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排序方式: 共有749条查询结果,搜索用时 875 毫秒
741.
Michelle Camenzuli Jessica M. Terry R. Andrew Shalliker Xavier A. Conlan Neil W. Barnett Paul S. Francis 《Analytica chimica acta》2013
We describe a new approach to multiplex detection for HPLC, exploiting parallel segmented outlet flow – a new column technology that provides pressure-regulated control of eluate flow through multiple outlet channels, which minimises the additional dead volume associated with conventional post-column flow splitting. Using three detectors: one UV-absorbance and two chemiluminescence systems (tris(2,2′-bipyridine)ruthenium(III) and permanganate), we examine the relative responses for six opium poppy (Papaver somniferum) alkaloids under conventional and multiplexed conditions, where approximately 30% of the eluate was distributed to each detector and the remaining solution directed to a collection vessel. The parallel segmented outlet flow mode of operation offers advantages in terms of solvent consumption, waste generation, total analysis time and solute band volume when applying multiple detectors to HPLC, but the manner in which each detection system is influenced by changes in solute concentration and solution flow rates must be carefully considered. 相似文献
742.
The reaction of a fluorinated iridium complex with cerium(IV) and organic reducing agents generates an intense emission with a significant hypsochromic shift compared to contemporary chemically-initiated luminescence from metal complexes. 相似文献
743.
Aaltonen T Adelman J Akimoto T Albrow MG González BA Amerio S Amidei D Anastassov A Annovi A Antos J Aoki M Apollinari G Apresyan A Arisawa T Artikov A Ashmanskas W Attal A Aurisano A Azfar F Azzi-Bacchetta P Azzurri P Bacchetta N Badgett W Barbaro-Galtieri A Barnes VE Barnett BA Baroiant S Bartsch V Bauer G Beauchemin PH Bedeschi F Bednar P Behari S Bellettini G Bellinger J Belloni A Benjamin D Beretvas A Beringer J Berry T Bhatti A Binkley M Bisello D Bizjak I Blair RE Blocker C Blumenfeld B 《Physical review letters》2008,100(4):041801
We report on the results of a search for standard model Higgs bosons produced in association with W bosons from pp[over] collisions at sqrt[s]=1.96 TeV. The search uses a data sample corresponding to approximately 1 fb(-1) of integrated luminosity. Events consistent with the W-->lnu and H-->bb[over] signature are selected by triggering on a high-p(T) electron or muon candidate and tagging one or two of the jet candidates as having originated from b quarks. A neural network filter rejects a fraction of tagged charm and light-flavor jets, increasing the b-jet purity in the sample. We observe no excess lnubb[over] production beyond the background expectation, and we set 95% confidence level upper limits on the production cross section times branching fraction sigma(pp[over]-->WH)Br(H-->bb[over]) ranging from 3.9 to 1.3 pb, for specific Higgs boson mass hypotheses in the range 110 to 150 GeV/c2, respectively. 相似文献
744.
Aaltonen T Adelman J Akimoto T Albrow MG González BA Amerio S Amidei D Anastassov A Annovi A Antos J Aoki M Apollinari G Apresyan A Arisawa T Artikov A Ashmanskas W Attal A Aurisano A Azfar F Azzi-Bacchetta P Azzurri P Bacchetta N Badgett W Barbaro-Galtieri A Barnes VE Barnett BA Baroiant S Bartsch V Bauer G Beauchemin PH Bedeschi F Bednar P Beecher D Behari S Bellettini G Bellinger J Belloni A Benjamin D Beretvas A Beringer J Berry T Bhatti A Binkley M Bisello D Bizjak I Blair RE Blocker C 《Physical review letters》2008,100(7):071801
A direct measurement of the total decay width of the W boson Gamma(W) is presented using 350 pb(-1) of data from pp[over ] collisions at square root s = 1.96 TeV collected with the CDF II detector at the Fermilab Tevatron. The width is determined by normalizing predicted signal and background distributions to 230 185 W candidates decaying to enu and micronu in the transverse-mass region 50相似文献
745.
