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21.
Saqlain Abbas Fucai Li Zulkarnain Abbas Taufeeq Ur Rehman Abbasi Xiaotong Tu Riffat Asim Pasha 《声与振动》2021,55(1):1-18
Structural health monitoring (SHM) is recognized as an efficient tool to interpret the reliability of a wide variety of infrastructures. To identify the structural abnormality by utilizing the electromechanical coupling property of piezoelectric transducers, the electromechanical impedance (EMI) approach is preferred. However, in real-time SHM applications, the monitored structure is exposed to several varying environmental and operating conditions (EOCs). The previous study has recognized the temperature variations as one of the serious EOCs that affect the optimal performance of the damage inspection process. In this framework, an experimental setup is developed in current research to identify the presence of fatigue crack in stainless steel (304) beam using EMI approach and estimate the effect of temperature variations on the electrical impedance of the piezoelectric sensors. A regular series of experiments are executed in a controlled temperature environment (25°C–160°C) using 202 V1 Constant Temperature Drying Oven Chamber (Q/TBXR20-2005). It has been observed that the dielectric constant ε33T which is recognized as the temperature-dependent constant of PZT sensor has sufficiently influenced the electrical impedance signature. Moreover, the effective frequency shift (EFS) approach is optimized in term of significant temperature compensation for the current impedance signature of PZT sensor relative to the reference signature at the extended frequency bandwidth of the developed measurement system with better outcomes as compared to the previous literature work. Hence, the current study also deals efficiently with the critical issue of the width of the frequency band for temperature compensation based on the frequency shift in SHM. The results of the experimental study demonstrate that the proposed methodology is qualified for the damage inspection in real-time monitoring applications under the temperature variations. It is capable to exclude one of the major reasons of false fault diagnosis by compensating the consequence of elevated temperature at extended frequency bandwidth in SHM. 相似文献
22.
Rajiv Karmakar Asim Bhaumik Biplab Banerjee Chhanda Mukhopadhyay 《Tetrahedron letters》2017,58(7):622-628
An enhanced one-pot synthesis of new functionalized 5,6-dihydro-5,5-dimethyl-2-phenyl-2H-pyridazino[3,4,5-kl]acridin-1(4H)-one derivatives with different substituted patterns by using mesoporous MCM-41 catalyst via a ring opening/ring closure reaction process has been established. This MCM-41 silica catalyst has been synthesized and characterized using an array of sophisticated analytical techniques like BET, XRD, UHRTEM, etc. This reaction could be conducted from inexpensive substrates within short period under neat reflux conditions. Compared with the usual methods, the remarkable advantages of this method are milder reaction conditions, operational simplicity, higher yields, short reaction times and an environmentally friendly procedure. 相似文献
23.
Asim Debnath 《Liquid crystals》2017,44(14-15):2192-2202
Four multicomponent room temperature mixtures were formulated using a pyrimidine-based achiral matrix as host and four terphenyl-based ester chiral compounds as dopants. Among the four mixtures, two exhibit antiferroelectric and two other exhibit ferroelectric phases at room temperature. Dopant molecules differ from each other by position and number of fluorine atom substitution at the benzoate group of the molecular rigid core. Number and location of fluorine atoms in the dopant structure show significant effect on the phase sequences as well as on different physical properties. All the mixtures found to have moderate spontaneous polarisation, high tilt angle, very fast switching time and low viscosity which are important for liquid crystal-based display applications. 相似文献
24.
New wormhole-like mesoporous TiO2 material has been synthesized through a convenient sol-gel method in the presence of a Schiff base secondary amine hexadecyl-2-pyrrole-methylamine (HPMA) containing chelating donor sites as template or structure directing agent (SDA). SDA molecules can be easily removed from the composite to generate mesoporosity and upon removal of the SDA molecule, this mesoporous TiO2 material showed very high surface area (480 ± 10 m2/g) with an average pore diameter of 2.57 ± 0.05 nm. When Rose Bengal dye is entrapped inside the nanopores of this material, it showed a drastic enhancement (ca. 40-folds) in the photoconductivity vis-à-vis mesoporous TiO2 alone under white light illumination. 相似文献
25.
