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991.
992.
P. Thomsen-Schmidt K. Hasche G. Ulm K. Herrmann M. Krumrey G. Ade J. Stümpel I. Busch S. Schädlich A. Schindler W. Frank D. Hirsch M. Procop U. Beck 《Applied Physics A: Materials Science & Processing》2004,78(5):645-649
High-accuracy film thickness measurements in the range below 100 nm can be made by various complex methods like spectral ellipsometry (SE), scanning force microscopy (SFM), grazing incidence X-ray reflectometry (GIXR), or X-ray fluorescence analysis (XRF). The measurement results achieved with these methods are based on different interactions between the film and the probe. A key question in nanotechnology is how to achieve consistent results on a level of uncertainty below one nanometre with different techniques.Two different types of thickness standards are realised. Metal film standards for X-ray techniques in the thickness range 10 to 50 nm are calibrated by GIXR with monochromatised synchrotron radiation of 8048 eV. The results obtained at four different facilities show excellent agreement. SiO2 on Si standards for SE and SFM in the thickness range 6 to 1000 nm are calibrated by GIXR with monochromatised synchrotron radiation of 1841 eV and with a metrological SFM. Consistent results within the combined uncertainties are obtained with the two methods. Surfaces and interfaces of both types of standards are additionally investigated by transmission electron microscopy (TEM). PACS 61.10.Kw; 68.55.Jk; 06.20.Fn; 06.60.Mr; 07.79.Lh 相似文献
993.
The early evolution of gas chromatography in the former German Democratic Republic (GDR) is surveyed and instrument development is outlined, describing the most important models manufactured in the GDR. The organization of the Arbeitsgemeinschaft für Gas-Chromatographie (Working Group for GC) is chronicled and its activities are discussed. Subsequent parts of this article will deal with the six symposia organized by the Arbeitsgemeinschaft between 1958 and 1968. 相似文献
994.
995.
Liquid chromatography-electrospray ionisation mass spectrometry was evaluated in the high-throughput analysis of microcystins and nodularins, cyanobacterial peptide hepatotoxins. Extracts originating from cyanobacterial strains and field material were separated on a 30 mm × 4 mm I.D. Merck Purospher STAR RP-18e column using a rapid gradient of aqueous formic acid and acetonitrile, ionised by electrospray technique and analysed on a Micromass Quattro II triple-quadrupole mass spectrometer operated in the selected ion recording (SIR) mode. The total analysis time per sample was 2.8 min corresponding to 514 samples a day. The system showed good robustness during a series of 320 repetitive injections of a field sample containing three major microcystins. 相似文献
996.
L.E. Payne 《Journal of Mathematical Analysis and Applications》2003,284(1):283-293
We consider some initial-boundary value problems for the linear and nonlinear heat equation where the gradient of the solution is prescribed on the boundary. Assuming that a solution exists, we obtain bounds for the solution and its gradient by maximum principle arguments or by means of differential and integral inequalities. 相似文献
997.
In this paper we investigate the distribution of the Heisenberg evolution of the number operator in the stochastic limit of
the quantum electromagnetic field without dipole approximation. We prove that in this case the usual Poisson statistics of
the free fields has to be replaced by a hypergeometric series whose coefficients we compute explicitly. The physical effects
of the new statistics should manifest themselves in situation which are not yet in the relativistic regime, but in which the
dipole approximation is no longer valid.
The text was submitted by the authors in English. 相似文献
998.
A study is conducted of the relationship between the asymptotic behavior of a subharmonic function of finite order in a cone and the distribution of the measure associated with it.Translated from Ukrainskii Matematicheskii Zhurnal, Vol. 43, No. 2, pp. 247–261, Febraury, 1991. 相似文献
999.
Michael Demuth Peter Stollmann Günter Stolz Jan van Casteren 《Integral Equations and Operator Theory》1995,23(2):145-153
We give trace norm estimates for products of integral operators and for diffusion semigroups. These are applied to differences of heat semigroups. A natural example of an integral operator with finite trace which is not trace class is given. 相似文献
1000.
I. L. Bataronov T. A. Nadeina 《Bulletin of the Russian Academy of Sciences: Physics》2007,71(10):1370-1374
The instability of the rectilinear form of parallel weakly interacting dislocations, manifesting itself in their spontaneous wave-like bending, has been investigated. It is shown that softening of a crystal leads to the enhancement of this instability. 相似文献