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41.
The control problem of axially moving strings occurs in a large class of mechanical systems. In addition to the longitudinal displacement, the strings are subject to undesirable transversal vibrations. In this work, in order to suppress these vibrations, we consider a control by a hydraulic touch-roll actuator at the right boundary. We prove uniform stability of the system using a viscoelastic material and an appropriate boundary control force applied to the touch rolls of the actuator. The features of the present work are: taking into account the mass flow entering in and out at the boundaries due to the axial movement of the string and overcoming the difficulty raised by the Kirchhoff coefficient which does not allow us to profit from the dissipativity of the system (as in the existing works so far). We shall make use of an inequality which is new in this theory.  相似文献   
42.
We investigated prospects for reported sustainable adoption and sharing of an educational innovation through survey research including online questionnaires and telephone interviews. This investigation is part of the Scaling-Up SimCalc experimental program, which combines dynamic representational algebra software (SimCalc MathWorlds) with integrated curriculum and small professional development workshops focused on how to use the software and how to integrate this intervention into the larger year-long curriculum. Teachers who (1) perceived the usefulness of the SimCalc professional development as being consistent with personal aims and (2) perceived specific affordances of the software/curriculum to be valuable were more likely to report continued use of the innovation after the research had ended and that they had shared it with colleagues over time.  相似文献   
43.
Oxazolidinethione compounds were synthesized starting from racemic and enantiopure β‐amino alcohols. The molecular structure of oxazolidinethione 6a was elucidated by single‐crystal x‐ray crystallography. Oxazolidinethione compounds screened for antimicrobial activity showed mild minimum inhibitory concentration values.  相似文献   
44.
Simple, rapid and highly sensitive spectrofluorimetric methods were developed for the determination of venlafaxine in pure and pharmaceutical preparations. The proposed methods were based on the reaction of venlafaxine as n-electron donor with π-acceptors namely, p-bromanil and p-chloranil. The method for the determination of venlafaxine over a concentration range of 5–100 and 5–150 ng/mL, for p-bromanil and p-chloranil methods, respectively. The intra- and inter-day precisions were satisfactory, the relative standard deviations did not exceed 1.69%. The proposed method was successfully applied to the determination of venlafaxine in its pharmaceutical preparations with good accuracy; the mean recovery percentages were 99.80%. The results were compared favorably with those of the reference method.  相似文献   
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46.
The aim through this work is to suppress the transverse vibrations of an axially moving viscoelastic strip. A controller mechanism (dynamic actuator) is attached at the right boundary to control the undesirable vibrations. The moving strip is modeled as a moving beam pulled at a constant speed through 2 eyelets. The left eyelet is fixed in the sense that there is no transverse displacement (see Figure 1 ). The mathematical model of this system consists of an integro‐partial differential equation describing the dynamic of the strip and an integro‐differential equation describing the dynamic of the actuator. The multiplier method is used to design a boundary control law ensuring an exponential stabilization result.  相似文献   
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48.
A simple, rapid and sensitive high performance liquid chromatography (HPLC) method was developed for the determination of metoclopramide in pharmaceutical preparation. The method is based on the derivatization of metoclopramide with fluorescamine. The separation was achieved on a C18 column using methanol‐water (70:30, V/V) mobile phase. Fluorescence detector was used at the excitation and emission of 403 and 485 nm, respectively. The method was validated for linearity, limit of detection, limit of quantification, precision, accuracy, recovery, robustness and system suitability. The assay was linear over the concentration range of 100–2000 ng/mL. The mean recovery was 100.37%. The proposed method was successfully applied to the assay of metoclopramide in tablet preparation. The preparation was also analyzed with an official method and statistical comparison by t‐ and F‐tests revealed that there was no significant difference between the results of the two methods with respect to mean values and standard deviations at the 95% confidence level.  相似文献   
49.
A novel precolumn derivatization reversed-phase high-performance liquid chromatography method with fluorescence detection is described for the determination of ranitidine in human plasma. The method was based on the reaction of ranitidine with 4-fluoro-7-nitrobenzo-2-oxa-1,3-diazole forming yellow colored fluorescent product. The separation was achieved on a C(18) column using methanol-water (60:40, v/v) mobile phase. Fluorescence detection was used at the excitation and emission of 458 and 521 nm, respectively. Lisinopril was utilized as an internal standard. The flow rate was 1.2 mL/min. Ranitidine and lisinopril appeared at 3.24 and 2.25 min, respectively. The method was validated for system suitability, precision, accuracy, linearity, limit of detection, limit of quantification, recovery and robustness. Intra- and inter-day precisions of the assays were in the range of 0.01-0.44%. The assay was linear over the concentration range of 50-2000 ng/mL. The mean recovery was determined to be 96.40 ± 0.02%. This method was successfully applied to a pharmacokinetic study after oral administration of a dose (150 mg) of ranitidine.  相似文献   
50.
A viscoelastic Timoshenko beam is investigated. We prove an exponential decay of solutions for a large class of kernels with weaker conditions than the existing ones in the literature. This will allow the use of other types of viscoelastic material for Timoshenko type beams than the usually used ones.  相似文献   
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