Sengupta P Sarkar AK Bhaumik U Chatterjee B Roy B Chakraborty US Pal TK 《Biomedical chromatography : BMC》2010,24(12):1342-1349
A simple, high‐throughput and specific high‐performance liquid chromatography tandem mass spectrometry method has been developed and validated according to the FDA guidelines for simultaneous quantification of olmesartan and pioglitazone in rat plasma. The bioanalytical method consists of liquid–liquid extraction and quantitation by triple quadrupole mass spectrometry using electrospray ionization technique, operating in multiple reaction monitoring and positive ion modes. The compounds were eluted isocratically on a C18 column with a mobile phase consisting of a mixture of methanol and water (containing 0.5% formic acid) in a ratio of 9:1. The response to olmesartan and pioglitazone was linear over the range 0.01–10 µg/mL. The validation results demonstrated that the method had satisfactory precision and accuracy across the calibration range. Intra‐ and inter‐day precisions ranged from 0.66 to 3.32 and from 0.94 to 2.93% (%CV), respectively. The accuracy determined at three quality control levels was within 91.27–107.28%. There was no evidence of instability of the analytes in rat plasma following the stability studies. The method proved highly reproducible and sensitive and was successfully applied in a pharmacokinetic study after single dose oral administration of olmesartan and pioglitazone to the rat. Copyright © 2010 John Wiley & Sons, Ltd. 相似文献
26.
The traditional viewpoint of fluid flow considers the transition to turbulence to occur by the secondary and nonlinear instability of wave packets, which have been created experimentally by localized harmonic excitation. The boundary layer has been shown theoretically to support spatiotemporal growing wave fronts by Sengupta, Rao, and Venkatasubbaiah [Phys. Rev. Lett. 96, 224504 (2006)] by a linear mechanism, which is shown here to grow continuously, causing the transition to turbulence. Here, we track spatiotemporal wave fronts to a nonlinear turbulent state by solving the full 2D Navier-Stokes equation, without any limiting assumptions. Thus, this is the only demonstration of deterministic disturbances evolving from a receptivity stage to the full turbulent flow. This is despite the prevalent competing conjectures of the event being three-dimensional and/or stochastic in nature. 相似文献
27.
Asim Kumar Ghosh 《The European Physical Journal B - Condensed Matter and Complex Systems》2011,82(1):19-27
We consider a one-dimensional Ising-like S =
\frac12\frac{1}{2} Heisenberg antiferromagnetic Hamiltonian and study the dynamics of domain wall excitations in presence of both uniform and
staggered Dzyaloshinskii-Moriya interactions. We obtain dispersion relations and dynamical spin
correlation functions, S
x
x
(q, ω) using the basis of domain wall pair states. It is shown that the line shapes of S
x
x
(q, ω) are highly asymmetric over the whole Brillouin zone such that the spectral weights mainly concentrate in the low energy
side. It is observed that presence of staggered Dzyaloshinskii-Moriya interaction explains the experimental results on the
Ising-like
antiferromagnetic compounds CsCoCl3 and CsCoBr3 very well. 相似文献
28.
Asim K. Das Sudhin K. Mondal Goutam Mukherjee 《Reaction Kinetics and Catalysis Letters》2001,73(2):257-265
Cetylpyridinium chloride (CPC) inhibits the Cr(VI) oxidation of ethanol and propan-1-ol while sodium dodecyl sulfate (SDS)
catalyzes the title reactions. At higher values of the [surfactant], the rate attains a limiting value. The micellar effect
has been explained by considering the preferential partitioning of the reactants in terms of the suggested mechanism. Applicability
of the Menger-Portnoy model and Piszkiewicz model to explain the observed micellar effect has been examined.
This revised version was published online in June 2006 with corrections to the Cover Date. 相似文献
29.
Transient response of hot electrons in narrow-gap semiconductors to a step electric field in the presence of a longitudinal quantizing magnetic field has been studied at low temperatures using displaced Maxwellian distribution. The energy and momentum balance equations are used assuming acoustic phonon scattering via deformation potential responsible for the energy relaxation and elastic acoustic phonon scattering together with ionized impurity scattering for momentum relaxation. The calculations for the variation of drift velocity and electron temperature as functions of time are made for n-Hg0.8Cd0.2 Te in the extreme quantum limit at 1.5 K and 4.2 K. The momentum and energy relaxation times are found to be of the same order of magnitudes as with the experimental values. The magnetic field and lattice temperature dependences of the relaxation rates have been investigated.One of the authors, Suchandra Bhaumik, acknowledges the Council of Scientific and Industrial Research (New Delhi) for financial support. 相似文献
30.