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101.
Forensic analyses of debris from the fatal explosion of an electrochemical cold fusion cell at SRI International were conducted at LLNL at the request of Cal-OSHA. One investigation focused on the possibility of conventional nuclear reaction mechanisms contributing to the total energy inventory of the incident. Selected metal components of the electrolysis apparatus were subjected to nondestructive -ray spectrometry with high-sensitivity, low-background Ge detector systems. The anticipated analytes in these studies were radioactivation products potentially induced in the explosion residue by either fast or thermal neutrons. The results of this investigation were negative within the temporal constraints of the incident and the analytical sensitivities of the instrumentation.  相似文献   
102.
2-Alkynylcyclohex-2-enones 1a–c and 2a–c react with H2O2/NaOH in MeOH to afford 1-alkynyl-7-oxabicyclo[4.1.0]heptan-2-ones 3a–c and 4a–c , respectively. The 3-unsubstituted bicyclic epoxy ketones 3a, 3b , and 4a, 4b react further with H2O2/NaOH, undergoing ring contraction and (formal) decarbonylation to give 2-alkynylcy-clopent-2-enols 5a, 5b , and 6a, 6b , respectively. Epoxy ketones 3 are also obtained under neutral conditions on irradiation (λ = 350 nm) of cyclohexenones 1 in air-saturated benzene solution. Similarly, under neutral conditions oxo-cycloalkenecarbonitriles 8 react (thermally) with H2O2 in MeCN to give the oxabicyclic carbonitriles 9 .  相似文献   
103.
5,5-Dimethyl-1,4,2-dioxazoles are readily installed by transketalization of 2,2-diethoxypropane, where both the NH and OH moieties are protected in a nonprotic form. The dioxazoles are stable to a wide variety of reaction conditions and readily revert back to the hydroxamic acid by treatment with Nafion-H in 2-propanol. The method is applicable to primary, secondary, tertiary, and aromatic hydroxamic acids, and the acidity of the protons adjacent to the dioxazole allows alpha-functionalization.  相似文献   
104.
Grating techniques are used to determine the three-dimensional deformation and the tangential strain of sheet metal. A grating is fixed on the surface and taken by stereo CCD cameras in different deformation states. By suitable line-following software, the grating coordinates in the images are determined with subpixel accuracy. Using photogrammetric methods, the three-dimensional coordinates are calculated from the image coordinates. The strain usually is determined by means of a deformation gradient, which is calculated from every deformed triangle. In this paper, the gradient is determined in the center of four neighboring meshes using a polynomial approximation of the displacement function in a reference position. The influence of the nontangential deformation is considered. By simulation, a flat sheet metal is deformed to a rotational symmetric surface. The difference of the known exact strain is compared with the numerically derived strain with respect to different grating pitches. The proposed method yields good results even in the case of large spatial deformation. It is applied to the deformation of a hatlike test specimen.  相似文献   
105.
We describe the observation of novel localization in mesoscopic quantum dots and quantum dot arrays, which are realized in high mobility GaAs/AlGaAs heterojunctions using the split‐gate technique. With a sufficient gate voltage applied to form the devices, their resistance diverges as the temperature is lowered below a degree Kelvin, behavior which we attribute to localization. Evidence for the localization is found over the entire range of gate voltage for which the dots are defined, persisting to conductances higher than 50e2/h.  相似文献   
106.
Mette Andresen  Lena Lindenskov 《ZDM》2009,41(1-2):213-222
A new concept, compulsory multi-disciplinary courses, was introduced in upper secondary school curriculum as a central part of a recent reform. This paper reports from a case study of such a triple/four-disciplinary project in mathematics, physics, chemistry and ‘general study preparation’ performed under the reform by a team of experienced teachers. The aim of the case study was to inquire how the teachers met the demands of the introduction of this new concept and, to look for signs of new relations established by the students between mathematics and other subjects, as a result of the multi-disciplinary teaching. The study revealed examples of good practice in planning and teaching. In addition, it served to illuminate interesting aspects of how students perceived the school subject mathematics and its relations to other subjects and to common sense.  相似文献   
107.
The MgB2 superconductor, synthesized using solid-state and liquid-phase sintering methods, have been characterized for various properties. The upper critical field, irreversibility line and critical current density have been determined using magnetization data. The current-voltage characteristics recorded under an applied magnetic field revealed the existence of vortex glass transition. The surface analysis using X-ray photoelectron spectroscopy shows that MgB2 is sensitive to atmospheric degradation.  相似文献   
108.
We consider the problem of minimizing the makespan in open shop scheduling. The decision problem whether a given sequence in open shop scheduling is irreducible has already been considered, however, has not been solved yet. A sequence is an acyclic orientation of the Hamming graph K n ×K m . Irreducible sequences in open shop are the local optimal elements. We present two variants of algorithms based on the specific properties of the H-comparability graph. The first is polynomial whereas the second is exponential. The irreducibility is co-NP. The stated properties argue whether it belongs to P. The complexity status of the considered decision problem is updated.  相似文献   
109.
A comparison of relative populations of ZnI and ZnII levels excited in equilibrium plasma, sputtering, gas-phase single collision, and beam foil sources is presented, and includes data on the first reported excitation studies under single collision conditions for a (transition metal atom)-(transition metal ion) interaction. A search for continuum emission from atomic chromium, like that seen during sputtering of chromium metal, produced a negative result.  相似文献   
110.
Let Gn be a complete transitively directed graph with n + 1 vertices v0, v1, …, vn. Let ψ(n) be the number of subgraphs H of Gn where each vertex in H lies along a directed path from v0 to vn in H. ψ(n) and some related quantities are calculated.  相似文献   
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