite entanglement under the influence of decoherence. A suitable generalization of concurrence reveals distinct scaling of the entanglement decay rate of Greenberger-Horne-Zeilinger and W states, for various environments. 相似文献
97.
We show that heating of harmonically trapped ions by periodic delta kicks is dramatically enhanced at isolated values of the Lamb-Dicke parameter. At these values, quasienergy eigenstates localized on island structures undergo avoided crossings with extended web states. 相似文献
98.
Low-pump-power,short-fiber copropagating dual-pumped (800 and 1050 nm) thulium-doped fiber amplifier
Gomes AS Carvalho MT Sundheimer ML Bastos-Filho CJ Martins-Filho JF Von der Weid JP Margulis W 《Optics letters》2003,28(5):334-336
Using optical frequency-domain reflectometry to reveal the gain distribution and allow us to optimize a thulium-doped fiber amplifier, we have demonstrated 18-dB gain by employing only 5 m of a 2000-parts-in-10(6)-Tm-doped fiber pumped with 145 mW of power at dual wavelengths of 800 and 1050 nm. The role of the 800-nm pump, which by itself does not permit population inversion, was clearly observed experimentally. 相似文献
99.
Aitala EM Amato S Anjos JC Appel JA Ashery D Banerjee S Bediaga I Blaylock G Bracker SB Burchat PR Burnstein RA Carter T Carvalho HS Copty NK Cremaldi LM Darling C Denisenko K Devmal S Fernandez A Fox GF Gagnon P Gobel C Gounder K Halling AM Herrera G Hurvits G James C Kasper PA Kwan S Langs DC Leslie J Lundberg B Magnin J Massafferri A MayTal-Beck S Meadows B de Mello Neto JR Mihalcea D Milburn RH de Miranda JM Napier A Nguyen A d'Oliveira AB O'Shaughnessy K Peng KC Perera LP Purohit MV 《Physical review letters》2001,86(5):770-774
From a sample of 1172 +/- 61 D(+)-->pi(-)pi(+)pi(+) decays, we find gamma(D(+)-->pi(-)pi(+)pi(+))/gamma(D(+)-->K-pi(+)pi(+)) = 0.0311 +/- 0.0018(+0.0016)(-0.0026). Using a coherent amplitude analysis to fit the Dalitz plot of these decays, we find strong evidence that a scalar resonance of mass 478(+24)(-23) +/- 17 MeV/c(2) and width 324(+42)(-40) +/- 21 MeV/c(2) accounts for approximately half of all decays. 相似文献
100.
José M. Arrieta Alexandre N. Carvalho 《Transactions of the American Mathematical Society》2000,352(1):285-310
We prove a local existence and uniqueness theorem for abstract parabolic problems of the type when the nonlinearity satisfies certain critical conditions. We apply this abstract result to the Navier-Stokes and heat equations.