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排序方式: 共有126条查询结果,搜索用时 16 毫秒
11.
Valeria Avataneo Alice Palermiti Amedeo De Nicol Jessica Cusato Gloria Giussani Andrea Calcagno Antonio DAvolio 《Molecules (Basel, Switzerland)》2022,27(3)
Vitamin D (VD) is a calcium- and phosphate-controlling hormone used to treat bone disorders; yet, several other effects are progressively emerging. VD deficiency is highly prevalent worldwide, with suboptimal exposure to sunlight listed among the leading causes: oral supplementation with either cholecalciferol or calcitriol is used. However, there is a scarcity of clinical studies investigating how quickly VD concentrations can increase after supplementation. In this pilot study, the commercial supplement ImmuD3 (by Erboristeria Magentina®) was chosen as the source of VD and 2000 IU/day was administered for one month to 21 healthy volunteers that had not taken any other VD supplements in the previous 30 days. Plasma VD levels were measured through liquid chromatography coupled to tandem mass spectrometry after 7, 14, and 28 days of supplementation. We found that 95% of the participants had insufficient VD levels at baseline (<30 ng/mL; median 23.72 ng/mL; IQR 18.10–26.15), but after 28 days of supplementation, this percentage dropped to 62% (median 28.35 ng/mL; IQR 25.78–35.20). The median increase in VD level was 3.09 ng/mL (IQR 1.60–5.68) after 7 days and 8.85 ng/mL (IQR 2.85–13.97F) after 28 days. This study suggests the need for continuing VD supplementation and for measuring target level attainment. 相似文献
12.
We propose a model for the electrostatics of globular proteins in which the low dielectric region is replaced by concentric spheres of the appropriate size. The method uses analytical formulas for the dielectric sphere and allows an efficient and accurate treatment of bulk charges. For surface charges, we propose a numerical determination of the sphere radius based on the solvent exposure of the individual atoms. The present implementation of the sphere model yields a good approximation of finite-difference Poisson solvation and interaction energies for a test set of 12 proteins. 相似文献
13.
Giovanna Bruni Vittorio Berbenni Franco Sartor Chiara Milanese Alessandro Girella Dionigio Franchi Amedeo Marini 《Journal of Thermal Analysis and Calorimetry》2012,108(1):235-241
In this work, thermoanalytical, diffractometry, and microscopy measurements have been performed in order to characterize the
effect of high energy milling on a drug active in the migraine prophylaxis and smoke cessation. We can assert that the mechanical
treatment induces only a partial amorphisation of the solid phase, in particular it reduces the crystal order by producing
lattice defects which propagate from the surface to the bulk crystal. For this reason, the DSC is able to detect the presence
of ordered solid, while the powder X-ray diffractometry, because of its low penetration depth, does not reach the crystalline
core of the particles. 相似文献
14.
C. Ratsch C. Anderson R. E. Caflisch L. Feigenbaum D. Shaevitz M. Sheffler C. Tiee 《Applied Mathematics Letters》2003,16(8):1165-1170
We adapt the level-set method to simulate epitaxial growth of thin films on a surface that consists of different reconstruction domains. Both the island boundaries and the boundaries of the reconstruction domains are described by different level-set functions. A formalism of coupled level-set functions that describe entirely different physical properties is introduced, where the velocity of each level-set function is determined by the value of the other level-set functions. 相似文献
15.
ABSTRACT We examined the effect as donors of three aryl β-D-galactosides (i.e. p-nitrophenyl β-D-galactopyranoside, o-nitrophenyl β-D-galactopyranoside and phenyl β-D-galacto-pyranoside) on the regioselectivity and the yield of the synthesis of N-acetyllactosamine obtained from the transglycosylation reaction catalyzed by a crude preparation of β-D-galactosidase from Bacillus circulans at 25 °C, 37 °C and 55 °C, respectively. Using p-nitrophenyl β-D-galactopyranoside the reaction results were fully regiospecific at all the temperatures considered: the maximum molar yield (74%) was obtained at an incubation temperature of 55 °C. Using o-nitrophenyl β-D-galactopyranoside as the donor the reaction was still highly regioselective and the maximum molar yield (50%) was achieved at an incubation temperature also of 55 °C. Using phenyl β-D-galactopyranoside transglycolytic products appear only at an incubation temperature of 55 °C but at very low molar yield (about 14%) and lower regioselectivity. 相似文献
16.
Orazio Attanasi Paolino Filippone Amedeo Mei Franco Serra-Zanetti 《Journal of heterocyclic chemistry》1986,23(1):25-28
The direct synthesis of a new class of unknown 1-heterocyclamino-3-carbonylpyrroles and 1-heterocyclamino-3-carboxypyrroles by copper(II) chloride-catalyzed reaction of heterocyclic conjugated azoalkene derivatives with β-diketones and β-ketoesters is reported. 相似文献
17.
This is the second of two papers on the zero-viscosity limit for the incompressible Navier-Stokes equations in a half-space
in either 2D or 3D. Under the assumption of analytic initial data, we construct solutions of Navier-Stokes for a short time
which is independent of the viscosity. The Navier-Stokes solution is constructed through a composite asymptotic expansion
involving the solutions of the Euler and Prandtl equations, which were constructed in the first paper, plus an error term.
This shows that the Navier-Stokes solution goes to an Euler solution outside a boundary layer and to a solution of the Prandtl
equations within the boundary layer. The error term is written as a sum of first order Euler and Prandtl corrections plus
a further error term. The equation for the error term is weakly nonlinear; its linear part is the time dependent Stokes equation.
This error equation is solved by inversion of the Stokes equation, through expressing the solution as a
regular (Euler-like) part plus a boundary layer (Prandtl-like) part. The main technical tool in this analysis is the Abstract
Cauchy-Kowalewski Theorem.
Received: 5 September 1996 / Accepted: 14 July 1997 相似文献
18.
Olga Bortolini Beatrice Russo Giovanni Sindona Amedeo Tocci 《Tetrahedron letters》2007,48(40):7125-7128
1,3-Dipolar cycloadditions of nitrones with alkenes afforded the corresponding isoxazolidines in ionic liquids in the presence of Er(OTf)3. The ionic liquid and the catalyst are recycled up to five times without any specific treatment or loss of activity. Extension of the procedure to the synthesis of isoxazolidinyl nucleosides has been investigated. 相似文献
19.
This is the first of two papers on the zero-viscosity limit for the incompressible Navier-Stokes equations in a half-space.
In this paper we prove short time existence theorems for the Euler and Prandtl equations with analytic initial data in either
two or three spatial dimensions. The main technical tool in this analysis is the abstract Cauchy-Kowalewski theorem. For
the Euler equations, the projection method is used in the primitive variables, to which the Cauchy-Kowalewski theorem is directly
applicable. For the Prandtl equations, Cauchy-Kowalewski is applicable once the diffusion operator in the vertical direction
is inverted.
Received: 5 September 1995 / Accepted: 14 July 1997 相似文献
20.