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Ling-yan Li Hui Gu Yong-jun Tian Toshiyuki Nishimura Joachim Bill 《Journal of Non》2009,355(48-49):2390-2395
Inner pore channels were commonly found in precursor-derived Si–C–N ceramics. After annealing in air at 1420 °C, their oxidation structures were investigated by analytical TEM. A carbon-rich ring was frequently observed under the silica layer inside the pore channels, which consisted of graphite-like clusters in size of 20–30 nm. Origin of such interfacial structure is due to the excessive free-carbon in the amorphous Si–C–N matrix that had survived the oxidation process. This graphitic interface could further improve the oxidation resistance of the SiO2 over-layer. This novel interfacial structure was also found by annealing in N2, reaffirming the effect of composition of Si–C–N matrix. 相似文献
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Adam A. Stokes David J. Clarke Stefan Weidt Pat Langridge-Smith C. Logan Mackay 《International journal of mass spectrometry》2010,289(1):54-57
We report high resolution spectra for the medium molecular weight proteins myoglobin and cytochrome-c obtained using a custom desorption electrospray ionisation (DESI) source coupled to a Bruker Daltonics 12 T Apex Qe Fourier transform ion cyclotron resonance mass spectrometer (FTICR-MS). The DESI source was designed for accurate alignment and reproduction of critical geometric variables. A two axis motorised stage was included to enable automated rastering of the sample under the DESI plume. Spectra for the intact proteins have been obtained under single-acquisition conditions and a top-down analysis of cytochrome-c was performed using both collision induced dissociation (CID) and electron capture dissociation (ECD) of the isolated [M+15H]15+ charge state. The sequence coverage is comparable to that obtained using electrospray ionisation, demonstrating the utility of top-down protein analysis by DESI FTICR-MS. 相似文献
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Fang Zhang Shaoan Cheng Deepak Pant Gilbert Van Bogaert Bruce E. Logan 《Electrochemistry communications》2009,11(11):2177-2179
An inexpensive activated carbon (AC) air cathode was developed as an alternative to a platinum-catalyzed electrode for oxygen reduction in a microbial fuel cell (MFC). AC was cold-pressed with a polytetrafluoroethylene (PTFE) binder to form the cathode around a Ni mesh current collector. This cathode construction avoided the need for carbon cloth or a metal catalyst, and produced a cathode with high activity for oxygen reduction at typical MFC current densities. Tests with the AC cathode produced a maximum power density of 1220 mW/m2 (normalized to cathode projected surface area; 36 W/m3 based on liquid volume) compared to 1060 mW/m2 obtained by Pt catalyzed carbon cloth cathode. The Coulombic efficiency ranged from 15% to 55%. These findings show that AC is a cost-effective material for achieving useful rates of oxygen reduction in air cathode MFCs. 相似文献
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Bill Domoney 《Research in Mathematics Education》2013,15(1):53-67
Previous research has shown that secondary school students’ understanding of fractions is dominated by the part-whole concept to the possible detriment of their understanding of a fraction as a number in its own right. The present paper reports on an investigation into the understanding of intending primary teachers in this area. Four representatives of a cohort of sixty students on a PGCE course specialising in the lower primary age range were asked detailed questions probing their knowledge of fractions. The conclusion was that the part-whole concept dominates. All of the students were familiar with the numerical concept from their work on the PGCE course, but they reverted to the more familiar part-whole ideas in attempting to solve problems. 相似文献
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Bill Jackson 《Journal of Geometry》2011,101(1-2):131-135
We describe characterizations of boundedness and rigidity of generic 2-dimensional direction?Clength frameworks, and give partial results for the open problem of characterizing the global rigidity of such frameworks. 相似文献
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