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排序方式: 共有273条查询结果,搜索用时 270 毫秒
31.
32.
Manisha S. Patil Amey V. Palav Chetan K. Khatri Ganesh U. Chaturbhuj 《Tetrahedron letters》2017,58(29):2859-2864
The present study describes a rapid, simple and straightforward approach to the synthesis of 1,8-dioxo-octahydroxanthenes, 14-phenyl-14H-dibenzo[a,j]xanthene and tetrahydrobenzoxanthene-11-ones under solvent-free conditions using sulfated polyborate as a highly efficient catalyst. The procedure offers several advantages including cleaner reaction profile, mild reaction condition, economic, recyclable and environmentally benign catalyst, high yields, simple experimental and workup procedures. While non-extractive work up/purification, along with reusability of catalyst make this method economically affordable for large scale. 相似文献
33.
The authors investigate limit-cycle oscillations of a wing/store configuration. Unlike typical aeroelastic studies that are based upon a linearized form of the governing equations, herein full system nonlinearities are retained, and include transonic flow effects, coupled responses from the structure, and store-related kinematics and dynamics. Unsteady aerodynamic loads are modeled with the equations from transonic small disturbance theory. The structural dynamics for the cantilevered wing are modeled by the nonlinear equations of motion for a beam. The effects of general store-placement are modeled by the nonlinear equations of motion related to the position-induced nonlinear kinematics. Chordwise deformations of the wing surface, as well as pylon and store flexibility, are assumed negligible. Nonlinear responses are studied by examining bifurcation and related response characteristics using direct simulation. Particular attention is given to cases for which large-time, time-dependent behavior is dependent on initial conditions, as observed for some configurations in flight test. Comparisons of results in which selective nonlinearities are excluded indicate that the accurate prediction of nonlinear responses such as limit cycle oscillations (LCOs) may depend upon consideration of all nonlinearities related to the full system. 相似文献
34.
Okada Y Dhital C Zhou W Huemiller ED Lin H Basak S Bansil A Huang YB Ding H Wang Z Wilson SD Madhavan V 《Physical review letters》2011,106(20):206805
We study interference patterns of a magnetically doped topological insulator Bi(2-x)Fe(x)Te(3+d) by using Fourier transform scanning tunneling spectroscopy and observe several new scattering channels. A comparison with angle-resolved photoemission spectroscopy allows us to unambiguously ascertain the momentum-space origin of distinct dispersing channels along high-symmetry directions and identify those originating from time-reversal symmetry breaking. Our analysis also reveals that the surface state survives far above the energy where angle-resolved photoemission spectroscopy finds the onset of continuum bulk bands. 相似文献
35.
The fabrication of high quality thin films of poly (vinylidene fluoride) embedded with multiwalled carbon nanotubes using pulsed laser deposition technique is reported. The prepared films were characterized for structural, morphology and dielectric properties. The morphology analysis revealed uniform dispersion of multiwalled carbon nanotubes throughout the polymer matrix. X-ray diffraction results suggested that the poly (vinylidene fluoride) film is in amorphous phase while addition of multiwalled carbon nanotubes showed presence of crystalline peaks in the nanocomposites films. It was interesting to note that the nanocomposite films exhibits significant enhancement of the ferroelectric β-phase as evidenced by the X-ray diffraction and Fourier transform infrared spectroscopy results. The dielectric analysis shows a remarkable enhancement in the dielectric permittivity of nanocomposites with lower loss and conductivity level. The results can be attributed to the formation of minicapacitor network and relatively higher percolation threshold in the nanocomposites. 相似文献
36.
Chetan Nayak 《General Relativity and Gravitation》1991,23(9):981-989
Einstein-Maxwell theory in 2+1 dimensions is considered as a toy model for the 3+1 theory and as a means for understanding field theories without a background space-time geometry. Two possible approaches to the quantization of this theory are presented, one based on a Schwinger-Tomonaga time evolution equation and the other on a loop space construction, and the problems arising in both of these are discussed. 相似文献
37.
We propose to use the recently predicted two-dimensional "weak-pairing" px + ipy superfluid state of fermionic cold atoms as a platform for topological quantum computation. In the core of a vortex, this state supports a zero-energy Majorana mode, which moves to finite energy in the corresponding topologically trivial "strong-pairing" state. By braiding vortices in the "weak-pairing" state, unitary quantum gates can be applied to the Hilbert space of Majorana zero modes. For readout of the topological qubits, we propose realistic schemes suitable for atomic superfluids. 相似文献
38.
Kalawati Meena Sudesh Kumari Jitender M. Khurana Amita Malik Chetan Sharma Harsh Panwar 《中国化学快报》2017,28(1):136-142
A simple and efficient three component procedure has been developed for the synthesis of highly substituted spiro[indolo-3,10'-indeno[1,2-b]quinolin]-2,4,11'-triones by one pot three component condensation of enaminones, isatin and indane-1,3-dione in ethanol:water (1:1) in presence of ceric ammonium nitrate (CAN) as catalyst. This method provides several advantages such as lesser reaction time, high yield of products and operational simplicity. The antimicrobial activity of some of the compounds has been investigated against six microbial strains, some of the tested compounds showed good antimicrobial activity. 相似文献
39.
Ayyalasomayajula KK Dikshit V Yueh FY Singh JP Smith LT 《Analytical and bioanalytical chemistry》2011,400(10):3315-3322
Laser-induced breakdown spectroscopy (LIBS) has been employed for the analysis of slurry samples. Quantitative analysis of
slurry samples is crucial and challenging. The problems associated with slurry samples include splashing, surface turbulence,
and the difficulties of obtaining reproducible samples due to sedimentation. The LIBS analysis has achieved limited success
due to inherent disadvantages when applied to slurry samples. In order to achieve improved measurement precision and accuracy,
a spin-on-glass sampling method was evaluated. Five elements (Al, Ca, Fe, Ni, and Si) were examined in five slurry simulants
containing varying amounts of each ion. Three calibration models were developed by using univariate calibration, multiple
linear regression, and partial least square regression. LIBS analysis results obtained from the partial least square regression
model were determined to be the best fit to results obtained from inductively coupled plasma optical emission spectroscopy
analysis. 相似文献
40.
Lactic acid produced by fermentation process mostly contains a number of aliphatic carboxylic acids as impurities. In this work, carboxylic acid impurities in lactic acid samples from a number of sources were determined at ppm levels. A simple HPLC method was developed that utilized a new generation polar embedded reverse phase, 20mM phosphate buffer at pH 2.20 (±0.05) and UV detection at 210 nm. The method enabled quantitative analysis of the above acids in lactic acid matrix. The experimental conditions for column temperature, mobile phase pH and flow rate were optimized. A detailed validation of the method was performed for linearity, precision, accuracy, selectivity, limit of detection (LOD), limit of quantitation (LOQ), ruggedness and repeatability and reproducibility (R&R). 相似文献