Aaltonen T Adelman J Akimoto T Albrow MG Alvarez González B Amerio S Amidei D Anastassov A Annovi A Antos J Apollinari G Apresyan A Arisawa T Artikov A Ashmanskas W Attal A Aurisano A Azfar F Azzurri P Badgett W Barbaro-Galtieri A Barnes VE Barnett BA Bartsch V Bauer G Beauchemin PH Bedeschi F Bednar P Beecher D Behari S Bellettini G Bellinger J Benjamin D Beretvas A Beringer J Bhatti A Binkley M Bisello D Bizjak I Blair RE Blocker C Blumenfeld B Bocci A Bodek A Boisvert V Bolla G Bortoletto D 《Physical review letters》2008,101(18):181602
We present the results of searches for large extra dimensions in samples of events with large missing transverse energy E_{T} and either a photon or a jet produced in pp[over ] collisions at sqrt[s]=1.96 TeV collected with the Collider Detector at Fermilab II. For gamma+E_{T} and jet+E_{T} candidate samples corresponding to 2.0 and 1.1 fb;{-1} of integrated luminosity, respectively, we observe good agreement with standard model expectations and obtain a combined lower limit on the fundamental parameter of the large extra dimensions model M_{D} as a function of the number of extra dimensions in the model. 相似文献
746.
Aaltonen T Abulencia A Adelman J Akimoto T Albrow MG Alvarez González B Amerio S Amidei D Anastassov A Annovi A Antos J Apollinari G Apresyan A Arisawa T Artikov A Ashmanskas W Attal A Aurisano A Azfar F Azzi-Bacchetta P Azzurri P Bacchetta N Badgett W Barbaro-Galtieri A Barnes VE Barnett BA Baroiant S Bartsch V Bauer G Beauchemin PH Bedeschi F Bednar P Behari S Bellettini G Bellinger J Belloni A Benjamin D Beretvas A Beringer J Berry T Bhatti A Binkley M Bisello D Bizjak I Blair RE Blocker C 《Physical review letters》2008,100(12):121803
We measure the mean lifetime tau=2/(Gamma_{L}+Gamma_{H}) and the decay-width difference DeltaGamma=Gamma_{L}-Gamma_{H} of the light and heavy mass eigenstates of the B_{s}{0} meson, B_{sL}{0} and B_{sH}{0}, in B_{s}{0}-->J/psivarphi decays using 1.7 fb;{-1} of data collected with the CDF II detector at the Fermilab Tevatron pp[over ] collider. Assuming CP conservation, a good approximation for the B_{s}{0} system in the standard model, we obtain DeltaGamma=0.076_{-0.063}{+0.059}(stat)+/-0.006(syst) ps{-1} and tau=1.52+/-0.04(stat)+/-0.02(syst) ps, the most precise measurements to date. Our constraints on the weak phase and DeltaGamma are consistent with CP conservation. 相似文献
747.
Stress relaxation during plastic deformation has been reported to improve ductility and alter the mechanical properties of metallic materials. The aim of the present study is to investigate the role of various mechanisms responsible for this in stainless steel SS 316L. The fractography of the tested samples is analysed using an image analyser and the void fraction at failure is correlated with the corresponding mechanisms. The parametric studies on stress relaxation at different pre-strain and relaxation time correlate well with the fractography results supporting the proposed mechanisms. TEM investigation of dislocation structures and void characterisation further confirm the role of dislocation annihilation. Moreover, a novel indentation technique combining micro- and nano-indentation techniques is used to verify the role of stress homogenisation mechanism. 相似文献
748.
Tan L. Jones J.A. Barnett A.C. Zhang H. Moore J.Z. Zhang Q. 《Experimental Techniques》2018,42(5):499-508
Experimental Techniques - A better understanding of needle-tissue interaction forces when needle is inserted into tissue during injection and minimally invasive surgery can lead to more accurate... 相似文献
749.
Lijuan J. Wang Margaret L. Grapperhaus Barnett S. Pitzele Timothy J. Hagen Kam F. Fok Jeffrey A. Scholten Dale P. Spangler Mihaly V. Toth Gina M. Jerome William M. Moore Pamela T. Manning James A. Sikorski 《Heteroatom Chemistry》2002,13(1):77-83
The efficient syntheses of two new types of conformationally constrained S‐[2‐[(1‐iminoethyl)amino]ethyl]homocysteine derivatives, 1‐amino‐3‐[2[(1‐iminoethyl)amino]ethylthio]cyclobutane carboxylic Acid ( 5 ) and (4S)‐4‐[[2‐[(1‐Iminoethyl)amino]ethyl]thio]‐L‐proline ( 6 ), are reported. These molecules represent the first attempts to probe conformational constraint near the α‐amino acid moiety of known homocysteine‐based inhibitors of nitric oxide synthase. Targets 5 and 6 were evaluated as potential inhibitors of the three human isoforms of nitric oxide synthase. © 2002 John Wiley & Sons, Inc. Heteroatom Chem 13:77–83, 2002; DOI 10.1002/hc.1109 相似文献