Single Crystal of Lanthanum Hydroxide La(OH)3: Controlled Synthesis by High Pressure Flux Method and Its Growth Mechanism

High pressure synthesis of solid material tends to increase the density,coordination number,symmetry of material and shorten bond length.The solid synthesized at a high pressure and decompressed to ambient pressure often exhibits a metastable "stretched" state,within the high pressure stability field.The crystal grown at a high pressure is of great importance with the development of high pressure technology.Crystal growth is an important factor in the material synthesis.And many methods including gas,solid and solution methods have been used to obtain various single crystals[1].Especially,flux method is an important method for crystal growth,where the components of the desired substance dissolved in a solvent(flux) grow in the process of deposit.Its advantage is that the crystal growth displays natural facets and the disadvantage is that the crystals are relatively small.Up to date,some solid materials have been successfully synthesized by high pressure flux method[2-7].     

Keggin型磷钼杂多蓝的制备新方法——射频氢等离子体固相还原法

将射频等离子体技术应用于杂多蓝的制备中, 成功地制备出四电子还原的磷钼杂多蓝, 并对所制备的杂多蓝进行了结构表征及性质研究, 探讨了磷钼杂多酸在射频氢等离子体中的还原行为.     

硬盘微晶玻璃基板化学机械抛光研究

利用自制的抛光液对硬盘微晶玻璃基板进行化学机械抛光.研究了抛光压力、SiO2浓度、pH和氧化剂过硫酸铵浓度等因素对材料去除速率MRR和表面粗糙度Ra的影响,系统分析了微晶玻璃抛光工艺过程中的影响因素,优化抛光工艺条件,利用原子力显微镜检测抛光后微晶玻璃的表面粗糙度.结果表明:当抛光盘转速为100 r/min、抛光液流量为25 mL/min、抛光压力为9.4 kPa、SiO2浓度为8wt;、pH=8、过硫酸铵浓度为2wt;时,能够得到较高的去除速率(MRR=86.2 nm/min)和较低表面粗糙度(Ra=0.1 nm).     

Characterization and separation of Al_(13) species using gel-filtration chromatography

Polyaluminum chloride (PAC) coagulant has been developed and widely used in water and wastewater treatment industry since the 1980s[1]. PAC is normally made by partial hydrolysis of acid aluminum chloride solution using slow alkaline titration method. However, this method would result in many different Al species. Among these Al species, it seems that tridecamer (Al13O4(OH) 724 , often denoted by Al13) is the most effective and stable polymeric Al species for water and wastewater treatme…     

模板法合成含镧的层状无机-有机纳米复合材料

以表面活性剂十二烷基磺酸钠为模板制备了含稀土元素La的无机-有机纳米复合材料。通过XRD、SEM、HRTEM、EDX等的表征，证明所得的稀土复合物为层状结构，且十二烷基磺酸钠与La的比例为1∶1。考察了反应温度、反应时间以及原料配比等对复合物结构的影响。     

复曲线上的Jackson型定理

令$\Ga$是复平面(z)中的光滑闭Jordan曲线. 作者借助于Hermite插值的基多项式, 引入连续函数插值, 它一致收敛于$f(z)\in C(\Ga)$,且具有和实区间$[-1, 1]$上Jackson定理1中一样的逼近阶, 并证明了这里逼近阶的精确性. 利用和以往工作不同的方法, 研究了同时逼近到函数及其导数, 并得到和实区间$[-1, 1]$上Jackson定理2一样的理想结果.     

石墨炉原子吸收光谱法测定交通警察精液中铅含量

本文法以２３名外勤交警作为接触组，用０．１ｍＬ的精液５倍稀释匹配标准系列，石墨炉原子吸收光谱法测定了精液中的含量。此方法具有良好的精密的准确度，相对标准偏差（ＲＳＤ）为２．３７％，回收率为９２．６２％－１０６．８５％。     

P-twisted affine Lie algebra and its realizations by twisted vertex operators

In this paper, we define a P-twisted affine Lie algebra, and construct its realizations by twisted vertex operators.     

带位势Landau-Lifshitz方程弱解的部分正则性

证明了三维或四维空间中带位势的Landau-Lifshitz方程的稳态解的部分正则性. 众所周知, 由于方法的限制, 对带位势的Landau-Lifshitz方程的稳态弱解的部分正则性需要对位势限制很强的条件. 由位势引起的主要困难是如何得到Scaling函数满足的方程, 这使得Blow-up方法失效. 作者通过直接估计Morrey能量以避开Blow-up方法而克服了该困难.     

夹心法免疫层析试条的数学模型与仿真研究

基于夹心法免疫层析试条检测原理,结合对流扩散方程和流体动力学方程,建立了夹心法免疫层析试条动态反应过程的数学模型,并通过COMSOL软件对试条动态反应过程进行仿真.分别探究了目标待测物A浓度在0 ～ 20 mol/L,标记物P浓度在1×10-2～1×103 mol/L以及硝酸纤维素膜的孔隙率在0～1范围内变化时,检测线上夹心复合物浓度关于位置和时间的浓度变化情况,并分析了各物质初始浓度以及试条结构对于检测结果和检测时间的影响.结果表明,在一定浓度范围内,目标待测物A以及标记物P浓度的增加将提高试条的定量检测性能,而孔隙率通过影响混合液流速和混合液中各物质反应接触情况来影响检测结果.