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31.
Amine Kassouf Maria El Rakwe Hanna Chebib Violette Ducruet Douglas N. Rutledge Jacqueline Maalouly 《Analytica chimica acta》2014
Olive oil is one of the most valued sources of fats in the Mediterranean diet. Its storage was generally done using glass or metallic packaging materials. Nowadays, plastic packaging has gained worldwide spread for the storage of olive oil. However, plastics are not inert and interaction phenomena may occur between packaging materials and olive oil. In this study, extra virgin olive oil samples were submitted to accelerated interaction conditions, in contact with polypropylene (PP) and polylactide (PLA) plastic packaging materials. 3D-front-face fluorescence spectroscopy, being a simple, fast and non destructive analytical technique, was used to study this interaction. Independent components analysis (ICA) was used to analyze raw 3D-front-face fluorescence spectra of olive oil. ICA was able to highlight a probable effect of a migration of substances with antioxidant activity. The signals extracted by ICA corresponded to natural olive oil fluorophores (tocopherols and polyphenols) as well as newly formed ones which were tentatively identified as fluorescent oxidation products. Based on the extracted fluorescent signals, olive oil in contact with plastics had slower aging rates in comparison with reference oils. Peroxide and free acidity values validated the results obtained by ICA, related to olive oil oxidation rates. Sorbed olive oil in plastic was also quantified given that this sorption could induce a swelling of the polymer thus promoting migration. 相似文献
32.
Katritzky AR Abo-Dya NE Abdelmajeid A Tala SR Amine MS El-Feky SA 《Organic & biomolecular chemistry》2011,9(2):596-599
The transprotection of N-Fmoc-cysteine containing di- and tripeptides possessing a free SH group to produce the corresponding S-Fm-cysteine di- and tripeptides bearing a free amino group is accomplished efficiently with DBU in dry THF. The N-Fmoc to S-Fm transformation mechanism is discussed. S-Fm-Cysteine di- and tripeptides readily form amide bonds on coupling with N-(Pg-α-aminoacyl)benzotriazoles and N-(Pg-α-dipeptidoyl)benzotriazoles to give larger peptides. 相似文献
33.
Periodica Mathematica Hungarica - We discuss the rational solutions of the Diophantine equations $$f(x)^2 \pm f(y)^2=z^2$$ . This problem can be solved either by the theory of elliptic curves or by... 相似文献
34.
Amine Asselah Fabienne Castell 《Annales de l'Institut Henri Poincaré (B) Probabilités et Statistiques》2007,43(2):163
We consider a random walk in random scenery {Xn=η(S0)+?+η(Sn),n∈N}, where a centered walk {Sn,n∈N} is independent of the scenery {η(x),x∈Zd}, consisting of symmetric i.i.d. with tail distribution P(η(x)>t)∼exp(−cαtα), with 1?α<d/2. We study the probability, when averaged over both randomness, that {Xn>ny} for y>0, and n large. In this note, we show that the large deviation estimate is of order exp(−ca(ny)), with a=α/(α+1). 相似文献
35.
Amine El Sahili 《Comptes Rendus Mathematique》2002,335(11):859-861
Consider two maps f and g from a set E into a set F such that f(x)≠g(x) for every x in E. What is the maximal cardinal of a subset A of E such that the images of the restriction of f and g to A are disjoint? Mekler, Pelletier and Taylor have shown that it is card(E) when the set E is infinite; in the finite case, we have proved that it is greater than or equal to card(E)/4. In this paper, using graph theoretical technics, we find these results as a direct application of a lemma of Erdös. Moreover, we show that if , then there exists a countable partition {En}n?1 of such that f(En)∩g(En)=φ, for every n?1. To cite this article: A. El Sahili, C. R. Acad. Sci. Paris, Ser. I 335 (2002) 859–861. 相似文献
36.
This paper presents a theoretical formulation in which the stream-tube method (STM) is examined through a variational approach for solving solid strain and fluid flow problems with finite elements. The analysis considers a reference domain, used as computational domain, related to the physical domain by an unknown transformation function to be determined numerically. Mass conservation is automatically verified by STM. The variational approach leads to eliminate the pressure in fluid problems and avoids to set up a mixed displacement–pressure procedure in the case of incompressible solids. Examples are given for fluid flows, applications and comparisons are also provided in the bending problem in elasticity. 相似文献
37.
Ion conductive characteristics of cross-linked network polysiloxane-based solid polymer electrolytes
Z. C. Zhang J. J. Jin F. Bautista L. J. Lyons N. Shariatzadeh D. Sherlock K. Amine R. West 《Solid State Ionics》2004,170(3-4):233-238
A series of cross-linked network polysiloxanes containing oligoethylene oxide units, (OCH2CH2)n, as internal free chains have been synthesized by performing hydrosilylation of partially PEO-substituted polysiloxane precursor with , ω-diallyl terminated poly(ethylene glycol). The polymer electrolytes were formed by complexing with LiN(CF3SO2)2 electrolyte salt and exhibited superior conductive property. The σRT of the network polymer electrolytes is in the range of 2.50×10−5 to 1.62×10−4 S/cm and depends on the cross-linking density (in terms of Si–H amount of the siloxane precursor), repeating unit number of internal oligoethylene oxide and chain length of the cross-linker. The significant enhancement of the conductivity was observed when low molecular weight dimethyl poly(ethylene glycol) was added as plasticizer. The temperature dependence of the ionic conductivity was also studied, following the Vogel–Tamman–Fulcher (VTF) equation. 相似文献
38.
39.
Amine Makkouk 《Mathematische Annalen》1973,204(3):199-201
Sans résumé 相似文献
40.
Amine Fawaz 《Central European Journal of Mathematics》2007,5(3):493-504
We compute the energy of conformal flows on Riemannian manifolds and we prove that conformal flows on manifolds of constant
curvature are critical if and only if they are isometric.
相似文献