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71.
72.
In this paper as the main result we prove that the projective special linear group L 16(2) is uniquely determined by its prime graph. In fact we give a positive answer to an open problem arose in Zavarnitsin (Algebra Logic 43(4), 220–231, 2006) and we obtain a first example of a finite group with connected prime graph which is uniquely determined by its prime graph. This research was in part supported by a grant from IPM (No. 86200023).  相似文献   
73.
We demonstrate herein the synthesis of a new copper Schiff base complex immobilized on silica‐coated Fe3O4 nanoparticles. The structure and composition of this magnetic nanocatalyst were analyzed using Fourier transform infrared (FT‐IR), X‐ray powder diffraction (XRD), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), energy dispersive X‐ray (EDX) and inductively coupled plasma atomic emission spectroscopy (ICP‐AES). This nanocomposite was found to be an efficient nanocatalyst for the synthesis of polysubstituted pyrrole derivatives and the products were isolated with high turnover number (TON) and high to excellent yields. Among the new synthesized polysubstituted pyrrole derivatives, we explored the first computational and experimental binding study of methyl 1‐benzyl‐4‐(furan‐2‐yl)‐2‐methyl‐1H‐pyrrole‐3‐carboxylate (SP‐10) with calf thymus deoxyribonucleic acid (ct‐DNA), suggesting their application as potential anticancer activity. In addition, the binding modes of SP‐10 with DNA and human serum albumin (HSA) were verified by molecular docking technique.  相似文献   
74.
This paper presents a new solution to the Active Noise Control problem based on the Q-learning algorithm. Unlike other common methods, this feedback method does not require any additional information about the primary and secondary transfer functions and it is fully robust to subsystems dynamics changes. The basic method is addressed for periodic acoustic disturbances at first. A number of challenges such as the need for the large memory block and long convergence time have led to the establishment of some new suggestions. These modifications have improved the system performances and decreased the computational burden. It is shown by simulation that these methods are robust not for in the subsystems dynamics changes but also at the presence of measurement noise.  相似文献   
75.
Polysubstituted pyridine derivatives were synthesized through economical one-pot multicomponent reactions of different α,β-unsaturated ketones, malononitrile, and ethanol or methanol in the presence of Amberlite IRA-400 (OH) at room temperature. The catalyst is recyclable several times without substantial loss of activity. Other valuable features include the wide range of functional group tolerance, easy and clean synthesis with a simple work-up procedure, and excellent yields under mild conditions.  相似文献   
76.
This paper describes a new approach to optimum weight design of truss structures. The force method is incorporated in an optimization algorithm based on the method of center points. Design variables are the member cross-sectional areas and the redundant forces evaluated for each independent loading condition acting on the structure. The optimization method utilizes the largest hyperspheres inscribed within the feasible space. The method of hyperspheres has been enhanced here to handle the compatibility equality constraints as well. By including the analysis step in the optimization cycle there is no longer the need to perform separate structural analyses thus saving computation time. The viability and efficiency of the proposed method are demonstrated for truss structures subject to multiple loading conditions and constraints on member stresses, nodal displacement and minimum gage. Numerical results are compared with those reported in the literature.  相似文献   
77.
The oximation of a variety of carbonyl compounds was efficiently carried out with DOWEX(R)50WX4/NH2OH·HCl system. The reactions were performed in ethanol to give Z‐aldoximation isomers of aldehydes and E‐oximaton of acetophenone derivatives in a perfect selectively. The oximation of compounds with two carbonyl groups was carried out selectively on one carbonyl moiety. Also, the oximation of aldehydes over ketones has been accomplished successfully by this system.  相似文献   
78.
We report on the salt-assisted liquid-liquid microextraction of cationic complexes of Cr(VI) ion using the hydrophilic ionic liquid (IL) 1-butyl-3-methylimidazolium tetrafluoraborate and potassium hydrogen phosphate. This is a novel, simple, non-toxic and effective technique for sample pretreatment technique that displays large extraction efficiency and represents a new platform where Cr(VI) is complexed with 1,5-diphenylcarbazide (DPC) in sulfuric acid medium. It was applied to the extraction of Cr(VI) in the form of the Cr(VI)-DPC complex prior to its determination by flame atomic absorption spectrometry. Cr(III) ion also can be determined by this procedure after oxidation to Cr(VI). Extraction is mainly affected by the amount of water-soluble IL, the kind and quantity of inorganic salts, by pH and the concentration of DPC. Calibration plots are linear in the range from 3 to 150?μg?L?1 of Cr(VI), and the limit of detection is 1.25?μg?L?1. The method was successfully applied to the speciation and determination of trace levels of Cr(III) and Cr(VI) in environmental water samples containing high levels of dissolved salts or food grade salts.
Figure
Schematic representation SALLME-IL enrichment method (Salt assisted liquid–liquid microextraction with hydrophilic ionic liquid)  相似文献   
79.
In Li and Chen (Sib. Math. J. 53(2), 243–247, 2012), it is proved that the simple group $A_1(p^n)$ is uniquely determined by the set of orders of its maximal abelian subgroups. Let $q=p^{\alpha }$ be a prime power and $L=A_2(q)$ . In this paper, we prove that if $q$ is not a Mersenne prime, then every finite group with the same orders of maximal abelian subgroups as $L$ , is isomorphic to $L$ or an extension of $L$ by a subgroup of the outer automorphism group of $L$ .  相似文献   
80.
<正>An efficient one-pot synthesis of 2,4,6-triarylpyridines has been described.This involves the three-component reaction of aldehydes,ketones and ammonium acetate in the presence of a catalytic amount of wet 2,4,6-trichloro-1,3,5-triazine(TCT) under solvent-free condition at 130℃.  相似文献   
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