双组元姿控发动机反流特性的DSMC模拟

为准确获得双组元姿控发动机的羽流及其反流特性,采用直接模拟蒙特卡罗(DSMC)方法结合可变软球(VSS)模型数值模拟以N2O4/MMH为推进剂的真空羽流。喷口参数由喷管流动的DSMC法计算得到。与文献比较表明本文计算程序可信。模拟结果表明,分子质量越小的气体越容易进入反流区;本文的计算条件下,在偏离X轴正向116°~140°范围内,组分数密度和质量流率以及温度均出现了最大值。     

广义非简谐振子的多尺度微扰理论

应用多尺度微扰理论到广义非简谐振子, 得到了一阶经典和量子微扰解. 特别是 我们的量子解在极限条件下能方便地转变为经典解, 并且坐标和动量算符的对易 关系的简化十分自然. 与Taylor级数解相比较, 无论是在经典还是在量子解 中频率移动都出现在各阶振动表达式中, 所以多尺度微扰解是弱耦合非简谐振动的较好解法.     

HL-2A װ��MW ������������ϵͳ��˿��Դ�����������

The main circuit topology, control hardware and control sequence of the cathode filament power supply for the HL-2A neutral beam heating system was introduced. Feedback control simulation of main circuit of filament power supply is carried out through MATLAB simulation software. It is found that the ripple factor is about 1%when the current is about 1000A, and the ripple coefficient increases to 3% when the current drops to 200A. Without the AC filter reactor in series L₁ and parallel harmonic filter LC in the low level control cabinet, the output current ripple coefficient becomes larger obviously. It shows that L₁ and LC not only absorb harmonic current, but also filter the chopper waveform after AC voltage regulation to make the output waveform smoother.     

对称双吡咯甲烷的合成与分子内氢键的研究

５－甲基吡咯－２－羧酸酯在磺酰氢，溴或四乙酸铅作用下，生成相应的在５－甲基上含取代基的产物，后者不经分离不便可自缩合得标题化合物，核磁共振氢谱研究和分子构象木匠，当３，３位的取代基为甲酸（酯）基或乙酸（酯）基时，可形成３，３位酯基与另一吡咯环上的氮氢之间的分子内氢键，而３，３位是其它取代基，如乙酰基，丙酸（酯）基，丁酸（酯）基时不能形成类似的分子内氢键。     

非相干光源用于“核-环比”法测量表面粗糙度

本文将文献[1-5]的用激光测量表面粗糙度的“核-环比”法推广到采用其他非相干光源,给出测量原理的定量公式及测量装置的结构框图。     

一维螺旋状3，6-哒嗪二甲酸镉(Ⅱ)配位聚合物的合成与结构

Using the ligand pyridazine-3，6-dicarboxylate (H₂pzdc)， a coordination polymer [Cd₂(pzdc)₂(H₂O)₄] was synthesized and characterized by elemental analysis， thermal analysis， IR and single-crystal X-ray diffraction. The complex crystallizes in the tetragonal system with space group I4₁/a. The crystallographic data are: a=1.470 6(4) nm， c=1.489 8(6) nm， V=3.222 0(19) nm³， Z=16， μ=2.725 mm^-1， D_c=2.594 g·cm^-3， R₁=0.017 8， wR₂=0.044 6. In the complex， the cadmium(Ⅱ) ions with the eight-coordinated dodecahedral geometry are linked by the pzdc ligands to generate one-dimensional chains， which are associated into the three-dimensional architecture via O-H…O hydrogen bonding. CCDC: 658853.     

WS2 超细粉体的固相法合成

WS2 超细粉体的固相法合成;WS2;固相反应;过硫系数;高能球磨;粒度     

铁形态分析进展

本文对Fe（Ⅱ）、Fe（Ⅲ）形态分析在1990－2000年间的发展概况作了综述，内容包括分光光度法、色谱法、流动注射分析法等。引用文献53篇。     

Solvent-free Synthesis of Dihydrofuran-fused [60]Fullerene Derivatives by High-speed Vibration Milling

Solvent-free organic reactions have been attracting great interest of chemists due to the elimination of the usage of harmful organic solvents,low costs,and simplicity in the procedure1.Solvent-free mechanochemical reactions of fullerenes were explored and are significant for the reactions of fullerenes because the low solubility of fullerenes in common organic solvents requires large quantity of organic solvents and some novel fullerene reactions could only occur in the solid-state reaction2.…     

Increase of Calcium Levels at Interphase in NIH 3T3 Cells

The fluorescent calcium ion indicator dye Fluo-3 and DNA-binding dye Hoechst 33342 were employed to determine, in a quantitative microspectrofluorometric study, the intracellular calcium ion concentration ([Ca~(2+)]_i) and the DNA content of individual living NIH3T3 cells. The well-separated excitation and emission properties of these dyes allowed us to establish for each cell both the phase of the cell cycle using DNA content and [Ca~(2+)]_i. We found that the transition from G_1, through S, to the G_2 phase is accompanied by a two-fold increase in [Ca~(2+)]_i. The [Ca~(2+)]_i was inhomologous in each phase of the interphase (G_1, S and G_2) although [Ca~(2+)]_i in the S and G_2 phases was never lower than certain threshold values in the G_1 and S phases respectively. [Ca~(2+)]_i in G_0 cells was lower than that in G_2 cells. These changes in [Ca~(2+)]_i suggest that [Ca~(2+)]_i may be an import regulator of cell cycle progression.